退火工艺对电池壳用IF钢的组织、织构及力学性能的影响Effect of annealing process on microstructure, texture and mechanical properties of IF steel for battery shell
张佳奇,宋新莉,贾涓,陈天宇,葛锐
摘要(Abstract):
新能源汽车电池壳用无间隙原子(IF)钢不仅要求有一定的强度,而且需要优异的深冲性能,因此需要优化退火工艺参数,控制组织织构演变以获得对深冲性能有利的{111}面织构与高强度。对厚度为0.30 mm的电池壳用IF钢冷轧板在720~810℃进行再结晶退火3 min,借助光学显微镜、电子背散射衍射(EBSD)技术和万能拉伸试验机等分析了退火IF钢的组织、织构、屈服强度、抗拉强度、塑性应变比r值与应变硬化指数n值,研究不同温度退火对IF钢组织、织构及力学性能等的影响规律与机理。结果表明:冷轧板晶粒沿轧制方向拉长,冷轧板在720~810℃退火3 min后,均得到等轴状铁素体,平均晶粒尺寸由8.43μm增大至11.64μm。冷轧IF钢退火后得到强的{111}面织构,主要由{111}<110>和{111}<112>两类取向晶粒组成,其含量随着退火温度的升高而增加。在780℃退火时由于部分{110}<001>织构吞噬{111}<110>、{111}<112>织构,导致{111}织构发生突降。随退火温度的升高,IF钢的屈服强度与抗拉强度下降;0°、45°与90°方向的塑性应变比r值增大,各向异性Δr值增大。
关键词(KeyWords): 无间隙原子钢;织构;塑性应变比;退火温度
基金项目(Foundation): 国家自然科学基金(51101114)
作者(Author): 张佳奇,宋新莉,贾涓,陈天宇,葛锐
DOI: 10.13289/j.issn.1009-6264.2023-0184
参考文献(References):
- [1] Gojic M,Laoshi K.The susceptibility to the hydro-gen embrittlement of low alloy Cr and CrMo steels[J].ISIJ International,1997,37(4):412-418.
- [2] 康永林.现代汽车板的质量控制与成型性[M].北京:冶金工业出版社,1999:40-44.KANG Yong-lin.Quality Control and Molding of Modern Automotive Steel[M].Beijing:Metallurgical Industry Press,1999:40-44.
- [3] 唐荻,江海涛,米振莉,等.国内冷轧汽车用钢的研发历史、现状及发展趋势[J].鞍钢技术,2010(1):1-6.TANG Di,JIANG Hai-tao,MI Zhen-li,et al.Research and development history of cold rolled steel for automobile and its current applications situation and development trend at home[J].Angang Technology,2010(1):1-6.
- [4] Li W,Zhu J,Xia Y,et al.Testing and modeling the effect of strain-rate on plastic anisotropy for a traditional high strength steel[C]//ASME International Mechanical Engineering Congress & Exposition,Huston,USA,2015.
- [5] 马全仓,毛卫民,杜磊,等.不同织构组分对IF钢板R(θ)值起伏的影响[J].钢铁,2005,40(5):58-61.MA Quan-cang,MAO Wei-min,DU Lei,et al.Influence of texture components on R(θ)-value of IF steel sheet[J].Iron and Steel,2005,40(5):58-61.
- [6] 董登超,刘志桥,张珂,等.不同温度退火后含铌钛IF钢的织构演变及其与塑性应变比和加工硬化指数的关系[J].机械工程材料,2019,43(1):27-30.DONG Deng-chao,LIU Zhi-qiao,ZHANG Ke,et al.Texture evolution and its relationship with plastic strain ratio and work hardening index of IF steel containing Nb and Ti after annealed at different temperatures[J].Materials for Mechanical Engineering,2019,43(1):27-30.
- [7] 张晓燕,张秀飞,郭冬青.不同罩式退火工艺对Ti-IF钢组织和性能的影响[J].包钢科技,2016,42(3):51-54.ZHANG Xiao-yan,ZHANG Xiu-fei,GUO Dong-qing.Effects of different batch annealing processes on microstructure and properties of Ti-IF steel[J].Science & Technology of Baotou Steel 2016,42(3):51-54.
- [8] 陈越,王洪斌,贾宏斌,等.细晶高强IF钢退火时间研究[J].材料热处理学报,2015,36(4):140-144.CHEN Yue,WANG Hong-bin,JIA Hong-bin,et al.Effect of annealing time on microstructure of a fine grain IF steel[J].Transactions of Materials and Heat Treatment,2015,36(4):140-144.
- [9] Ray R K,Jonas J J,Hook R K.Cold rolling and an-nealing textures in low carbon and extra low carbon steels[J].International Materials Reviews,1994,39(4):129-172.
