耿俊昭,刘天成,李立军,潘贇,刘瑞雪

• 1:中国钢研科技集团有限公司
• 2:安泰科技股份有限公司

摘要(Abstract)：

研究了纵向磁场不同温度退火处理对组成为Fe_(73.7)Si_(15.3)Cu_1Nb_3B_7的1k107B纳米晶合金带材的组织结构和软磁性能的影响。结果表明：在纵向加磁电流为150 A、退火温度区间为525～595℃时，合金的矩形比均在0.97以上，晶粒尺寸(D)和矫顽力(H_c)小幅度增加，最大磁导率(μ_m)则与之相反，损耗(P_s)在575℃时取得最小值(99 W/kg@50 kHz, 0.4 T);有效磁导率(μ_e)随着退火温度的升高呈先增加后减小的趋势；通过磁光克尔显微镜观察到纵向磁场退火后合金内部形成规则的平行于磁场方向的条纹畴，且随着退火温度的升高磁畴壁厚度逐渐增大。

关键词(KeyWords)： 铁基纳米晶合金;软磁性能;纵向磁场退火处理;磁畴

Abstract:

Keywords:

基金项目(Foundation): 国家重点研发计划(2021YFB3800505)

作者(Author): 耿俊昭,刘天成,李立军,潘贇,刘瑞雪

DOI: 10.13289/j.issn.1009-6264.2022-0129

参考文献(References)：

• [1]Zhang Y,Wang Z,Li X H,et al.Effect of annealing temperature on structure and high-temperature soft magnetic properties of(Fe0.9Co0.1)72.7Al0.8Si13.5Cu1Nb3B8V1 nanocrystalline alloy[J].Materials Research Bulletin,2021,138(2):111212.
• [2]Kong F,Chang C,Inoue A,et al.Fe-based amorphous soft magnetic alloys with high saturation magnetization and good bending ductility[J].Journal of Alloys and Compounds,2014,615:163-166.
• [3]Li X,Kato H,Yubuta K,et al.Effect of Cu on nanocrystallization and plastic properties of Fe Si BPCu bulk metallic glasses[J].Materials Science and Enineering A,2010,527(10/11):2598-2602.
• [4]Ding J,Xu H,Shi Z,et al.Effect of primary α-Fe on soft magnetic properties of Fe Cu Nb Si B amorphous/nanocrystalline alloy[J].Journal of Non-Crystalline Solids,2021,571:121079.
• [5]Bhattacharya S,Lass E,Poon S,et al.High thermal stability of soft magnetic (Fe,Co)-Mo-B-C-P-Si metallic glasses[J].Journal of Alloys and Compounds,2009,488(1):79-83.
• [6]?ztürk S,I?in K,Gen?türk M,et al.Effect of heat treatment process on the structural and soft magnetic properties of Fe38Co38Mo8B15Cu ribbons[J].Journal of Non-Crystalline Solids,2020,527:119745.
• [7]姚可夫,施凌翔,陈双琴,等.铁基软磁非晶/纳米晶合金研究进展及应用前景[J].物理学报,2018,67(1):8-15.YAO Ke-fu,SHI Ling-xiang,CHEN Shuang-qin,et al.Research progress and application prospect of Fe-based soft magnetic aporphous/nanocrystalline alloys[J].Acta Physica Sinica,2018,67(1):8-15.
• [8]Gutflfleisch O,Willand M A,Bruck E,et al.Magnetic materials and devices for the 21st century:stronger,lighter,and more energy efficient[J].Advanced Materials,2011,23(7):821-842.
• [9]李霏.一种高效率开关电源的设计与研究[D].武汉:武汉理工大学,2016.LI Fei.Decision and research of a high efficiency switching power supply[D].Wuhan:Wuhan University of Technology,2016.
• [10]毛圣华.Fe73.5Cu1Nb3-xVx Si13.5B9纳米晶带材磁性能及其磁放大器研究[D].南昌:南昌大学,2014.MAO Sheng-hua.Research of magnetic properties of Fe73.5Cu1Nb3-xVx Si13.5B9 nanocrystalline strip and its magnetic amplifier[D].Nanchang:Nanchang University,2014.
• [11]邢宇涵.基于磁放大器的耦合谐振式无线电能传输自适应调谐研究[D].天津:天津大学,2018.XING Yu-han.Research of adaptive tuning magnetically coupled resonant wireless power transfer system based on magnetic amplifier[D].Tianjin:Tianjin University,2018.
