Fe-Ga-Tb合金轧制薄带的织构与磁致伸缩性能Texture and magnetostrictive properties of Fe-Ga-Tb alloy rolled thin sheet
都宏基,和正华,翟欣雅,郝宏波,朱晓飞,陈立佳
摘要(Abstract):
利用X射线衍射(XRD)、扫描电镜(SEM)与电子背散射衍射(EBSD)技术等研究了Fe-Ga-Tb合金薄带轧制与退火过程中的微结构、织构及磁致伸缩性能演变规律。结果表明:初次再结晶退火板的平均晶粒尺寸为15.5μm,再结晶织构由{111}<112>为峰值的强γ织构与弱Goss织构组成,尺寸为30~150 nm的碳化物与硫化物析出相在初次再结晶基体均匀分布,这种微结构与织构特征可为Goss织构发生异常长大提供有利条件。当退火温度升高至925℃时,再结晶基体晶粒尺寸仅为25μm,少量Goss晶粒异常长大至2.5 mm,退火温度达到1000℃时,Goss晶粒达到厘米尺寸,占据样品表面的98%,仅残留少量非Goss织构的岛状晶粒。高温退火过程中随着二次再结晶对Goss织构的强化,Fe-Ga-Tb合金薄带的磁致伸缩系数大幅提高,1000℃退火后磁致伸缩系数可达284×10~(-6)。
关键词(KeyWords): Fe-Ga合金;轧制薄带;磁致伸缩材料;二次再结晶;织构
基金项目(Foundation): 国家自然科学基金(52004164);; 内蒙古自然科学基金重点项目(2018ZD10);; 辽宁省教育厅项目(LQGD2020013)
作者(Author): 都宏基,和正华,翟欣雅,郝宏波,朱晓飞,陈立佳
DOI: 10.13289/j.issn.1009-6264.2022-0043
参考文献(References):
- [1] Clark A E,Restorff J B,Wun-Fogle M,et al.Magnetostrictive properties of body-centered cubic Fe-Ga and Fe-Ga-Al alloys[J].IEEE Transactions on Magnetics,2000,36(5):3238-3240.
- [2] Clark A E,Wun-Fogle M,Restorff J B,et al.Effect of quenching on the magnetostriction of Fe1-xGax (0.13
- [3] Guruswamy S,Srisukhumbowornchai N,Clark A E,et al.Strong,ductile,and low-field-magnetostrictive alloys based on Fe-Ga[J].Scripta Materialia,2000,43(3):239-244.
- [4] Kellogg R A,Russell A M,Lograsso T A,et al.Tensile properties of magnetostrictive iron-gallium alloys[J].Acta Materialia,2004,52(17):5043-5050.
- [5] Fu Q,Sha Y H,Zhang F,et al.Correlative effect of critical parameters for η recrystallization texture development in rolled Fe81Ga19 sheet:Modeling and experiment[J].Acta Materialia,2019,167:167-180.
- [6] Srisukhumbowornchai N,Guruswamy S.Crystallographic textures in rolled and annealed Fe-Ga and Fe-Al alloys[J].Metallurgical and Materials and Transaction A,2004,35(9):2963-2970.
- [7] 李纪恒,高学绪,朱洁,等.轧制Fe-Ga合金的织构及磁致伸缩[J].金属学报,2008,44(9):1031-1034.LI Ji-heng,GAO Xue-xu,ZHU Jie,et al.Texture and magnetostriction in rolled Fe-Ga alloy[J].Acta Metallurgica Sinica,2008,44(9):1031-1034.
- [8] Na S M,Yoo J H,Flatau A B.Abnormal (110) grain growth and magnetostriction in recrystallized galfenol with dispersed niobium carbide[J].IEEE Transactions on Magnetics,2009,45(10):4132-4135.
- [9] He Z H,Sha Y H,Zhang F,et al.Development of strong η fiber recrystallization texture in rolled Fe81Ga19 thin sheet[J].Metallurgical and Materials Transactions A,2014,45(1):129-133.
- [10] He Z H,Sha Y H,Fu Q,et al.Secondary recrystallization and magnetostriction in binary Fe81Ga19 thin sheets[J].Journal of Applied Physics,2016,119(12):123904.
- [11] He Z H,Sha Y H,Shan N,et al.Secondary recrystallization Goss texture development in a binary Fe81Ga19 sheet induced by inherent grain boundary mobility[J].Metals,2019,9(12):1254.
- [12] 和正华,沙玉辉,张芳,等.轧制Fe81Ga19合金薄带再结晶织构演变[J].东北大学学报(自然科学版),2017,38(12):1707-1711.HE Zheng-hua,SHA Yu-hui,ZHANG Fang,et al.Recrystallization texture evolution in rolled Fe81Ga19 alloy thin sheet[J].Journal of Northeastern University (Natural Science),2017,38(12):1707-1711.
- [13] Na S M,Flatau A B.Single grain growth and large magnetostriction in secondarily recrystallized Fe-Ga thin sheet with sharp Goss (011)[100] orientation[J].Scripta Materialia,2012,66(5):307-310.
