固溶处理对半固态注射成形Mg-Al-Zn合金组织及性能的影响Effect of solution treatment on microstructure and properties of semi-solid injection molding Mg-Al-Zn alloy
胡宇阳,牛立斌,高冲,安玉姣,李玉华,张腾,陈勇
摘要(Abstract):
采用注射成形法制备了AZ91D合金试样,利用扫描电镜(SEM)、X射线衍射(XRD)和拉伸试验等研究固溶处理对试样的显微组织、相组成和力学性能的影响。结果表明:镁合金试样经不同温度固溶处理8 h后,其抗拉强度和伸长率先升高后降低,在390℃固溶处理8 h后达到最大值,分别为164.48 MPa和18.55%。根据显微组织观察与XRD分析结果,合金组织中存在片状分布的Mg_(17)Al_(12)相,随固溶时间的增加,Mg_(17)Al_(12)相溶入基体。经390℃固溶处理8 h后,Mg_(17)Al_(12)相溶入合金基体且晶粒无明显长大,固溶效果较佳。
关键词(KeyWords): 半固态AZ91D镁合金;注射成形;固溶处理;显微组织;力学性能
基金项目(Foundation): 陕西省自然科学基础研究计划资助项目(2018JQ5087)
作者(Author): 胡宇阳,牛立斌,高冲,安玉姣,李玉华,张腾,陈勇
DOI: 10.13289/j.issn.1009-6264.2022-0001
参考文献(References):
- [1] Chourasiya S K,Gautam G.Enhancing the microstructure and tribological performance of spray formed Al alloy by cryorolling[J].Silicon,2019,13 (9):2857-2868.
- [2] Yam Z H,Yu Y D,Qian J H.Fabrication of high-strength Mg-Gd-Nd-Zn-Sn-Zr alloy via extrusion and aging[J].Metals and Materials International,2021,27:4182-4194.
- [3] 林鑫,黄卫东.应用于航空领域的金属高性能增材制造技术[J].中国材料进展,2015,34(9):684-688.LIN Xin,HUANG Wei-dong.High performance metal additive manufacturing technology applied in aviation field[J].Materials China,2015,34(9):684-688.
- [4] Verma R,Nath S K,Jayaganthan R.Effect of microstructural constituents on mechanical behaviour of Mg-Zn-Gd alloy processed through hybrid severe plastic deformation[J].Materials Letters,2021,285:129-131.
- [5] Chen J X,Tan L L,Etim I P,et al.Comparative study of the effect of Nd and Y content on the mechanical and biodegradable properties of Mg-Zn-Zr-(x)Nd/Y (x=0.5,1,2) alloys[J].Materials Technology,2018,33(10):659-671.
- [6] Etim I P,Zhang W,Tan L L,et al.Influence of stamping on the biodegradation behavior of Mg-2Zn-0.5Nd (ZN20) sheet[J].Bioactive Materials,2020,5(1):133-141.
- [7] Ding Y F,Wen C E,Hodgson P,et al.Effects of alloying elements on the corrosion behavior and biocompatibility of biodegradable magnesium alloys:A review[J].Journal of Materials Chemistry B,2014,2(14):1912-1933.
- [8] Hu Y,Yu N,Zhao L Z,et al.Effect of Sm on the microstructure and properties of Mg-9Al alloy[J].International Journal of Cast Metals Research,2017,30(6):317-321.
- [9] 刘笑霖,毛萍莉,王瑞峰,等.预制孪晶对AZ31镁合金板材高速变形行为的影响[J].中国有色金属学报,2021,31(3):649-658.LIU Xiao-lin,MAO Ping-li,WANG Rui-feng.Influence of pre-twinning on high strain rate compressive behavior of AZ31 Mg alloy rolling sheet[J].The Chinese Journal of Nonferrous Metals,2021,31(3):649-658.
- [10] Liu Y Y,Mao P L,Zhang F,et al.Effect of temperature on the anisotropy of AZ31 magnesium alloy rolling sheet under high strain rate deformation[J].Philosophical Magazine,2018,98:1068-1086.
- [11] Liu Y Y,Mao P L,Liu Z,et al.Deformation mechanism of highly textured AZ31 sheet under high strain rates[J].Journal of Alloys and Compounds,2017,48(11):1093-1102.
