微孔在一种三代镍基单晶高温合金热处理及持久试验过程中的演化Evolution of micro-pores during heat treatment and stress rupture testing in a third-generation nickel based single crystal superalloy
张雪煜,刘丽荣,赵云松,张剑
摘要(Abstract):
利用扫描电镜、Image Pro Plus软件和Nano Measurer软件研究了微孔在铸态、固溶处理态和完全热处理态的一种三代镍基单晶高温合金中的形貌及尺寸,采用蠕变试验机研究了微孔在合金持久试验过程中的演化。结果表明:铸态合金枝晶间区域γ/γ′共晶边缘存在少量的不规则形状的微孔,微孔的体积分数约为0.09%,平均尺寸约为9.54μm;经固溶处理后合金中会产生圆形和方形的固溶微孔,固溶处理(1325℃)时间由4 h延长到8 h,固溶微孔的体积分数由0.42%增加到0.46%,增加了约10%。时效处理对固溶微孔的体积分数没有明显影响。固溶微孔会在合金持久过程中发展为裂纹源,最终导致持久断裂,方形微孔更易发展成裂纹。
关键词(KeyWords): 镍基单晶高温合金;微孔;固溶处理;持久试验
基金项目(Foundation): 国家自然科学基金(52001297)
作者(Author): 张雪煜,刘丽荣,赵云松,张剑
DOI: 10.13289/j.issn.1009-6264.2023-0499
参考文献(References):
- [1] Roskosz S,Adamiec J.Methodology of quantitative evaluation of porosity,dendrite arm spacing and grain size in directionally solidified blades made of CMSX-6 nickel alloy[J].Materials Characterization,2009,10(60):1120-1126.
- [2] Liu P,Liu X,Huang Y,et al.Effect of heating processing on the formation of micro-pores during solution treatment of high generation nickel-based single crystal superalloy[J].Materials Characterization,2022,189:111994.
- [3] Reed R C,Cox D C,Rae C M F.Damage accumulation during creep deformation of a single crystal superalloy at 1150 ℃[J].Materials Science and Engineering A,2007,448(1/2):88-96.
- [4] Lamm M,Singer R F.The effect of casting conditions on the high-cycle fatigue properties of the single-crystal nickel-base superalloy PWA 1483[J].Metallurgical and Materials Transactions A,2007,38:1177-1183.
- [5] Prasad K,Sarkar R,Gopinath K.Role of shrinkage pores,carbides on cyclic deformation behaviour of conventionally cast nickel base superalloy CM247LC? at 870 ℃[J].Materials Science and Engineering A,2016,654:381-389.
- [6] 谭子昊.一种新型低成本镍基单晶高温合金微观组织与性能研究[D].沈阳:沈阳工业大学,2020.TAN Zi-hao.Study on microstructure and properties of a novel low-cost nickel-based single crystal superalloy[D].Shenyang:Shenyang University of Technology,2020.
- [7] 何禹锋.单晶高温合金中显微孔洞的演变规律及对力学性能影响研究[D].合肥:中国科学技术大学,2022.HE Yu-feng.Evolution of micro-pore and the effect on the mechanical properties of Ni-based single crystal superalloy[D].Hefei:University of Science and Technology of China,2022.
- [8] 黄亚奇.条纹晶和显微孔洞的形成机理及其对单晶高温合金力学性能的影响[D].合肥:中国科学技术大学,2021.HUANG Ya-qi.Formation mechanism of sliver defect and micro-pore and the effect on the mechanical property of Ni-based single crystal superalloy[D].Hefei:University of Science and Technology of China,2021.
- [9] He Y F,Wang S G,Shen J,et al.Evolution of micro-pores in a single crystal nickel-based superalloy during 980 ℃ creep[J].Acta Metallurgica Sinica (English Letters),2022,35(8):1397-1406.
- [10] 石倩颖,李相辉,郑运荣,等.HRS和LMC工艺制备的两种镍基单晶高温合金铸态及固溶微孔的形成[J].金属学报,2012,48(10):1237-1247.SHI Qian-ying,LI Xiang-hui,ZHENG Yun-rong,et al.Formation of solidification and homogenization micropores in two single crystal superalloys produced by HRS and LMC processes[J].Acta Metallurgica Sinica,2012,48(10):1237-1247.
