Fe-Al/Al2O3复合阻氚涂层热处理对CLF-1钢组织与性能的影响Effect of heat treatment of Fe-Al/Al2O3 composite tritium resistant coating on microstructure and properties of CLF-1 steel
袁晓明,杨洪广,迟于喆,占勤
摘要(Abstract):
采用显微硬度测试、X射线衍射、组织观察观察及室温、高温拉伸试验研究了采用粉末包埋渗铝-原位氧化工艺制备的Fe-Al/Al_2O_3复合涂层热处理对CLF-1低活化钢基体微观组织及力学性能的影响。结果表明:经涂层热处理后,CLF-1钢晶粒尺寸约为9.91μm,组织为板条马氏体,板条宽度约为600 nm;硬度值为222 HV0.2,室温拉伸强度可达723 MPa,伸长率约为24.05%;在600℃下,拉伸强度可达353 MPa,伸长率约为34.4%;涂层热处理工艺对CLF-1钢基体性能影响不大,涂层处理后基体性能满足微观结构与力学的设计指标。
关键词(KeyWords): Fe-Al/Al2O3复合涂层;涂层热处理;显微组织;力学性能
基金项目(Foundation): 国家磁约束核聚变堆专项(ITER2014GB111003)
作者(Author): 袁晓明,杨洪广,迟于喆,占勤
DOI: 10.13289/j.issn.1009-6264.2018-0022
参考文献(References):
- [1]李兴彦,黄永章,张新,等.防氚渗透涂层的研究进展[J].金属功能材料,2011,18(2):74-78.LI Xing-yan,HUANG Yong-zhang,ZHANG Xin,et al.Review on tritium penetration barrier[J].Metallic Functional Materials,2011,18(2):74-78.
- [2]Liu S,Huang Q,Li C,et al.Influence of non-metal inclusions on mechanical properties of CLAM steel[J].Fusion Engineering and Design,2009,84(7):1214-1218.
- [3]付海英,王平怀,谌继明.CLF-1低活化铁素体/马氏体钢的热处理工艺[J].机械工程材料,2010,34(1):28-37.FU Hai-ying,WANG Ping-huai,CHEN Ji-ming.Heat treatment process for CLF-1 reduced activation ferritic/martensitic steel[J].Materials for Mechanical Engineering,2010,34(1):28-37.
- [4]Ennis P J,Czyrska-Filemonowicz A.Recent advances in creep-resistant steels for power plant applications[J].Sadhana,2003,28(3/4):709-730.
- [5]施正,张弛,夏志新,等.低活化钢中MX相析出行为研究[J].原子能科学技术,2011,45(2):200-205.SHI Zheng,ZHANG Chi,XIA Zhi-xin,et al.Investigation on precipitation behaviors of MX Phase in reduced activation steels[J].Atomic Energy Science and Technology,2011,45(2):200-205.
- [6]Tamura M,Kusuyama H,Shinozuka K,et al.Long-term stability of Ta C particles during tempering of 8%Cr-2%W steel[J].Journal of Nuclear Materials,2007,367:137-141.
- [7]Danon A,Alamo A.Behavior of Eurofer97 reduced activation martensitic steel upon heating and continuous cooling[J].Journal of Nuclear Materials,2002,307:479-483.
- [8]Lindau R,M9slang A,Schirra M.Thermal and mechanical behaviour of the reduced-activation-ferritic-martensitic steel EUROFER[J].Fusion Engineering and Design,2002,61:659-664.
- [9]Nagasaka T,Hishinuma Y,Muroga T,et al.Extraction residue analysis on F82H-BA07 heat and other reduced activation ferritic/martensitic steels[J].Fusion Engineering and Design,2011,86(9/11):2581-2584.
- [10]Sakasegawa H,Tanigawa H,Kano S,et al.Precipitation behavior in F82H during heat treatments of blanket fabrication[J].Fusion Engineering and Design,2011,86(9/11):2541-2544.
- [11]Chen J G,Liu C X,Liu Y C,et al.Effects of tantalum content on the microstructure and mechanical properties of low-carbon RAFM steel[J].Journal of Nuclear Materials,2016,479:295-301.
- [12]Liu W B,Zhang C,Yang Z G,et al.Nanocrystallization of a quenched RAFM steel and microstructure evolution during annealing heat treatment[J].Materials Science and Engineering A,2013,583:61-68.
- [13]Han Kyu Kim,Ji Won Lee,Joonoh Moon,et al.Effects of Ti and Ta addition on microstructure stability and tensile properties of reduced activation ferritic/martensitic steel for nuclear fusion reactors[J].Journal of Nuclear Materials,2018,500:327-336.
- [14]Wu S K,Zhang J C,Yang J X,et al.Investigation on microstructure and properties of narrow-gap laser welding on reduced activation ferritic/martensitic steel CLF-1 with a thickness of 35 mm[J].Journal of Nuclear Materials,2018,503:66-74.
- [15]Xiao X,Liu G Q,Hu B F,et al.Microstructure stability of V and Ta microalloyed 12%Cr reduced activation ferrite/martensite steel during long-term aging at 650℃[J].Journal of Materials Science&Technology,2015,31(3):311-319.
- [16]Klueh R L,Alexander D J,Rieth M.The effect of tantalum on the mechanical properties of a 9Cr-2W-0.25V-0.07Ta-0.1C steel[J].Journal of Nuclear Materials,1999,273(2):146-154.
- [17]Kimura A,Kasada R,Morishita K,et al.High resistance to helium embrittlement in reduced activation martensitic steels[J].Journal of Nuclear Materials,2002,307:521-526.
文章评论(Comment):
|
||||||||||||||||||
|
||||||||||||||||||