不同Al2O3含量的Al2O3/Cu复合材料的热变形行为Hot deformation behavior of Al2O3/Cu composites with different Al2O3 contents
徐国杨,国秀花,李韶林,宋克兴,刘嵩,肖振朋
摘要(Abstract):
为探究Al_2O_3含量对Al_2O_3/Cu复合材料热变形行为的影响,采用内氧化法制备了3种Al_2O_3含量(0.28、0.66和1.13 mass%)的Al_2O_3/Cu复合材料,通过热模拟实验对其热变形行为进行了研究。结果表明:在823、923和1223 K时,随着Al_2O_3/Cu复合材料中Al_2O_3含量的增加,复合材料的峰值应力逐渐增大;显微组织观察发现,由于1.13 Al_2O_3/Cu复合材料内动态软化积累程度最大,导致其在1023和1123 K下出现了峰值应力下降现象。经热挤压后,在热变形过程中Al_2O_3/Cu复合材料的软化效果以动态回复为主。同时,发现0.28 Al_2O_3/Cu和0.66 Al_2O_3/Cu复合材料的热激活能相近,1.13 Al_2O_3/Cu复合材料的热激活能远高于前两者,并分别获得了不同Al_2O_3含量的Al_2O_3/Cu复合材料本构关系。采用动态材料模型(DMM)建立了Al_2O_3/Cu复合材料的热加工图,随着Al_2O_3含量的增加,热加工图中功率耗散系数η>0.3区域逐渐减小且向高温高应变速率方向移动;就失稳面积而言,0.66 Al_2O_3/Cu复合材料的失稳区域占比最小。
关键词(KeyWords): Al_2O_3/Cu复合材料;热压缩;本构关系;热激活能;热加工图
基金项目(Foundation): 中国博士后科学基金(2020T130172,2020M682288);; 河南省重点研与推广专项(212102210110);; 河南省博士后经费资助(202002063);; 河南省高等学校重点科研项目(21A430014)
作者(Author): 徐国杨,国秀花,李韶林,宋克兴,刘嵩,肖振朋
DOI: 10.13289/j.issn.1009-6264.2022-0613
参考文献(References):
- [1] 张雪辉,魏星,刘美霞,等.Al2O3/Cu复合材料的高温变形行为[J].复合材料学报,2017,34(8):1825-1832.ZHANG Xue-hui,WEI Xing,LIU Mei-xia,et al.High temperature deformation behavior of Al2O3/Cu composites[J].Acta Materiae Compositae Sinica,2017,34(8):1825-1832.
- [2] Ren F Z,Zhi A J,Zhang D W,et al.Preparation of Cu-Al2O3 bulk nano-composites by combining Cu-Al alloy sheets internal oxidation with hot extrusion[J].Journal of Alloys and Compounds,2015,633(5):323-328.
- [3] Zhang X H,Zhang Y,Tian B H,et al.Review of nano-phase effects in high strength and conductivity copper alloys[J].Nanotechnology Reviews,2019,8(1):383-395.
- [4] 冯江,宋克兴,梁淑华,等.混杂增强铜基复合材料的设计与研究进展[J].材料热处理学报,2018,39(5):1-9.FENG Jiang,SONG Ke-xing,LIANG Shu-hua,et al.Design and research progress of hybrid reinforced copper matrix composites[J].Transactions of Materials and Heat Treatment,2018,39(5):1-9.
- [5] 李玄,赵科,刘金铃.20 vol%体积分数纳米Al2O3颗粒增强铝基复合材料的高温压缩性能[J].复合材料学报,2023,40(2):1118-1128.LI Xuan,ZHAO Ke,LIU Jin-ling.High-temperature compressive properties of 20 vol% volume fraction nano-Al2O3 particles reinforced aluminum matrix composite[J].Acta Materiae Compositae Sinica,2023,40(2):1118-1128.
