nav emailalert searchbtn searchbox tablepage yinyongbenwen piczone journalimg searchdiv qikanlogo popupnotification paper
2025 05 v.46 112-121
退火温度和时间对W350高牌号无取向硅钢组织及织构的影响
基金项目(Foundation): 国家自然科学基金(51804003,52374316); 安徽省教育厅科学研究重点项目(2022AH050291); 江西省重大科研专项项目(20213AAE01009)
邮箱(Email): whjchina@yeah.net;
DOI: 10.13289/j.issn.1009-6264.2024-0332
中文作者单位:

安徽工业大学冶金工程学院;钢铁研究总院有限公司;

摘要(Abstract):

采用光学显微镜与X射线衍射仪(XRD)研究了不同温度(850、900和950℃)退火保温不同时间(2、3、5和7 min)对W350高牌号无取向硅钢显微组织和宏观织构的影响。结果表明:W350高牌号无取向硅钢冷轧板的显微组织存在较多形变带,织构类型以γ纤维织构和α纤维织构为主;经850~950℃退火后,样品均发生了完全再结晶,形变带全部消失,呈现等轴晶组织形态;整体上看,退火温度越高,保温时间越长,再结晶所形成的平均晶粒尺寸越大,退火板织构类型主要是γ纤维织构和α*纤维织构。与冷轧试样相比,随退火温度的升高和保温时间的延长,α纤维织构逐渐向α*纤维织构转化和立方织构向{001}<210>聚集,且γ纤维织构组分与强度明显降低;保温2和3 min时,随退火温度的升高,因平均晶粒尺寸的增大,试样的铁损始终逐渐降低,但保温5和7 min时,随退火温度升高,铁损先下降后上升,950℃退火时,保温时间过长导致晶粒过大,铁损出现升高现象。总体上看,随着退火温度的升高和保温时间的延长,W350无取向硅钢的磁感应强度始终在降低,但变化范围较小,在950℃退火保温3 min后,其磁性能最佳,P1.5/50=2.48 W/kg,B50=1.680 T。

关键词(KeyWords): 无取向硅钢;退火;组织;织构;磁性能
参考文献

[1] 程朝阳,钟柏林,倪正轩,等.新能源汽车驱动电机用高强无取向硅钢力、磁性能调控研究进展[J].工程科学学报,2023,45(9):1482-1492.CHENG Zhao-yang,ZHONG Bo-lin,NI Zheng-xuan,et al.Research progress on simultaneous control of mechanical and magnetic properties of high-strength non-oriented silicon steel for new energy vehicle driving motors[J].Chinese Journal of Engineering,2023,45(9):1482-1492.

[2] 龚坚,罗海文.新能源汽车驱动电机用高强度无取向硅钢片的研究与进展[J].材料工程,2015,43(6):102-112.GONG Jian,LUO Hai-wen.Progress on the research of high-strength non-orientde silicon steel sheets in traction motors of hybrid/electrical vehicles[J].Materials Engineering,2015,43(6):102-112.

[3] 石文敏,杨光,吴章汉,等.退火加热速度对高牌号无取向硅钢组织、织构及磁性能的影响[J].材料热处理学报,2023,44(4):138-145.SHI Wen-min,YANG Guang,WU Zhang-han,et al.Effect of heating rate on microstructure,texture and magnetic properties of high grade non-oriented silicon steel during annealing[J].Transactions of Materials and Heat Treatment,2023,44(4):138-145.

[4] 焦海涛.薄带连铸高牌号无取向硅钢热处理工艺研究 [D].沈阳:东北大学,2015.JIAO Hai-tao.Study on heat treatment process for high-grade non-oriented silicon steel produced by strip casting [D].Shenyang:Northeastern University,2015.

