热等静压成型温度对雾化合金粉制备的9Cr-ODS合金钢组织及拉伸性能的影响Effect of hot isostatic pressing temperature on microstructure and tensile properties of 9Cr-ODS alloy steel prepared from atomized alloy powders
谢锐,吕铮,王晴,刘春明
摘要(Abstract):
以雾化合金粉为原料采用热等静压成型制备了9Cr-ODS合金钢。首先,使用扫描电镜(SEM)和能谱仪(EDS)分析了雾化法制备的合金粉的表面形貌和化学成分。利用电子背散射衍射(EBSD)、透射电镜(TEM)、小角X射线散射(SAXS)等研究了9Cr-ODS合金钢的晶粒形貌及平均尺寸、析出相的形貌及分布密度。结果表明:随着热等静压温度的升高,9Cr-ODS合金钢样品的晶粒逐渐长大,抗拉强度逐渐降低;900℃成型制备的9Cr-ODS合金钢的平均晶粒尺寸为0.62μm,其强度高于其他两个成型温度制备的样品。9Cr-ODS合金钢中各类型析出相的分布密度随着成型温度的升高而降低,尺寸则呈现长大的趋势。测试温度越高样品的抗拉强度越低,700℃测量时3个样品的抗拉强度比较接近。测试温度的升高会使样品的伸长率升高,但900℃成型制备的样品的伸长率在700℃测量时出现下降的现象。
关键词(KeyWords): 9Cr-ODS合金钢;微观组织;纳米尺寸析出相;小角X射线散射;力学性能
基金项目(Foundation): 辽宁省教育厅基本科研项目(青年项目)(LJKQZ2021061)
作者(Author): 谢锐,吕铮,王晴,刘春明
DOI: 10.13289/j.issn.1009-6264.2022-0114
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