- [6] 张彦敏,王永健,陈赛,等.Cu-Al2O3(0.68%)弥散强化铜合金塑性变形特性[J].精密成形工程,2017,9(5):128-133.ZHANG Yan-min,WANG Yong-jian,CHEN Sai,et al.Plastic deformation characteristics of Cu-Al2O3(0.68%) dispersion strengthened copper alloy[J].Journal of Netshape Forming Engineering,2017,9(5),128-133.
- [7] 杨雪瑞,田保红,张毅,等.纳米和微米Al2O3混杂颗粒增强弥散铜组织和热变形行为[J].材料热处理学报,2014,35(1):1-5.YANG Xue-rui,TIAN Bao-hong,ZHANG Yi,et al.Microstructure and hot deformation behavior of nano and micron hybrid Al2O3 particles dispersion strengthened copper base composites[J].Transactions of Materials and Heat Treatment,2014,35(1):1-5.
- [8] Guo M X,Wang F,Huang G J,et al.Influences of strain rate and load direction on the thermo-mechanical behavior of a nano-alumina-containing copper alloy bar[J].Journal of Electronic Materials,2015,44(10):3523-3533.
- [9] Guo M X,Wang M P.The compression characteristics of particle-containing Cu alloys under different conditions[J].Materials Science and Engineering A,2012,556(10):807-815.
- [10] Guo M X,Wang M P.Effects of particle size,volume fraction,orientation and distribution on the high temperature compression and dynamical recrystallization behaviors of particle-containing alloys[J].Materials Science and Engineering A,2012,546(1):15-20.
- [11] Xiang Z Q,Zhou L,Lei Q,et al.High temperature mechanical behavior of alumina dispersion strengthened copper alloy with high content of alumina[J].Transactions of Nonferrous Metals Society of China,2015,25(2):444-450.
- [12] 张晓伟.弥散铜复合材料的性能分析与动态再结晶研究[J].有色金属材料与工程,2017,38(4):210-214.ZHANG Xiao-wei.Performance analysis and dynamic recrystallization of Cu-Al2O3 composites[J].Nonferrous Metal Materials and Engineering,2017,38(4):210-214.
- [13] Malas J C,Seetharaman V.Using material behavior models to develop process control strategies[J].JOM,1992,44(6):8-13.
- [14] 贾超凡,苏娟华,李韶林,等.服役参数对Cf-Al2O3/Cu复合材料摩擦磨损性能的影响[J].材料热处理学报,2022,43(8):27-36.JIA Chao-fan,SU Juan-hua,LI Shao-lin,et al.Effect of service parameters on friction and wear properties of Cf-Al2O3/Cu composites[J].Transactions of Materials and Heat Treatment,2022,43(8):27-36.
- [15] 林焕然.载流摩擦领域用新型(WC+SiCw)/Cu-Al2O3 复合材料制备及其性能研究[D].洛阳:河南科技大学,2021.LIN Huan-ran.Preparation and properties of new (WC+SiCw)/Cu-Al2O3 composites for current carrying friction field[D].Luoyang:University of Science and Technology Henan,2021.
- [16] 王颂博,李全安,陈晓亚,等.Mg-11Gd-3Y-1.1Zn-0.5Zr的高温热压缩行为及热加工图[J].材料导报,2020,34(18):18104-18108.WANG Song-bo,LI Quan-an,CHEN Xiao-ya,et al.High temperature thermal compression behavior and processing map of Mg-11Gd-3Y-1.1Zn-0.5Zr[J].Materials Reports,2020,34(18):18104-18108.
- [17] Krishna S C,Muneshwar P,Pant B,et al.Hot deformation behavior and processing map of Cu-Cr-Nb-Zr alloy[J].Journal of Materials Engineering and Performance,2021,31(4):1325-1337.
- [18] An J C,Zhou M,Tian B H,et al.Hot deformation behavior of nano-Al2O3-dispersion-strengthened Cu20W composite[J].Science and Engineering of Composite Materials,2021,28(1):500-515.
