高温合金服役及修复过程中组织演化规律Microstructure evolution and rejuvenation heat treatment of service superalloy
董键,周煜,张峥,赵子华
摘要(Abstract):
研究了ЖC6y合金服役过程中的组织演化规律与恢复热处理后组织形貌的变化。结果表明:经过高温长时服役后合金主要强化相的γ'粒子出现显著退化,γ'粒子的粗化存在Ostwald熟化机制与粒子聚集机制,它的粗化行为可以通过γ'相的形貌特征参数进行表征。MC碳化物在服役中发生分解,转变为周围包覆一层γ'膜的M6C型碳化物。在一定条件下,基体中可直接析出M6C型碳化物。晶界处碳化物有更强烈的分解趋势,晶界处形成包覆一层γ'膜的不连续M6C型碳化物。此种恢复热处理工艺优化了γ'粒子的形貌、尺寸、分布,有效恢复合金的组织退化及显微硬度,形成锯齿晶界,使合金持久性能得到恢复,提高了合金使用寿命。
关键词(KeyWords): 高温合金;显微组织;恢复热处理;持久性能
基金项目(Foundation): 中航工业产学研合作创新工程(201110026-01)
作者(Author): 董键,周煜,张峥,赵子华
DOI: 10.13289/j.issn.1009-6264.2013.08.033
参考文献(References):
- [1]崔彤,王磊,杨洪才,等.GH4586A合金长期时效后的组织和性能[J].材料热处理学报,2005,26(1):53-56.CUI Tong,WANG Lei,YANG Hong-cai,et al.Microstructures and mechanical properties of a superalloy GH4568A aged for long-terms[J].Transactions of Materials and Heat Treatment,2005,26(1):53-56.
- [2]崔彤,王继杰,王磊,等.长期时效对一种新型镍基合金的组织及持久性能的影响[J].材料热处理学报,2006,27(5):56-59.CUI Tong,WANG Ji-jie,WANG Lei,et al.Microstructures and high-temperature properties of a new Ni-based superalloy after long-term aging[J].Transactions of Materials and Heat Treatment,2006,27(5):56-59.
- [3]Hosseini S S,Nategh S,Ekrami A A.Change ofγ'precipitate characteristics in damaged superalloy IN738LC during different stages of rejuvenationheat treatment cycles[J].Materials Science and Technology,2012,28(2):213-219.
- [4]Liburdi J,Lowden P,Nagy D,et al.ASME turbo expo 2009 gas turbine technical congress and exposition[C].ASME,2009.
- [5]James A.Review of rejuvenation process for nickel base superalloy[J].Materials Science and Technology,2001,17(5):481-486.
- [6]Zhou Yu,Zhang Zheng,Zhao Zihua,et al.Morphological evolution ofγ'precipitates in a Nickel-based superalloy during various solution treatments[J].Rare Metals,2012,31(3):221-226.
- [7]Xie Y J,Wang M C,Zhang G,et al.Analysis of superalloy turbine blade tip cracking during service[J].Engineering Failure Analysis,2006,13(8):1429-1436.
- [8]Yang Jinxia,Zheng Qi,Sun Xiaofeng,et al.Morphological evolution of MC carbide in K465 superalloy[J].Journal of Materials Science,2006,41(19):6476-6478.
- [9]许婷婷,水丽,杨金侠.K465合金在冷热循环过程中MC碳化物的转变[J].铸造,2009,58(12):1253-1255.XU Ting-ting,SHUI Li,YANG Jin-xia.Transformation of MC type carbide in K465 alloy during heat/cooling cycles[J].Foundry,2009,58(12):1253-1255.
- [10]温莹,田高峰,刘国权,等.镍基粉末高温合金中γ'相的形貌特征的定量表征研究[J].中国体式学与图像分析,2007,12(3):162-166.WEN Ying,TIAN Gao-feng,LIU Guo-quan,et al.Morphology characterization ofγ'phase in a P/M nickel-base superalloy[J].Chinese Journal ofStereology and Image Analysis,2007,12(3):162-166.
- [11]Baldan A.Review progress in Ostwald ripening theories and their applications to nickel-base superalloys part I:Ostwald ripening theories[J].Journalof Materials Science,2002,37(11):2171-2202.
- [12]Mitchell R J,Preuss M.Inter-relationships between composition,γ'morphology hardness,andγ-γ'mismatch in advanced polycrystalline nickel-basesuperalloys during aging at 800℃[J].Metallurgical and Materials Transactions A,2007,38(3):615-627.
- [13]Qin X Z,Guo J T,Yuan C,et al.Decomposition of primary MC carbide and its effects on the fracture behaviors of a cast Ni-base superalloy[J].Materials Science and Engineering A,2008,485(1-2):74-79.
- [14]蔡玉林,郑运荣.高温合金的金相研究[M].北京:国防工业出版社,1986.
- [15]Lvov G,Levit V,Kaufman M.Mechanism of primary MC carbide decomposition in Ni-base superalloys[J].Metallurgical and Materials TransactionsA,2004,35(6):1669-1679.
- [16]Koul A K,Thamburaj R.Serrated grain boundary formation potential of Ni-based superalloys and its implications[J].Metallurgical and MaterialsTransactions A,1985,16(1):17-26.
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