- [14] Na S M,Flatau A B.Global Goss grain growth and grain boundary characteristics in magnetostrictive Galfenol sheets[J].Smart Materials and Structures,2013,22(12):125026.
- [15] Na S M,Atwater K M,Flatau A B.Particle pinning force thresholds for promoting abnormal grain growth in magnetostrictive Fe-Ga alloy sheets[J].Scripta Materialia,2015,100(1):1-4.
- [16] Yuan C,Li J H,Zhang W L,et al.Sharp Goss orientation and large magnetostriction in the rolled columnar-grained Fe-Ga alloys[J].Journal of Magnetism and Magnetic Materials,2015,374(1):459-462.
- [17] Yuan C,Li J H,Zhang W L,et al.Secondary recrystallization behavior in the rolled columnar-grained Fe-Ga alloys[J].Journal of Magnetism and Magnetic Materials,2015,391(10):145-150.
- [18] Li J H,Zhang W L,Yuan C,et al.Inhibition force of precipitates for promoting abnormal grain growth in magnetostrictive Fe83Ga17-(B,NbC) alloy sheets[J].Rare Metals,2017,36(11):886-893.
- [19] He Z H,Hao H B,Sha Y H,et al.Sharp secondary recrystallization and large magnetostriction in Fe81Ga19 sheet induced by composite nanometer-sized inhibitors[J].Journal of Magnetism and Magnetic Materials,2019,478:109-115.
- [20] He Z H,Du H J,Sha Y H,et al.Secondary recrystallization behavior in magnetostrictive Fe-Ga thin sheets induced by nano-sized composite precipitates[J].AIP Advances,2021,11(3):035313.
- [21] Jiang L P,Zhang G R,Yang J D,et al.Research on microstructure and magnetostriction of Fe83Ga17Dyx alloys[J].Journal of Rare Earths,2010,28(S1):409-412.
- [22] Jiang L P,Yang J D,Hao H B,et al.Giant enhancement in the magnetostrictive effect of FeGa alloys doped with low levels of terbium[J].Applied Physics Letters,2013,102(22):222409.
- [23] Ma T Y,Hu S S,Bai G H,et al.Structural origin for the local strong anisotropy in melt-spun Fe-Ga-Tb:Tetragonal nanoparticles[J].Applied Physics Letters,2015,106(11):112401.
- [24] He Y K,Jiang C B,Wu W,et al.Giant heterogeneous magnetostriction in Fe-Ga alloys:Effect of trace element doping[J].Acta Materialia,2016,109(9):177-186.
- [25] 蒋成保,贺杨堃.铁镓磁致伸缩合金研究现状与发展趋势[J].金属功能材料,2016,23(6):1-8.JIANG Cheng-bao,HE Yang-kun.Recent development of Fe-Ga magnetostrictive materials[J].Metallic Functional Materials,2016,23(6):1-8.
- [26] Chen Y,Wang J,Yang B,et al.Morphology evolution and enhanced magnetostriction of (Fe0.81Ga0.19)99.9Tb0.1 crystals prepared by liquid metal cooling Bridgman directional solidification[J].Journal of Alloys and Compounds,2021,856:158166.
- [27] Zhao L,Tian X,Yao Z,et al.Enhanced magnetostrictive properties of lightly Pr-doped Fe83Ga17 alloys[J].Journal of Rare Earths,2020,38(3):257-264.
- [28] Zhao X,Tian X,Yao Z,et al.The origin of large magnetostrictive properties of rare earth doped Fe-Ga as-cast alloys[J].Journal of Magnetism and Magnetic Materials,2020,514:167289.
- [29] Zhao X,Tian X,Yao Z,et al.Flexible Pr-doped Fe-Ga composite materials:Preparation,microstructure,and magnetostrictive properties[J].Advanced Engineering Materials,2020,22(12):2000080.
- [30] Meng C Z,Wang H,Wu Y Y,et al.Investigating enhanced mechanical properties in dual-phase Fe-Ga-Tb alloys[J].Scientific Reports,2016,6:34258.
- [31] Meng C Z,Wu Y Y,Jiang C B.Design of high ductility FeGa magnetostrictive alloys:Tb doping and directional solidification[J].Materials and Design,2017,130(17):183-189.
- [32] Lei F,Sha Y,He Z,et al.Rapid secondary recrystallization of the Goss texture in Fe81Ga19 sheets using nanosized NbC particles[J].Materials,2021,14(14):3818.
- [33] Hayakawa Y,Szpunar J A.A new model of Goss texture development during secondary recrystallization of electrical steel[J].Acta Materialia,1997,45(11):4713-4720.
- [34] Hayakawa Y,Muraki M,Szpunar J A.The changes of grain boundary character distribution during the secondary recrystallization of electrical steel[J].Acta Materialia,1998,46(3):1063-1073.
- [35] 王龙妹,谭清元,李娜,等.稀土在无取向电工钢中应用的研究进展[J].中国稀土学报,2014,32(5):513-539.WANG Long-mei,TAN Qing-yuan,LI Na,et al.Research progress on rare earth application technology in non-oriented electrical steels[J].Journal of the Chinese Society of Rare Earths,2014,32(5):513-539.
文章评论(Comment):
|
||||||||||||||||||
|
||||||||||||||||||