[5] 王健,李俊,郭文渊,等.冷轧无取向硅钢再结晶退火组织和织构演变研究进展[J].材料导报,2010,24(19):100-103.WANG Jian,LI Jun,GUO Wen-yuan,et al.Process in evolution of structure and texture during annealing in cold rolled non-oriented silicon steel[J].Materials Review,2010,24(19):100-103.

[6] Park J T,Szpunar J A,Cha S Y.Effect of heating rate on the development of annealing texture in nonoriented electrical steels[J].ISIJ International,2003,43(10):1611-1614.

[7] 谭玄,袁童欣,尤学文,等.退火温度对3.1Si-0.8Al-1.3Mn高强无取向硅钢组织与性能的影响[J].材料热处理学报,2022,43(10):136-144.TAN Xuan,YUAN Tong-xin,YOU Xue-wen,et al.Effect of annealing temperture on microstructure and properties of 3.1Si-0.8Al-1.3Mn high strength non-oriented silicon steel[J].Transactions of Materials and Heat Treatment,2022,43(10):136-144.

[8] 张婷.双辊铸轧 3% Si 无取向硅钢薄带组织、织构的演变规律[D].沈阳:东北大学,2010.ZHANG Ting.Evolution on the Microstructure and texture of the 3%Si non-oriented silicon steels prepared by twin-roll casting process[D].Shenyang:Northeastern University,2010.

[9] Lin Y,Wang H,Wei H,et al.Thick-gauge ultra-high-strength high-silicon non-oriented silicon steel with balanced mechanical and magnetic properties controlled by partial recrystallization annealing[J].JOM,2022,74(10):3788-3798.

[10] Zhong B,Cheng Z,Volkova O,et al.Effect of microstructure modification on magnetic and mechanical properties of high-grade non-oriented silicon steel during annealing treatment[J].Journal of Materials Research and Technology,2023,27:7730-7739.

[11] Yasuda M,Kataoka T,Ushigami Y,et al.Texture evolution during recrystallization and grain growth in heavily cold-rolled Fe-3%Si alloy[J].ISIJ International,2018,58(10):1893-1900.

[12] 于雷,罗海文.部分再结晶退火对无取向硅钢的磁性能与力学性能的影响[J].金属学报,2019,56(3):291-300.YU Lei,LUO Hai-wen.Effect of partial recrystallization annealing on magnetic properties and mechanical properties of non-oriented silicon steel[J].Acta Metallurgica Sinica,2019,56(3):291-300.

[13] Park J T,Szpunar J A.Effect of initial grain size on texture evolution and magnetic properties in nonoriented electrical steels[J].Journal of Magnetism and Magnetic Materials,2009,321(13):1928-1932.

[14] An L Z,Wang Y P,Wang G D,et al.Fabrication of high-performance low silicon non-oriented electrical steels by a new method:Low-finishing-temperature hot rolling combined with batch annealing[J].Journal of Magnetism and Magnetic Materials,2022,546:168907.

[15] 张永刚,王星,周琳琳,等.热轧工艺对Zr-Sn-Nb锆合金板材组织与性能的影响[J].金属热处理,2019,44(8):118-121.ZHANG Yong-gang,WANG Xing,ZHOU Lin-lin,et al.Effect of hot rolling process on microstructure and properties of Zr-Sn-Nb zirconium alloy sheet[J].Heat Treatment of Metals,2019,44(8):118-121.

[16] 苏梦瑶,王阿龙,李苗苗.表面温度对铁素体不锈钢组织和性能的影响[J].特种铸造及有色合金,2019,39(10):1065-1068.SU Meng-yao,WANG A-long,LI Miao-miao.Effects of surface temperature on microstructure and mechanical properties of ferritic stainless Steel[J].Special Casting & Nonferrous Alloys,2019,39(10):1065-1068.

[17] Quan G Z,Zhang P,Zhang Y Q,et al.Characterization of grain growth behaviors by BP-ANN and Sellars models for nickle-base superalloy and their comparisons[J].Transactions of Nonferrous Metals Society of China,2020,30(9):2435-2448.

