等径弯曲通道变形制备超细晶铜的热稳定性Thermal stability of ultra-fine grained copper processed by equal channel angular pressing
王庆娟,张平平,杜忠泽,王静怡
摘要(Abstract):
室温下采用等径弯曲通道变形(Equal Channel Angular Pressing,ECAP)C方式进行了纯铜(99.95%)12道次挤压变形。通过等温和等时退火,研究ECAP变形后铜的退火行为,并研究了等径弯曲通道变形和退火后纯铜的显微硬度和显微结构变化。分析了ECAP应变量、退火时间和退火温度对超细晶铜的再结晶行为、抗软化性能的影响。结果表明:ECAP变形后的超细晶铜在退火过程中,表现出不连续再结晶现象;ECAP降低了铜的热稳定性,变形道次越高再结晶温度越低。退火后稳态晶粒尺寸随变形道次的增加而细化,硬度值随变形道次的增加而增大,回归分析表明,晶粒尺寸与硬度之间的关系符合Hall-Petch公式。
关键词(KeyWords): 等径弯曲通道;超细晶铜;退火;热稳定性
基金项目(Foundation): 国家自然科学基金项目(51104113);; 陕西省教育厅科研计划项目(2010JK650)
作者(Author): 王庆娟,张平平,杜忠泽,王静怡
DOI: 10.13289/j.issn.1009-6264.2012.08.020
参考文献(References):
- [1]Valiev R Z,Islamgaliev R K,Alexandrov I V.Bulk nanostructured materials from severe plastic deformation[J].Progress in Materials Science,2000,45(2):103-189.
- [2]Cao W Q,Godfrey A,Liu W,et al.EBSP study of the annealing behavior of aluminum deformed by equal channel angular processing[J].MaterialsScience and Engineering A,2003,360(1-2):420-425.
- [3]Wang G,Wu S D,Zuo L,et al.Microstructure,texture,grain boundaries in recrystallization regions in pure Cu ECAE samples[J].MaterialsScience and Engineering A,2003,346(1-2):83-90.
- [4]Ferrasse S,Segal V M,Alford F.Texture evolution during equal channel angular extrusion(ECAE):Part II.An effect of post-deformationannealing[J].Materials Sciences and Engineering A,2004,372(1-2):235-244.
- [5]石凤健,王雷刚,王海龙,等.等径角挤压制备CuCrZr合金的抗软化性能[J].材料热处理学报,2009,30(12):94-97.SHI Feng-jian,WANG Lei-gang,WANG Hai-long,et al.Softening resistance of CuCrZr alloy fabricated by equal channel angular pressing[J].Transactions of Materials and Heat Treatment,2009,30(12):94-97.
- [6]Horita Z,Fujinami T,Nemoto M,et al.Improvement of mechnaical properties for Al alloys using equal-channel angular pressing[J].Journal ofMaterials Proeessing Technology,2001,117(3):288-292.
- [7]姜庆伟,刘印,王尧,等.超细晶铜在退火与高温条件下微观结构的不稳定性研究[J].金属学报,2009,45(7):873-879.Jiang Qing-wei,Liu Yin,Wang Yao,et al.Microstructural instability of ultrafine grained copper under annealing and high-temperature deforming[J].Acta Metallurgica Sinica,2009,45(7):873-879.
- [8]Langdon T G.The principles of grain refinement in equal-channel angular pressing[J].Materials Science and Engineering A,2007,462(1-2):3-11.
- [9]Poortmans S,Verlinden B.Thermal stability of CP-aluminium during annealing after ECAE[J].Mater Sci Forum,2004,467-470(10):319-1324.
- [10]Li S Y,Beyerlein I J,Alexander D J,et al.Texture evolution during multi-pass equal channel angular extrusion of copper:Neutron diffractioncharacterization and polycrystal modeling[J].Acta Mater,2005,53(7):2111-2125.
- [11]Yu C Y,Sun P L,Kao P W,et al.Evolution of microstructure during annealing of a severely deformed aluminum[J].Materials Science andEngineering A,2004,366(1-2):310-317.
- [12]Molodova X,Gottstein G,Winning M,et al.Thermal stability of ECAP processed pure copper[J].Materials Science and Engineering A,2007,460-461(1-2):204-213.
- [13]Kyung T P,Dong H S.Annealing behavior of submicrometer grained ferrite in a low carbon steel fabricated by severe plastic deformation[J].Materials Science and Engineering A,2002,334(1-2):79-86.
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