超声处理方式对电铸铜层组织及性能的影响Effects of ultrasonic treatment method on microstructure and strength of electroformed copper layer
廖强,朱立群,李卫平,刘慧丛
摘要(Abstract):
通过采用不同的超声方式对电铸铜层进行处理,电铸过程中无超声(试样C1)、在电铸过程中超声(C2)、电铸后超声(C3)以及电铸后进行玻璃珠辅助超声(C4),获得了与普通电铸铜层相比结构更致密,抗拉强度更高的电铸铜层。并对不同超声方式下得到的电铸铜层进行微观形貌观察及拉伸性能的测试。结果表明:试样C2由于超声作用使电铸铜层晶粒细化,并抑制了晶粒过分生长,因而与C1相比其抗拉强度提高了23.8%;而电铸后超声对电铸铜微观结构及抗拉性能几乎没有影响;试样C4在玻璃珠的碰撞与摩擦作用下获得了具有纳米晶结构,抗拉强度与C1相比提高了65.2%。
关键词(KeyWords): 电铸铜层;超声处理;纳米结构;抗拉强度
基金项目(Foundation): 国家自然科学基金(50771010)
作者(Author): 廖强,朱立群,李卫平,刘慧丛
DOI: 10.13289/j.issn.1009-6264.2010.11.031
参考文献(References):
- [1]Hart T,Wstson A.The nickel development institute[J].Electroforming,1999(8):388-399.
- [2]朱立群.功能膜层的电沉积理论与技术[M].北京:北京航空航天大学出版社,2005.
- [3]赵阳培,葛世荣,张君伟,等.射流电铸快速成型纳米晶铜的组织与性能[J].机械工程材料,2008,32(1):37-39.ZHAO Yang-pei,GE Shi-rong,ZHANG Jun-wei.Microstructure and properties of nanocrystall ine copper prepared by rapid prototyping oriented by jet electroforming[J].Materials for Mechanical Engineering,2008,32(1):37-39.
- [4]Wong K P,Chan K C,Yue T M.Influence of spike current in different shaped waveforms on the hardness and grain size of nickel electroforms[J].Journal of Materials Processing Technology,2001(117):97-104.
- [5]雷卫宁,朱荻,曲宁松.纳米晶粒精密电铸层力学性能的试验与研究[J].中国机械工程,2004,40(12):126-127.LEI Wei-ning,ZHU Di,QU Ning-song.Research on mechanical properties of nanocrystalline electroforming layer[J].Chinese Journal of Mechanical Engineering,2004,40(12):126-127.
- [6]ZHAO Hai-jun,LIU Lei,WU Ya-ting,et al.Investigation on wear and corrosion behavior of Cu-graphite composites prepared by eledtroforming[J].Composites Science and Technology,2007,67:1210-1217.
- [7]ZHU Jian-hua,LIU Lei,HU Guo-hua,et al.Study on composite electroforming of Cu/Sip composites[J].Materials Letters,2004(58):1634-1637.
- [8]Touyeras F,Hihn J Y,Delalande S,et al.Ultrasound influence on the activation step before electroless coating[J].Ultrasonics Sonochemistry,2003,10(6):363-368.
- [9]Rao V,Kannan E,Prakash R,et al.Observation of two stage dislocation dynamics from nonlinear ultrasonic response during the plastic deformation of AA7175-T7351aluminum alloy[J].Materials Science and Engineering A,2009,512(1-2):92-99.
- [10]Touyeras F,Hihn J Y,Bourgoin X,et al.Effects of ultrasonic irradiation on the properties of coatings obtained by electroless plating and electro plating[J].Ultrasonics Sonochemistry,2005,12(1-2):13-19.
- [11]Rajendran V,Kumaran S M,Jayakumar T,et al.Microstructure and ultrasonic behaviour on thermal heat-treated Al-Li8090alloy[J].Journal of Alloys Compounds,2009,478(1-2):147-153.
- [12]Chang L M,Guo H F,An M Z.Electrodeposition of Ni-Co/Al2O3composite coating by pulse reverse method under ultrasonic condition[J].Materials Letters,2008,62(19):3313-3315.
- [13]Suslick K S,Casadonte D J,Green M LH,et al.Effects of high intensity ultrasound in inorganic solids[J].Ultrasonics,1986,25(1):56-59.
- [14]Liao Q,Zhu L Q,Liu H C,et al.Mechanical properties of electroformed copper layers with gradient microstructure[J].International Journal of Minerals Metallurgy and Materials,2010,17(1):69-74.
- [15]李春喜,王子镐.超声技术在纳米材料制备中的应用[J].化学通报,2001,5(1):268-271.LI Chun-xi,WANG Zi-hao.Applications of ultrasound in preparing nanosized materials[J].Chemistry Online,2001,5(1):268-271.
- [16]吴其胜.无机材料机械力化学[M].北京:化学工业出版社,2008.
- [17]Hall E O.The deformation and ageing of mild steel:III discussion of results[J].Proceedings of the Royal Society of London Series B,1951,64:747-753.
- [18]Petch N J.The cleavage strength of crystals[J].Journal of Iron Steel Institute,1953,74(1):25-26.
文章评论(Comment):
|
||||||||||||||||||
|
||||||||||||||||||