• [12]周少雄,卢志超,陈金昌.非晶态物理与软磁材料的产业化[J].物理,2002(7):430-436.ZHOU Shao-xiong,LU Zhi-chao,CHEN Jin-chang.Amorphous state physics and the manufacture of soft magnetic materials[J].Physics,2002(7):430-436.
• [13]Makino A.Nanocrystalline soft magnetic Fe-Si-BP-Cu alloys with high B of 1.8-1.9 T contributable to energy saving[J].IEEETransactions on Magnetics,2012,48(4):1331-1335.
• [14]Lu G,Zhang H,Pan L,et al.Tuning of soft magnetic properties in Fe Co Hf O thin films by various sputtering power and pressure[J].Materials Research Innovations,2014,18(S4):619-624.
• [15]Xu Y,Zhu Z,Lei Y,et al.Effect of continuous DC longitudinal magnetic field heat treatment on soft magnetic properties of Fe78Si9B13 amorphous cores[J].IOP Conference Series:Materials Science and Engineering,2017,242:012024.
• [16]Li Y,Jia X,Xu Y,et al.Soft magnetic Fe-Si-B-Cu nanocrystalline alloys with high Cu concentrations[J].Journal of Alloys and Compounds,2017,722:859-863.
• [17]朱乾科.新型Fe基非晶纳米晶软磁合金的成分设计与性能优化[D].太原:太原科技大学,2020.ZHU Qian-ke.Composition design and performance optimization of new types of Fe-based amorphous nanocrystalline soft magnetic alloys[D].Taiyuan:Taiyuan University of Science and Technology,2020.
• [18]Herzer G.Nanocrystalline soft magnetic alloys[J].Handbook of Magnetic Materials,1997,10:415-462.
• [19]潘琳茹.Fe基非晶/纳米晶磁芯热处理工艺及性能研究[D].济南:山东大学,2021.PAN Lin-ru.Research on heat treatment process and performance of Fe-based amorphous/nanocrystalline core[D].Jinan:Shandong University,2021.
• [20]车相辉.纵向磁场退火对Fe Co基纳米晶合金软磁性能影响的研究[D].天津:天津大学,2008.CHE Xiang-hui.Effect of longitudinal magnetic field annealing on the soft magnetic properties of Fe Co-based nanocrystalline alloys[D].Tianjin:Tianjin University,2008.
• [21]张宗阳.Fe80Si8B6Nb5Cu纳米晶磁粉芯制备与软磁性能研究[D].合肥:安徽大学,2019.ZHANG Zong-yang.Study on the preparation and soft magnetic properties of the Fe80Si8B6Nb5Cu nanocrystalline power core[D].Hefei:Anhui University,2019.
• [22]苗宝雯,罗强,沈军,等.纵向磁场热处理对高饱和磁感应强度Fe基非晶-纳米晶软磁性能的影响[J].热加工工艺,2018,47(8):153-157.MIAO Bao-wen,LUO Qiang,SHEN Jun.Effect of longitudinal magnetic heat treatment on soft magnetic properties of Fe-based amorphous-nanocrystalline with high saturation magnetic induction[J].Hot Working Technology,2018,47(8):153-157.
• [23]郭璐,朱乾科,陈哲,等.退火温度对Fe Ga Ge BCu(P)非晶纳米晶合金组织结构和软磁性能的影响[J].功能材料,2022,53(1):1210-1215.GUO Lu,ZHU Qian-ke,CHEN Zhe,et al.Effect of annealing temperatuer on microstructure and soft magnetic properties of Fe Ga Ge BCu(P) amorphous and nanocrystaline alloy[J].Journal of Function Materials,2022,53(1):1210-1215.
• [24]江林.纵向磁场退火对纳米晶合金磁性能的影响[D].天津:天津大学,2009.JIANG Lin.Effect of longitudinal magnetic field annealing on the magnetic properties of nanocrystalline alloys[D].Tianjin:Tianjin University,2009.
• [25]Günes T.Optimum circumstances for heat treatment mechanisms:soft magnetic properties and microstructural evaluation in nanocrystalline Fe Cu Nb Si B alloys[J].Journal of Non-Crystalline Solids,2019,513:97-104.

文章评论(Comment)：