0Cr18Ni9钢表面熔盐法渗硅层的组织与性能Microstructure and properties of silicide layer deposited on 0Cr18Ni9 stainless steel by siliconizing in molten salt
安亮,贾建刚,尤少君,马勤,郭铁明,季根顺
摘要(Abstract):
利用摩尔比为NaCl∶KCl∶NaF=2∶2∶1的碱金属卤化物混合体系做载体,等摩尔比的Na2SiF6和Si粉作渗硅剂,在900℃下利用熔融盐法对0Cr18Ni9不锈钢进行了渗硅处理。采用X射线衍射仪(XRD)和附带能量色散谱仪(EDS)附件的扫描电子显微镜(SEM)研究了渗层截面的物相组成、成分、显微形貌及渗硅层的形成机理。结果表明,900℃下保温3 h渗层厚度在250μm以上,渗层物相为富含Cr、Ni合金元素的Fe3Si型金属间化合物,渗层中Si的含量为6.75 wt%,Cr的含量仅为其在基体中含量的50%左右,Ni在基体和渗层中的含量相当,渗层表面致密,硬度在700 HV左右,远高于基体硬度200 HV。
关键词(KeyWords): Fe3Si;硅化物渗层;渗硅机理;0Cr18Ni9不锈钢
基金项目(Foundation): 国家自然科学青年基金项目(51001057)
作者(Author): 安亮,贾建刚,尤少君,马勤,郭铁明,季根顺
DOI: 10.13289/j.issn.1009-6264.2011.03.029
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