短碳纤维表面电沉积均匀镀铜工艺Deposition of homogeneous copper layer on short carbon fibers using electrochemical method
程韬,贾建刚,马勤,季根顺,郭铁明
摘要(Abstract):
采用X射线衍射仪(XRD)和扫面电子显微镜(SEM)研究了短碳纤维表面镀铜层的物相及镀铜层的生长过程,分析了电沉积镀铜机理,优化了其工艺。结果表明,当镀铜电压为1 V时,Cu在碳纤维表面择优位置形核,形核率和长大速度较低,沉积30 min碳纤维表面形成的Cu镀层不完整;1.5 V时沉积30 min的Cu镀层完整性较1 V时明显改善,电压为2 V时沉积30 min可以得到均匀的镀层;当电压为2.5 V时,Cu镀层生长速度显著加快,镀层易脱落。
关键词(KeyWords): 短碳纤维;电沉积;镀铜;增强体
基金项目(Foundation): 国家自然科学基金青年基金项目(51001057);; 兰州理工大学红柳青年教师培养计划(201203)
作者(Author): 程韬,贾建刚,马勤,季根顺,郭铁明
DOI: 10.13289/j.issn.1009-6264.2014.09.033
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