[18] Jiao H T,Xie X X,Wu W,et al.Effect of pre-recovery annealing on recrystallisation behaviour of strip-cast non-oriented electrical steel[J].Materials Science and Technology,2023,39(10):1255-1266.

[19] 毛卫民,杨平.电工钢的材料学原理[M].北京:高等教育出版社,2013.MAO Wei-ming,YANG Ping.Material Science Principles on Electrical Steels[M].Beijing:Higher Education Press,2013.

[20] Wang J,LI J,Wang X F,et al.Effect of heating rate on microstructure evolution and magnetic properties of cold rolled non-oriented electrical steel[J].Journal of Iron and Steel Research International,2010,17(11):54-61.

[21] 雷秀川.5xxx系铝合金再结晶动力学及其形核机制的研究[D].重庆:重庆大学,2021.LEI Xiu-chuan.Recrystallization Kinetics and nucleation mechanism of 5xxx aluminum alloys[D].Chongqing:Chongqing University,2021.

[22] 朱志勇,郭海荣,李化龙.常化温度对50W470无取向硅钢组织及磁性能的影响[J].上海金属,2018,40(6):50-54.ZHU Zhi-yong,GUO Hai-rong,LI Hua-long.Influence of normalizing temperature on microstructure and magnetic properties of 50W470 non-oriented silicon steel[J].Shanghai Metal,2018,40(6):50-54.

[23] 杨洁,侯迪文,王佳乐,等.Fe-1.5%Si无取向硅钢的冷轧变形组织及织构演变[J].金属热处理,2023,48(12):166-174.YANG Jie,HOU Di-wen,WANG Jia-le,et al.Microstructure and texture evolution of cold-rolled deformed Fe-1.5%Si non-oriented silicon steel[J].Heat Treatment of Metals,2023,48(12):166-174.

[24] 谢顺卿,焦海涛,韩琼琼,等.不同冷轧退火工艺下薄带连铸无取向硅钢的组织和磁性能[J].机械工程材料,2016,40(5):25-30.XIE Shun-qing,JIAO Hai-tao,HAN Qiong-qiong,et al.Microstructure and magnetic properties of strip-casting non-oriented silicon steel at different cold rolling and annealing processes[J].Materials for Mechanical Engineering,2016,40(5):25-30.

[25] Li N,Ma L,Xiang L,et al.Evolution of texture in a 2.8% Si non-oriented electrical steel annealed at 1100 ℃[J].Materials Transactions,2014,55(2):387-390.

[26] Yasuda M,Kataoka T,Ushigami Y,et al.Texture evolution during recrystallization and grain growth in heavily cold-rolled Fe-3%Si alloy[J].ISIJ International,2018,58(10):1893-1900.

[27] Qin J,Yang J,Zhang Y,et al.Strong {1 0 0}〈0 1 2〉-{4 1 1}〈1 4 8〉 recrystallization textures in heavily hot-rolled non-oriented electrical steels[J].Materials Letters,2020,259:126844.

[28] Jain V,Modak P,Patra S,et al.Origin of Goss texture in grain oriented electrical steel:Role of shear bands[J].Materialia,2022,22:101398.

基本信息:

DOI:10.13289/j.issn.1009-6264.2024-0332

中图分类号:TG142.1;TG156.2

引用信息:

[1]尹萍,牛宇豪,邵凯旋等.退火温度和时间对W350高牌号无取向硅钢组织及织构的影响[J].材料热处理学报,2025,46(05):112-121.DOI:10.13289/j.issn.1009-6264.2024-0332.

基金信息:

国家自然科学基金(51804003,52374316); 安徽省教育厅科学研究重点项目(2022AH050291); 江西省重大科研专项项目(20213AAE01009)

检 索 高级检索

引用

GB/T 7714-2015 格式引文
MLA格式引文
APA格式引文