- [11] Link T,Zabler S,Epishin A,et al.Synchrotron tomography of porosity in single-crystal nickel-base superalloys[J].Materials Science and Engineering A,2006,425(1/2):47-54.
- [12] Epishin A,Link T,Svetlov I L,et al.Mechanism of porosity growth during homogenization in single crystal nickel-based superalloys[J].International Journal of Materials Research,2013,104(8):776-782.
- [13] Bokstein B S,Epishin A I,Link T,et al.Model for the porosity growth in single-crystal nickel-base superalloys during homogenization[J].Scripta Materialia,2007,57(9):801-804.
- [14] 韩东宇,姜卫国,肖久寒,等.截面尺寸和固溶制度对单晶高温合金DD33中显微孔洞的影响[J].材料研究学报,2018,32(3):168-176.HAN Dong-yu,JIANG Wei-guo,XIAO Jiu-han,et al.Effect of section size and solution treatment on micropore of a third-generation single crystal superalloy DD33[J].Chinese Journal of Materials Research,2018,32(3):168-176.
- [15] 孙乃荣,赵彦杰.原始孔洞缺陷周围应力分布对镍基单晶高温合金组织演变的影响[J].材料热处理学报,2019,40(2):154-159.SUN Nai-rong,ZHAO Yan-jie.Effect of stress distribution around original pore defects on microstructure evolution of Ni-based single crystal superalloy[J].Transactions of Materials and Heat Treatment,2019,40(2):154-159.
- [16] Tian S G,Jiang C L,Zhang S,et al.Influence and analysis of defects on creep behaviors of a single crystal nickel-based superalloy[J].Materials Science and Engineering A,2014,613:184-192.
- [17] Buck H,Wollgramm P,Parsa A B,et al.A quantitative metallographic assessment of the evolution of porosity during processing and creep in single crystal Ni-base super alloys[J].Materials Science and Engineering Technology,2015,46(6):577-590.
- [18] Li X W,Wang L,Dong J S,et al.Evolution of micro-pores in a single-crystal nickel-based superalloy during solution heat treatment[J].Metallurgical and Materials Transactions A,2017,48:2682-2686.
- [19] Du Y L,Yang Y H,Diao A M,et al.Effect of solution heat treatment on creep properties of a nickel-based single crystal superalloy[J].Journal of Materials Research and Technology,2021,15:4702-4713.
- [20] Anton D L,Giamei A F.Porosity distribution and growth during homogenization in single crystals of a nickel-base superalloy[J].Materials Science and Engineering,1985,76:173-180.
- [21] 曾强,陈旭辉,吴保平,等.固溶时效处理工艺对一种四代镍基单晶高温合金组织及性能的影响[J].稀有金属材料与工程,2022,51(9):3394-3402.ZENG Qiang,CHEN Xu-hui,WU Bao-ping,et al.Effect of solution and aging heat treatment on microstructures and stress rupture properties of fourth generation ni-based single crystal superalloy[J].Rare Metal Materials and Engineering,2022,51(9):3394-3402.
- [22] Whitesell H S,Overfelt R A.Influence of solidification variables on the microstructure,macrosegregation,and porosity of directionally solidified Mar-M247[J].Materials Science and Engineering A,2001,318(1/2):264-276.
- [23] 刘可立,王俊升,郭跃岭,等.镍基单晶高温合金孔洞缺陷数值模拟与控制方法研究进展[J].航空制造技术,2020,63(16):75-85.LIU Ke-li,WANG Jun-sheng,GUO Yue-ling,et al.Modeling and control of porosity defects in nickel-based single crystal superalloys:A Review[J].Aeronautical Manufacturing Technology,2020,63(16):75-85.
- [24] Epishin A,Link T,Svetlov I L,et al.Mechanism of porosity growth during homogenization in single crystal nickel-based superalloys[J].International Journal of Materials Research,2013,104(8):776-782.
- [25] Wang A D,Lv J J,Chen C F,et al.Effects of heat treatment on microstructure and high-temperature tensile properties of nickel-based single-crystal superalloys[J].Materials Research Express,2019,6(12):126527.
- [26] Safari J,Nategh S.On the heat treatment of Rene-80 nickel-base superalloy[J].Journal of Materials Processing Technology,2006,176(1/3):240-250.
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