- [12] Etim I P,Zhang W,Tan L L,et al.Influence of stamping on the biodegradation behavior of Mg-2Zn-0.5Nd(ZN20) sheet[J].Bioactive Materials,2020,5(1):133-141.
- [13] Swetha C V,Ravikumar D,Anand K S,et al.Influence of heat treatment on the machinability and corrosion behavior of AZ91 Mg alloy[J].Journal of Magnesium and Alloys,2018,6(1):52-58.
- [14] Johannes G S,Martin W,Thomas E,et al.Powder metal injection moulding and heat treatment of AZ81 Mg alloy[J].Journal of Materials Processing Technology,2018,247:241-246.
- [15] Obasi G C,Ferri O M,Ebel T,et al.Influence of processing parameters on mechanical properties of Ti-6Al-4V alloy fabricated by MIM[J].Materials Science and Engineering A,2010,527(16/17):3929-3935.
- [16] Feyerabend F,Fischer J,Holtz J,et al.Evaluation of shor-term effects of rare earth and other elements used in magnesium alloys on primary cells and cell lines[J].Acta Biomaterialia,2010,6(5):1834-1842.
- [17] Long T,Zhang X H,Huang Q L,et al.Novel Mg-based alloys by selective laser melting for biomedical applications:microstructure evolution,microhardness and in vitro degradation behaviour[J].Virtual and Physical Prototyping,2017,13(2):71-81.
- [18] 张金玲,刘阳力,周京,等.T6处理对Mg-9Al-Zn-0.16La合金耐蚀性能的影响[J].材料热处理学报,2014,35(5):64-68.ZHANG Jin-ling,LIU Yang-li,ZHOU Jing,et al.Influence of T6 treatment on corrosion resistance of Mg-9Al-Zn-0.16La alloy[J] Transactions of Materials and Heat Treatment,2014,35(5):64-68.
- [19] Xu Y,Hu L X,Sun Y.Dynamic recrystallization kinetics of as-cast AZ91D alloy[J].Transactions of Nonferrous Metals Society of China,2014,24(6):1683-1689.
- [20] Yasi J A,Hector Jr L G,Trinkle D R.First-principles data for solid-solution strengthening of magnesium:From geometry and chemistry to properties[J].Acta Materialia,2010,58(17):5704-5713.
- [21] Zhao J,Gao L L,Gao H,et al.Biodegradable behavior and fatigue life of ZEK100 magnesium alloy in simulated physiological environment[J].International Journal of Fatigue,2015,38(8):904-913.
- [22] 师慧娜,贺俊光,文九巴,等.稀土元素Dy对Mg-2Zn-0.5Zr 生物镁合金组织与性能的影响[J].材料热处理学报,2020,41(1):12-18.SHI Hui-na,HE Jun-guang,WE Jiu-ba,et al.Effect of rare earth element Dy on microstructure and properties of Mg-2Zn-0.5Zr bio-magnesium alloy[J].Transactions of Materials and Heat Treatment,2020,41(1):12-18.
- [23] Xu Y,Hu L X,Sun Y.Dynamic recrystallization kinetics of as-cast AZ91D alloy[J].Transactions of Nonferrous Metals Society of China,2014,24(6):1683-1689.
- [24] Wu B L,Zhao Y H,Du X H,et al.Ductility enhancement of extruded magnesium via yttrium addition[J].Materials Science and Engineering A,2010,527(16/17):4334-4340.
- [25] 刘光明,杨丽峡,黄庆学,等.轧后热处理工艺AZ31镁合金铸轧板组织性能的影响[J].材料热处理学报,2019,40(6):26-32.LIU Guang-ming,YANG Li-xia,HUANG Qing-xue,et al.Effect of post-rolling heat treatment on microstructure and properties of AZ31 magnesium alloy cast-rolled sheet[J].Transactions of Materials and Heat Treatment,2019,40(6):26-32.
- [26] Modigell M,Annalisa P,Marialaura A T.Rheological characterization of semi-solid metals:A review[J].Metals,2018,8(4):245-248.
文章评论(Comment):
|
||||||||||||||||||
|
||||||||||||||||||