- [10] Zhao H,Rama S C,Barber G C,et al.Experimental study of deep drawability of hot rolled IF steel[J].Journal of Materials Processing Technology,2002,128(1/3):73-79.
- [11] 李媛媛.稀土微合金化高强IF钢热轧过程中P的析出行为的研究[D].包头:内蒙古科技大学,2019.LI Yuan-yuan.Research of P precipitation behavior of rare earth microalloyed high strength IF steel during hot rolling[D].Baotou:Inner Mongolia University of Science & Technology,2019.
- [12] 张士轩.稀土高强IF钢连续退火工艺对组织演变行为的影响[D].包头:内蒙古科技大学,2019.ZHANG Shi-xuan.Effect of continuous annealing process on microstructure evolution behavior of rare earth high strength IF steel[D].Baotou:Inner Mongolia University of Science & Technology,2019.
- [13] 毛卫民,杨平.电工钢的材料学原理[M].北京:高等教育出版社,2013:162-163.MAO Wei-min,YANG Ping.Principles of Material Science of Electrical Steel[M].Beijing:Higher Education Press,2013:162-163.
- [14] 王迪,宋新莉,袁泽喜,等.退火温度对Ti-IF钢性能及织构的影响[J].武汉科技大学学报,2009,32(6):610-614.WANG Di,SONG Xin-li,YUAN Ze-xi,et al.Influence of annealing temperature on properties and texture of Ti-IF steel[J].Journal of Wuhan University of Science and Technology,2009,32(6):610-614.
- [15] Zheng R W,Song R B,Fan W Y.Effects of annealing cooling rates on mechanical properties,microstructure and texture in continuous annealed IF steel[J].Journal of Alloys and Compounds,2017,692:503-514.
- [16] Jahan N,Reihanian M,Gheisari K.Kinetics of recrystallization and microstructure distribution during isothermal annealing of cold rolled nickel[J].Materials Research Express,2019,6(9):96504.
- [17] Surthi K K,Khatirkar R K,Sapate S G.Effect of mode of rolling on recrystallization kinetics and microstructure evolution in interstitial free high strength steel sheet[J].ISIJ International,2013,53(2):356-364.
- [18] Oyarzábal M,Martínez G A,Gutiérrez I.Effect of stored energy and recovery on the overall recrystallization kinetics of a cold rolled low carbon steel[J].Materials Science and Engineering A,2008,485(1/2):200-209.
- [19] Nave M D,Barnett M R.Texture change near grain boundaries and triple points in cold-rolled interstitial-free steel[J].Materials Science and Engineering A,2004,386(1/2):244-253.
- [20] Lindh E,Hutchinson B,Bate P.Texture evolution during recrystallization of ultra-low carbon steel[J].Materials Science Forum,1994,157(6):997-1002.
- [21] 毛卫民,杨平.经济型取向电工钢的定位与发展[J].世界科技研究与发展,2006,28(6):23-26.MAO Wei-min,YANG Ping.Definition and development of economical grade grain-oriented electrical steels[J].World Sci-tech R & D,2006,28(6):23-26.
- [22] 任东.稀土对440 MPa高强IF钢罩式退火组织及P析出行为的影响[D].包头:内蒙古科技大学,2019.REN Dong.Effect of rare earth on batch annealing microstructure and P precipitation behavior of 440 MPa high strength IF steel[D].Baotou:Inner Mongolia University of Science & Technology,2019.
- [23] Primig S,Leitner H,Knabl W,et al.Influence of the heating rate on the recrystallization behavior of molybdenum[J].Materials Science and Engineering A,2012,512:316-324.
- [24] Humphreys F J,Hatherly M.Preface to the First Edition:Recrystallization and Related Annealing Phenomena-3rd ed,Recryst[M].UK:Elsevier Sciencs,2017:411-412.
- [25] 任志恒.冷轧及连续退火工艺对稀土高强IF钢组织和性能的影响[D].包头:内蒙古科技大学,2019.REN Zhi-heng.Effect of cold rolling and continuous annealing on the microstructure and properties of rare earth alloyed high strength IF steel[D].Baotou:Inner Mongolia University of Science & Technology,2019.
- [26] 张力文.退火工艺对细晶高强IF钢微观织构影响的研究[D].鞍山:辽宁科技大学,2012.ZHANG Li-wen.The effect on micro texture of fine grain high strength IF steel after annealing[D].Anshan:University of Science and Technology Liaoning,2012.
- [27] 罗磊.退火工艺对高强IF钢组织织构和性能的影响[D].成都:西华大学,2015.LUO Lei.Effect of annealing temperature on microstructure,textures and properties of high-strength IF steel[D].Chengdu:Xihua University,2015.
- [28] Deeparekha N,Aman G,Murat D,et al.Cold rolling of an interstitial free (IF) steel—Experiments and simulations[J].Mechanics of Materials,2020,148:103420.
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