等通道转角挤压制备7075Al/AZ31复合板界面组织及结合强度Interfacial microstructure and bonding strength of 7075Al/AZ31 composite plates fabricated by equal channel angular pressing
任广笑,王红霞,周斌,刘一鸣,王斌兵
摘要(Abstract):
在573 K,通过等通道转角挤压成功制备了7075Al/AZ31复合板,并采用SEM、EDS、XRD和剪切实验研究了挤压道次及退火温度对复合板界面层组织和性能的影响及剪切断裂面的组成。结果表明:1道次等通道转角挤压制备的复合板界面处形成厚度为20μm均匀致密的扩散层,由Al_3Mg_2相和Mg_(17)Al_(12)相组成,Al_3Mg_2相层厚(17μm)是Mg_(17)Al_(12)相层厚(3μm)的5.6倍。2道次等通道挤压后,扩散层厚度无变化,但是出现了裂纹,剪切强度大幅下降,剪切断裂面发生在Al_3Mg_2相层。复合板界面层在473 K退火,扩散层厚度无变化,裂纹无改善,剪切强度略有提高;573 K退火,复合板扩散层中的Al_3Mg_2相层和β-Mg_(17)Al_(12)相层均急剧增厚,微裂纹被焊合,剪切强度均大幅下降。在相同处理状态下,1道次ECAP复合板剪切强度均高于2道次ECAP复合板,473 K退火处理后,强度高出30.11%。573 K退火处理后,强度高出12.4%。故利用等通道转角挤压法制备7075Al/AZ31复合板,1道次比较合适,扩散层退火温度不宜超过473 K。
关键词(KeyWords): 复合板;等通道转角挤压;界面微观组织;结合强度
基金项目(Foundation): 国家自然科学基金(51301118);; 山西省国际合作项目(2014081002);; 山西省高等学校科技创新项目(2013108)
作者(Author): 任广笑,王红霞,周斌,刘一鸣,王斌兵
DOI: 10.13289/j.issn.1009-6264.2016.05.007
参考文献(References):
- [1]Aghion E,Bronfin B,Eliezer D.The role of the magnesium industry in protecting the environment[J].Journal of Materials Processing Technology,2001,117:381-385.
- [2]Xu S N,Ikpi M E,Dong J H,et al.Effects of cadmium alloying on the corrosion and mechanical properties of magnesium[J].International Journal of Electrochemical Science,2012,7:4735-4755.
- [3]Zhang T,Shao Y W,Meng G Z,et al.Corrosion of hot extrusion AZ91 magnesium alloy:I-relation between the microstructure and corrosion behavior[J].Corrosion Science,2011,53:1960-1968.
- [4]Liu F C,Liang W,Li X R,et al.Improvement of corrosion resistance of pure magnesium via vacuum pack treatment[J].Journal of Alloys and Compounds,2008,461:399-403.
- [5]张艳,梁伟,王红霞,等.AZ91D镁合金表面真空扩散渗铝层结构及性能研究[J].稀有金属材料与工程,2008,37(11):2023-2026.ZANG Yan,LIANG Wei,WANG Hong-xia,et al.Research on microstructure and properties of aluminum alloyed coating on AZ91D magnesium alloy by vacuum solid diffusion[J].Rare Metal Materials and Engineering,2008,37(11):2023-2026.
- [6]Li X R,Liang W,Zhao X G,et al.Bonding of Mg and Al with Mg-Al eutectic alloy and its application in aluminum coating on magnesium[J].Journal of Alloys and Compounds,2009,471:408-411.
- [7]朱波,梁伟,李线绒.热压法制备镁铝复合板的层界面组织与性能研究[J].热加工工艺,2011,40(16):100-102.ZHU Bo,LIANG Wei,LI Xian-rong.Microstructure and properties of magnesium-aluminum laminated composite plate prepared by hot pressing[J].Hot Working Technology,2011,40(16):100-102.
- [8]Yan Y B,Zhang Z W,Shen W,et al.Microstructure and properties of magnesium AZ31B-aluminum 7075 explosively welded composite plate[J].Materials Science and Engineering A,2010,527:2241-2245.
- [9]Zhang X P,Yang T H,Castagne S,et al.Proposal of bond criterion for hot roll bonding and its application[J].Materials and Design,2011,32:2239-2245.
- [10]Bae J H,Rao AP,Kim K H,et al.Cladding of Mg alloy with Al by twin-roll casting[J].Scripta Materialia,2011,64:836-839.
- [11]LUO Chang-zeng,LIANG Wei,CHEN Zhi-qiang,et al.Effect of high temperature annealing and subsequent hot rolling on microstructural evolution at the bond-interface of Al/Mg/Al alloy laminated composites[J].Materials Characterization,2013,84:34-40.
- [12]Liu X B,Chen R S,Han E H.Preliminary investigations on the Mg-Al-Zn/Al laminated composite fabricated by equal channel angular extrusion[J].Journal of Materials Processing Technology,2009,209:4675-4681.
- [13]Wang S Q,Liang W,Wang Y,et al.A modified die for equal channel angular pressing[J].Journal of Materials Processing Technology,2009,209(7):3182-3186.
- [14]周金枝,姜久红.材料力学[M].武汉:武汉理工大学出版社,2013:87-97.
- [15]陈泽军,刘庆,王国华,等.1100/7075/1100复合板热轧复合和热处理工艺[J].材料热处理学报,2015,36(6):154-158.CHEN Ze-jun,LIU Qing,WANG Guo-hua,et al.Fabrication of 1100/7075/1100 aluminum alloy clad sheet by hot roll bonding and heat treatment[J].Transactions of Materials and Heat Treatment,2015,36(6):154-158.
- [16]付晓鹏,梁伟,李线绒,等.AZ91D镁合金表面覆铝的显微组织及性能[J].金属热处理,2009,34(11):23-26.FU Xiao-peng,LIANG Wei,LI Xian-rong,et al.Microstructure and properties of AZ91D magnesium alloy coated with aluminum foil[J].Heat Treatment of Metals,2009,34(11):23-26.
- [17]赵品,谢辅洲,孙振国,等.材料科学基础教程[M].哈尔滨:哈尔滨工业大学出版社,2003.
- [18]刘政军,刘继伟,苏允海,等.Mg/Al固相连接接头扩散界面区的显微组织[J].沈阳工业大学学报,2015,37(4):377-381.LIU Zheng-jun,LIU Ji-wei,SU Yun-hai,et al.Microstructure of diffusion interface region of Mg/Al solid phase connection joint[J].Journal of Shenyang University of Technology,2015,37(4):377-381.
- [19]Zhang X P,Yang T H,Castagne S,et al.Proposal of bond criterion for hot roll bonding and its application[J].Materials and Design,2011,32:2239-2245.
- [20]Zhu B,Liang W,Li X R.Interfacial microstructure,bonding strength and fracture of magnesium-aluminum laminated composite plates fabricated by direct hot pressing[J].Materials Science and Engineering A,2011,528:6584-6588.
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