Al2O3/Cu多孔复合材料的微观形貌和压缩性能Morphology and compressive properties of Al2O3/Cu porous composites
杨腾,佟海云,郑毅,储爱民,董泽熙,李滔,赵玉萍
摘要(Abstract):
采用高能球磨-粉末冶金法制备了Al_2O_3/Cu多孔复合材料(A-C-M)。首先利用高能球磨法将Cu粉和Al_2O_3粉末均匀细化,然后将Al_2O_3/Cu复合粉末与造孔剂尿素均匀混合后,再将混合粉末冷压成型,最后通过溶脱-烧结工艺制得A-C-M。采用X射线衍射(XRD)和扫描电镜(SEM)对粉末原料和A-C-M的微观形貌进行表征分析,使用万能试验机对A-C-M进行压缩性能测试,探讨了尿素和Al_2O_3含量对A-C-M性能的影响。结果表明:高能球磨使Al_2O_3/Cu复合粉末的形貌由球状变为片状,复合粉末尺寸先减小后增大,在球磨4 h时获得最小平均粒径为25μm; A-C-M含有两种特征孔,100~300μm的大孔和1~10μm的微孔;随尿素含量的增加,孔的连通程度及复合材料的孔隙率逐渐增加,其压缩强度逐渐降低;随Al_2O_3含量的增加,A-C-M孔隙率逐渐增加,其压缩强度逐渐降低,当Al_2O_3含量为4 mass%时,A-C-M的压缩强度急剧下降。
关键词(KeyWords): Al_2O_3/Cu多孔复合材料;高能球磨;微观形貌;压缩性能;尿素
基金项目(Foundation): 国家自然科学基金(52174344);; 湖南省自然科学基金(2023JJ30222,2021JJ30250);; 湖南省大学生创业训练项目(S202210534024X)
作者(Author): 杨腾,佟海云,郑毅,储爱民,董泽熙,李滔,赵玉萍
DOI: 10.13289/j.issn.1009-6264.2023-0227
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