两种不同热处理工艺对铸造IN 939合金微观组织及室温拉伸性能的影响Effect of two different heat treatment processes on microstructure and room temperature tensile properties of as-cast IN 939 alloy
陈豪豪,操光辉
摘要(Abstract):
对铸态IN 939(Inconel 939)合金进行了两种不同工艺的热处理:固溶+时效(SA),双固溶+双时效(DSA),并研究了热处理对其显微组织及室温拉伸性能的影响。结果表明:铸态IN 939合金的显微组织由γ、γ′、MC碳化物、η相及γ/γ′共晶组成,其中γ′相有细小和粗化两种形貌。固溶+时效热处理后合金内的η相和粗大γ′相固溶进基体中重新析出细小γ′相,由于细小γ′相充分弥散而得到较为均匀的组织,MC碳化物转变为M_(23)C_6和少许粗化的γ′相;双固溶+双时效热处理使得合金中溶解了更多的析出相,使显微组织更均匀,γ′相充分长大。两种工艺热处理后合金的室温拉伸屈服强度较铸态都有一定提高,固溶+时效热处理试样提升了13.5%,双固溶+双时效试样提升了2.2%,但室温抗拉强度和塑性相比于铸态均有所降低。铸态IN 939合金的断裂机制属于韧性断裂,而SA和DSA试样均属于脆性断裂,DSA试样与SA试样相比,其室温下的塑性和拉伸性能都相对较好。
关键词(KeyWords): IN 939合金;热处理;微观组织;拉伸性能
基金项目(Foundation):
作者(Author): 陈豪豪,操光辉
DOI: 10.13289/j.issn.1009-6264.2022-0172
参考文献(References):
- [1] Wang Y,Shao W Z,Zhen L,et al.Tensile deformation behavior of superalloy 718 at elevated temperatures[J].Journal of Alloys and Compounds,2009,471(1/2):331-335.
- [2] Lalvani H M,Rist M A,Brooks J W.Effect of delta phase on the hot deformation behaviour and microstructural evolution of Inconel 718[J].Advanced Materials Research,2010,89:313-318.
- [3] Pickering E J,Mathur H,Bhowmik A,et al.Grain-boundary precipitation in Allvac 718Plus[J].Acta Materialia,2012,60(6/7):2757-2769.
- [4] Wang M Q,Du J H,Deng Q,et al.Effect of the precipitation of the η-Ni3Al0.5Nb0.5 phase on the microstructure and mechanical properties of ATI 718Plus[J].Journal of Alloys Compounds,2017,701:635-644.
- [5] Gu Y F,Cui C,Ping D,et al.Creep behavior of new kinds of Ni-Co-base superalloys[J].Materials Science and Engineering A,2009,510-511:250-255.
- [6] Gu Y F,Fukuda T,Cui C,et al.Comparison of mechanical properties of TMW alloys,new generation of cast-and-wrought superalloys for disk applications[J].Metallurgical and Materials Transactions A,2009,40(13):3047-3050.
- [7] 沈寅忠.新型的工业及舰船用汽轮机叶片合金IN 939[J].水利电力机械,1994(5):49-52.SHEN Yin-zhong.A new type of alloy IN 939 for industrial and marine steam turbine blade[J].Water Conservancy & Electric Power Machinery,1994(5):49-52.
- [8] 邹敦叙,陈振兰,龚风阶.In 939,U500和543镍基高温合金的低温热腐蚀[J].钢铁研究总院学报,1984,4(4):395-398.ZOU Dun-xu,CHEN Zhen-lan,GONG Feng-jie.Hot corrosion resistance of In 939,U500 and 543 nickel-base superalloys at low temperature[J].Central Iron and Steel Research Institute Technical Bulletin,1984,4(4):395-398.
- [9] Kanagarajah P,Brenne F,Niendorf T,et al.Inconel 939 processed by selective laser melting:Effect of microstructure and temperature on the mechanical properties under static and cyclic loading[J].Materials Science and Engineering A,2013,588:188-195.
