电脉冲连续退火对AZ91镁合金带材组织和性能的影响Influence of electropulsing continuous annealing on microstructure and properties of AZ91 Mg alloy strip
姜雁斌,官磊,莫永达
摘要(Abstract):
研究了电脉冲连续退火对冷轧时效态AZ91镁合金带材显微组织和力学性能的影响。结果表明:电脉冲退火在较低的温度下快速完成了α-Mg基体的再结晶,可显著细化晶粒。当退火温度为210℃时,α-Mg基体发生完全再结晶,其平均晶粒尺寸由冷轧态的约30μm减小为约7μm,带材的抗拉强度由冷轧态的410 MPa减小至334 MPa,断后伸长率由冷轧态的3.7%增大至23%。电脉冲退火后带材的拉伸断裂方式由冷轧态的脆性沿晶断裂转变为韧性穿晶断裂。电脉冲在其热效应和非热效应的共同作用下快速完成再结晶过程以及β-Mg17Al12相阻碍α-Mg基体晶粒长大,是电脉冲退火细化晶粒的主要原因。
关键词(KeyWords): 镁合金;电脉冲退火;再结晶;力学性能
基金项目(Foundation): 国家自然科学基金(51104016);; 稀贵金属综合利用新技术国家重点实验室开放课题资助(SKL-SPM-201204)
作者(Author): 姜雁斌,官磊,莫永达
DOI: 10.13289/j.issn.1009-6264.2015.03.025
参考文献(References):
- [1]Mordike B L,Ebert T.Magnesium properties-applications-potential[J].Materials Science and Engineering A,2001,302(1):37-45.
- [2]金军兵,王智祥,刘雪峰,等.均匀化处理对AZ91镁合金组织和力学性能的影响[J].金属学报,2006,42(10):1014-1018.JIN Jun-bing,WANG Zhi-xiang,LIU Xue-feng,et al.Effect of homogenizing treatment on microstructures and mechanical properties of AZ91magnesium alloy[J].Acta Metallurgica Sinica,2006,42(10):1014-1018.
- [3]夏鹏举,蒋百灵,张菊梅.Mg-Al系镁合金离异共晶β相的研究[J].特种铸造及有色合金,2007,27(5):360-363.XIA Peng-ju,JIANG Bai-ling,ZHANG Ju-mei.Divorced Eutecticβphase in Mg-Al series magnesium alloy[J].Special Casting and Nonferrous Alloy,2007,27(5):360-363.
- [4]张菊梅,蒋百灵,王志虎.固溶及时效处理对AZ80镁合金显微组织的影响[J].金属热处理,2007,32(10):6-10.ZHANG Ju-mei,JIANG Bai-ling,WANG Zhi-hu.Effects of solution and aging on microstructure of AZ80 magnesium alloy[J].Heat Treatment of Metals,2007,32(10):6-10.
- [5]时惠英,陈梓山,张菊梅,等.β-Mg17Al12相析出形态对AZ91镁合金力学性能的影响[J].金属热处理,2010,35(1):42-46.SHI Hui-ying,CHEN Zi-shan,ZHANG Ju-mei,et al.Effects of precipitation morphology ofβ-Mg17Al12phase on mechanical properties of AZ91magnesium alloy[J].Heat Treatment of Metals,2010,35(1):42-46.
- [6]Xu Z H,Tang G Y,Ding F,et al.The effect of multiple pulse treatment on the recrystallization behavior of Mg-3Al-1Zn alloy strip[J].Appl Phys A,2007,88(2):429-433.
- [7]Lin C Y,Bor H Y,Chao C G,et al.Enhanced ductility of the ZA85 magnesium alloy fabricated by equal-channel angular pressing[J].J Alloys Compd,2013,556:26-31.
- [8]Lin D L,Jin L,Zeng X Q,et al.Equal-channel angular pressing of magnesium alloy AZ91 and its effects on microstructure and mechanical properties[J].Mater Sci Eng A,2008,483-484:113-116.
- [9]Yuan Y C,Ma A B,Jiang J H,et al.Mechanical properties and precipitate behavior of Mg-9Al-1Zn alloy processed by equal-channel angular pressing and aging[J].J Alloys Compd,2014,594:182-188.
- [10]Braszczyn’ska-Malik K N.Spherical shape ofγ-Mg17Al12precipitates in AZ91 magnesium alloy processed by equal-channel angular pressing[J].J Alloys Compd,2009,487:263-268.
- [11]Pe'rez-Prado M T,Del Valle J A,Ruano O A.Achieving high strength in commercial Mg cast alloys through large strain rolling[J].Mater Lett,2005,59(26):3299-3303.
- [12]Pe'rez-Prado M T,Del Valle J A,Ruano O A.Grain refinement of Mg-Al-Zn alloys via accumulative roll bonding[J].Scripta Mater,2004,51(11):1093-1097.
- [13]Pe'rez-Prado M T,Del Valle J A,Contreras J M,et al.Microstructural evolution during large strain hot rolling of an AM60 Mg alloy[J].Scripta Mater.2004,50(5):661-665.
- [14]Jiang Y B,Guan L,Tang G Y,et al.Influence of electropulsing treatment on microstructure and mechanical properties of cold-rolled Mg-9Al-1Zn alloy strip[J].Mater Sci Eng A,2011,528:5627-5635.
- [15]Jiang Y B,Tang G Y,Shek C H,et al.Microstructure and texture evolution of the cold-rolled AZ91 magnesium alloy strip under electropulsing treatment[J].J Alloys Compd,2011,509:4308-4313.
- [16]Jiang Y B,Tang G Y,Shek C H,et al.Mechanism of electropulsing induced recrystallization in a cold-rolled Mg-9Al-1Zn alloy[J].J Alloys Compd,2012,536:94-105.
- [17]Jiang Y B,Tang G Y,Shek C H,et al.On the thermodynamics and kinetics of electropulsing induced dissolution ofβ-Mg17Al12phase in an aged Mg-9Al-1Zn alloy[J].Acta Mater,2009,57(16):4797-4808.
- [18]Jiang Y B,Zhang Z H,Guan L,et al.Recrystallization and precipitation ofβ-Mg17Al12phase of the cold-rolled Mg-9Al-1Zn alloy strip during isothermal annealing[J].Material Science Forum,2014,789:336-343.
- [19]Koike J,Kobayashi T,Mukai T,et al.The activity of non-basal slip systems and dynamic recovery at room temperature in fine-grained AZ31B magnesium alloys[J].Acta Mater,2003,51(7):2055-2065.
文章评论(Comment):
|
||||||||||||||||||
|
||||||||||||||||||