- [19] 曹召勋,王军,刘辰,等.铸态Mg-2Y-0.8Mn-0.6Ca-0.5Zn镁合金热变形行为研究[J].材料导报,2022,36(S1):431-435.CAO Zhao-xun,WANG Jun,LIU Chen,et al.Study on hot deformation behavior of as cast Mg-2Y-0.8Mn-0.6Ca-0.5Zn magnesium alloy[J].Materials Reports,2022,36(S1):431-435.
- [20] Bobbili R,Madhu V.Hot deformation behavior and processing maps of Ti-15Al-12Nb alloy[J].Rare Metals,2016,41(10):2316-2323.
- [21] 郭利平,何学清,阳代军,等.Cu-0.5Cr-0.1Zr合金的热压缩变形行为[J].金属热处理,2021,46(9):180-187.GUO Li-ping,HE Xue-qing,YANG Dai-jun,et al.Hot compression deformation behavior of Cu-0.5Cr-0.1Zr alloy[J].Heat Treatment of Metals,2021,46(9):180-187.
- [22] 梁后权,郭鸿镇,宁永权,等.基于软化机制的TC18钛合金本构关系研究[J].金属学报,2014,50(7):871-878.LIANG Hou-quan,GUO Hong-zhang,NING Yong-quan,et al.Analysis on the constitutive relationship of TC18 titanium alloy based on the softening mechanism[J].Acta Metallurgica Sinica,2014,50(7):871-878.
- [23] Najafizadeh A,Jonas J J.Predicting the critical stress for initiation of dynamic[J].ISIJ International,2006,46(11):1679-1684.
- [24] 郭明星.纳米弥散强化铜合金短流程制备方法及其相关基础问题研究[D].长沙:中南大学,2008.GUO Ming-xing.Short-flowing preparation methods and several fundamental research of nanoparticle dispersion strengthened copper alloys[D].Changsha:Central South University,2008.
- [25] Li C M,Huang L,Zhao M J,et al.Influence of hot deformation on dynamic recrystallization behavior of 300M steel:Rules and modeling[J].Materials Science and Engineering A,2020,797(21):139925.
- [26] 刘超,王鑫,门月,等.Ti-6Al-4V合金热压缩过程中的动态再结晶[J].材料研究学报,2021,35(8):583-590.LIU Chao,WANG Xin,MEN Yue,et al.Dynamic recrystallization of Ti-6Al-4V alloy during hot compression[J].Chinese Journal of Materials Research,2021,35(8):583-590.
- [27] 张兵,刘鹏茹,陈韩锋,等.铸态GH2132合金热变形行为和热加工图[J].中国有色金属学报,2022,32(2):466-475.ZHANG Bing,LIU Peng-ru,CHEN Han-feng,et al.Thermal deformation behavior and hot processing map of as-cast GH2132 alloy[J].The Chinese Journal of Nonferrous Metals,2022,32(2):466-475.
- [28] Zhang H D,Liu Y,Zhang F,et al.Hot deformation behavior and processing maps of diamond/Cu composites[J].Metallurgical and Materials Transactions A,2018,49(6):2202-2212.
- [29] Zhang Y,Chai Z,Volinskyalex A,et al.Processing maps for the Cu-Cr-Zr-Y alloy hot deformation behavior[J].Materials Science and Engineering A,2016,662(26):320-329.
- [30] Xi T,Yang C G,Babar S M,et al.Study of the processing map and hot deformation behavior of a Cu-bearing 317LN austenitic stainless steel[J].Materials & Design,2015,87(15):303-312.
- [31] Zhang L,Li Z,Qian L,et al.Hot deformation behavior of Cu-8.0Ni-1.8Si-0.15Mg alloy[J].Materials Science and Engineering A,2011,528(3):1641-1647.
- [32] Patnamsetty M,Somani M C,Ghosh S,et al.Processing map for controlling microstructure and unraveling various deformation mechanisms during hot working of Co Cr Fe Mn Ni high entropy alloy[J].Materials Science and Engineering A,2020,793:139840.
文章评论(Comment):
|
||||||||||||||||||
|
||||||||||||||||||