- [10] 卢习江.超声辅助激光再制造IN 939高温合金组织调控及性能研究[D].杭州:浙江工业大学,2020.LU Xi-jiang.Microstructure regulation and performance studies on ultrasonic assisted laser remanufacturing of IN 939 superalloy[D].Hangzhou:Zhejiang University of Technology,2020.
- [11] Wimmer T,Mick Y,Weigand B.Experimental investigation into capabilities of laser powder bed fusion to produce wavy macro-channels from IN 939[J].Additive Manufacturing,2020,35:101345.
- [12] 盛家锦.激光熔覆IN 939镍基高温合金裂纹控制及热处理研究[D].杭州:浙江工业大学,2020.SHENG Jia-jin.Study of crack control and heat treatment of laser cladded IN 939 nickel-base superalloy[D].Hangzhou:Zhejiang University of Technology,2020.
- [13] Marchese G,Parizia S,Saboori A,et al.The influence of the process parameters on the densification and microstructure development of laser powder bed fused Inconel 939[J].Metals,2020,10(7):882.
- [14] 盛家锦,王梁,刘蓉,等.热处理对激光熔覆IN 939合金涂层组织与性能的影响[J].表面技术,2020,49(6):202-209.SHENG Jia-jin,WANG Liang,LIU Rong,et al.Effects of heat treatment on microstructure and performance of laser cladded IN 939 alloy[J].Surface Technology,2020,49(6):202-209.
- [15] 夏国俊,姚喆赫,陈健,等.激光增材再制造IN 939修复区显微组织与拉伸性能研究[J].表面技术,2021,50(2):277-286.XIA Guo-jun,YAO Zhe-he,CHEN Jian,et al.Microstructure and tensile properties of IN 939 repaired zone by laser additive remanufacturing[J].Surface Technology,2021,50(2):277-286.
- [16] Li Y,Liang X,Yu Y,et al.Microstructures and mechanical properties evolution of IN 939 alloy during electron beam selective melting process[J].Journal of Alloys and Compounds,2021,883:160934.
- [17] Delargy K M,Shaw S W K,Smith G D W.Effects of heat treatment on mechanical properties of high-chromium nickel-base superalloy IN 939[J].Materials Science and Technology,1986,2(10):1031-1037.
- [18] Whittaker D.2015 欧洲粉末冶金大会的金属增材制造:高温合金,粉末雾化,喷墨和激光金属沉积工艺的进展[J].粉末冶金工业,2016,26(3):1-12.Whittaker D.Metal AM at Euro PM2015:superalloys,powder atomization and advances in inkjet and LMD processes[J].Powder Metallurgy Industry,2016,26(3):1-12.
- [19] Jahangiri M R,Arabi H,Boutorabi S M A.Comparison of microstructural stability of IN 939 superalloy with two different manufacturing routes during long-time aging[J].Transactions of Nonferrous Metals Society of China,2014,24(6):1717-1729.
- [20] Abedini M,Jahangiri M R,Karimi P.Rejuvenation of the microstructure and mechanical properties of a service-exposed IN 939 superalloy by heat treatments[J].Materials at High Temperatures,2019,36(1):19-26.
- [21] Wan W J,Han G W,Deng B.Influence of aging treatment on precipitation behavior of η phase in Ni-Co-Cr alloy[J].Journal of Iron and Steel Research International,2010,17(1):64-69.
- [22] Seifollahi M,Razavi S H,Abbasi S M.The mechanism of η phase precipitation in A286 superalloy during heat treatment[J].Journal of Materials Engineering and Performance,2013,22(10):3063-3069.
- [23] Evans N D,Maziasz P J,Swindeman R W,et al.Microstructure and phase stability in INCONEL alloy 740 during creep[J].Scripta Materialia,2004,51(6):503-507.
- [24] Qin X Z,Guo J T,Yuan C,et al.Long-term thermal exposure responses of the microstructure and properties of a cast Ni-base superalloy[J].Materials Science and Engineering A,2012,543:121-128.
- [25] Hou K,Ou M,Wang M,et al.Precipitation of η phase and its effects on stress rupture properties of K4750 alloy[J].Materials Science and Engineering A,2019,763:138137.
文章评论(Comment):
|
||||||||||||||||||
|
||||||||||||||||||