650℃/500 MPa应力时效对GH4169合金板材组织及室温拉伸性能的影响Effect of 650 ℃/500 MPa stress aging on microstructure and room temperature tensile properties of GH4169 alloy plate
刘砚飞,丁承尧,贺进,钟燕,田伟,余心宏,王建国
摘要(Abstract):
对固溶+时效处理的GH4169合金板材分别进行了不同时间的应力时效和无应力时效处理,采用光学显微镜(OM)、扫描电镜(SEM)和电子万能试验机等分析了不同应力时效处理后合金的显微组织和室温拉伸性能。结果表明:应力对GH4169合金板材的显微组织无明显影响,经过应力时效和无应力时效处理后γ″相仅发生略微粗化,尺寸由19.02 nm增长至23 nm左右,仍为圆形颗粒状形貌。无应力时效处理对板材的室温拉伸性能基本无影响,这是由于GH4169合金板材的室温变形机制为位错做剪切γ″相运动,板材经无应力时效处理后γ″相的尺寸与经固溶+时效处理的γ″相的尺寸相当,位错剪切γ″所需的应力相当使得室温拉伸性能未变化。随应力时效时间的增加,板材的室温拉伸强度逐渐降低,室温拉伸塑性逐渐增加,这是由于应力时效过程中板材已发生残余塑性变形,位错已切入γ″相,后续室温拉伸过程中,位错再次剪切γ″相所需的应力减小进而导致板材室温拉伸强度降低,拉伸塑性增加。
关键词(KeyWords): GH4169合金板材;应力时效;显微组织;室温拉伸性能
基金项目(Foundation):
作者(Author): 刘砚飞,丁承尧,贺进,钟燕,田伟,余心宏,王建国
DOI: 10.13289/j.issn.1009-6264.2023-0403
参考文献(References):
- [1] 庄景云,杜金辉,邓群,等.变形高温合金GH4169[M].北京:冶金工业出版社,2006.
- [2] Hosseini E,Popovich V A.A review of mechanical properties of additively manufactured Inconel 718[J].Additive Manufacturing,2019,30:100877.
- [3] 张勇,李鑫旭,韦康,等.三联熔炼GH4169合金大规格铸锭与棒材元素偏析行为[J].金属学报,2020,56(8):1123-1132.ZHANG Yong,LI Xin-xu,WEI Kang,et al.Element segregation in GH4169 superalloy large-scale ingot and billet manufactured by triple-Melting[J].Acta Metallurgica Sinica,2020,56(8):1123-1132.
- [4] Qin H L,Bi Z N,Yu H Y,et al.Assessment of the stress-oriented precipitation hardening designed by interior residual stress during ageing in IN718 superalloy[J].Materials Science and Engineering A,2018,728:183-195.
- [5] Yuan H,Liu W C.Effect of the δ phase on the hot deformation behavior of Inconel 718[J].Materials Science and Engineering A,2005,408:281-289.
- [6] Rafiei M,Mirzadeh H,Malekan M.Micro-mechanisms and precipitation kinetics of delta (δ) phase in Inconel 718 superalloy during aging[J].Journal of Alloys and Compounds,2019,795:207-212.
- [7] 郑欣,师玉英,陈玉宝.时效处理对GH4169合金组织和性能的影响[J].金属热处理,2018,43(6):162-165.ZHENG Xin,SHI Yu-ying,CHEN Yu-bao.Effect of aging treatment on microstructure and properties of GH4169 alloy[J].Heat Treatment of Metals,2018,43(6):162-165.
- [8] 牛静,张凡云,杨树林,等.不同时效处理对GH4169合金组织性能的影响[J].航空制造技术,2016(20):45-48.NIU Jing,ZHANG Fan-yun,YANG Shu-lin,et al.Effects of aging treatments on the microstructure and mechanical properties of GH4169 alloy[J].Aeronautical Manufacturing Technology,2016(20):45-48.
- [9] 谢孝昌,李旭东,汤春峰,等.直接时效对GH4169合金应力集中敏感性的影响[J].材料工程,2016,44(2):88-93.XIE Xiao-chang,LI Xu-dong,TANG Chun-feng,et al.Effect of direct aging on stress concentration sensitivity of GH4169 superalloy[J].Journal of Materials Engineering,2016,44(2):88-93.
- [10] 刘杨,王磊,何思斯,等.长期时效对GH4169合金动态拉伸变形行为的影响[J].金属学报,2012,48(1):49-55.LIU Yang,WANG Lei,HE Si-si,et al.Effect of long-term aging on dynamic tensile deformation behavior of GH4169 alloy[J].Acta Metallurgica Sinica,2012,48(1):49-55.
- [11] 齐欢.INCONEL 718(GH4169)高温合金的发展与工艺[J].材料工程,2012(8):92-100.QI Huan.Review of INCONEL 718 alloy:Its history,properties,processing and developing substitutes[J].Journal of Materials Engineering,2012(8):92-100.
- [12] 谷怀鹏,曹腊梅,薛明,等.持久应力对DD10单晶高温合金1100 ℃组织稳定性的影响[J].航空材料学报,2014,34(2):1-5.GU Huai-peng,CAO La-mei,XUE Ming,et al.Effect of stress on microstructural stability of DD10 single crystal superalloy[J].Journal of Aeronautical Materials,2014,34(2):1-5.
- [13] 田宁,田素贵,张宝帅,等.应力时效对DZ125镍基合金组织演化及蠕变抗力的影响[J].中国有色金属学报,2018,28(3):536-546.TIAN Ning,TIAN Su-gui,ZHANG Bao-shuai,et al.Effect of stress aging on microstructure evolution and creep resistance of DZ125 nickel-based superalloy[J].The Chinese Journal of Nonferrous Metals,2018,28(3):536-546.
- [14] 刘晨光,赵云松,张剑,等.应力时效对DD11单晶高温合金TCP相析出行为的影响[J].机械工程材料,2018,42(6):36-41.LIU Chen-guang,ZHAO Yun-song,ZHANG Jian,et al.Effects of stressed aging on TCP phase precipitation behaviour of DD11 single crystal superalloy[J].Materials for Mechanical Engineering,2018,42(6):36-41.
- [15] 迟海,郭霞,秦海龙,等.外应力对GH4169合金时效强化作用的影响[J].分析仪器,2018(2):171-173.CHI Hai,GUO Xia,QIN Hai-long,et al.Effects of external stress on age hardening of GH4169 alloy[J].Analytical Instrumentation,2018(2):171-173.
- [16] 刘剑辉,杨树峰,赵跃文.应力时效对发动机用GH4169镍基合金组织演化及蠕变抗力的影响[J].热加工工艺,2018,47(16):196-199.LIU Jian-hui,YANG Shu-feng,ZHAO Yue-wen.Effects of stress aging on microstructure evolution and creep resistance of GH4169 Ni-base alloy for engine[J].Hot Working Technology,2018,47(16):196-199.
- [17] Kulawik K,Buffat P A,Kruk A,et al.Imaging and characterization of γ′ and γ″ nanoparticles in Inconel 718 by EDX elemental mapping and FIB—SEM tomography[J].Materials Characterization,2015,100:74-80.
- [18] Kuo C M,Yang Y T,Bor H Y,et al.Aging effects on the microstructure and creep behavior of Inconel 718 superalloy[J].Materials Science and Engineering A,2009,A510-511:289.
- [19] 刘永康.GH4169高温合金热锻-冷轧细晶工艺及性能研究[D].秦皇岛:燕山大学,2016.LIU Yong-kang.Study on properties and the hot forging cold rolling fine grained process of GH4169 supperalloy[D].Qinhuangdao:Yanshan University,2016.
- [20] 徐依,张兵,杨艳,等.GH4169合金在冷轧和热处理过程中的组织演变和力学性能[J].稀有金属材料与工程,2023,52(7):2385-2395.XU Yi,ZHANG Bing,YANG Yan,et al.Microstructure evolution and mechanical properties of GH4169 alloy during cold rolling and heat treatment[J].Rare Metal Materials and Engineering,2023,52(7):2385-2395.
- [21] Nembach W,Neite G.Precipitation hardening of superalloys by ordered γ′-particles[J].Progress in Materials Science,1985,29(3):177-319.
- [22] 田伟,钟燕,刘砚飞,等.GH4169合金板材γ″相在长期时效过程中的粗化行为[J].钢铁研究学报,2023,35(8):1037-1043.TIAN Wei,ZHONG Yan,LIU Yan-fei,et al.Coarsening behavior of γ″ phase in GH4169 alloy plate during long-term aging[J].Journal of Iron and Steel Research,2023,35(8):1037-1043.
- [23] 张程.GH4169合金中γ″相的析出与粗化行为研究[D].天津:天津大学,2014.ZHANG Cheng.Research on the precipitation and coarsening behavior of γ″ phase in alloy GH4169[D].Tianjin:Tianjin University,2014.
- [24] 蔡文良.长期时效对GH4169合金组织演化及疲劳裂纹扩展行为的影响[D].沈阳:东北大学,2014.CAI Wen-liang.Effect of long-term aging on microstructure evolvement and fatigue crack growth behavior of GH4169 alloy[D].Shenyang:Northeastern University,2014.
- [25] 安金岚.长期时效对GH4169合金组织演化及低周疲劳行为的影响[D].沈阳:东北大学,2014.AN Jin-lan.Influence of long-term aging on the microstructure evolution behavior and low cycle fatigue of GH4169 alloy[D].Shenyang:Northeastern University,2014.
文章评论(Comment):
|
||||||||||||||||||
|
||||||||||||||||||