14Cr-ODS钢的显微组织和拉伸性能及热稳定性Microstructure, tensile properties and thermal stability of 14Cr-ODS steel
陈灵芝,李少夫,廖璐,董浩,车洪艳,周张健
摘要(Abstract):
采用机械合金化结合热等静压法制备了14Cr-ODS钢,并在700℃进行最长至5000 h的时效处理。利用扫描电镜(SEM)和透射电镜(TEM)对其显微组织,尤其是时效前后纳米氧化物弥散粒子的特征进行了研究。结果表明:粉末冶金法制备的14Cr-ODS钢具有亚微米细晶组织,晶内弥散分布具有很高数密度的平均尺寸小于10 nm的超细Y_2Ti_2O_7粒子,这种独特的显微组织使得14Cr-ODS钢具有较为优良的拉伸性能;在700℃长期时效后,14Cr-ODS钢的弥散粒子的尺寸、形貌和成分保持稳定,其显微硬度由于应力消除而明显降低,但是拉伸性能没有发生明显变化。
关键词(KeyWords): ODS钢;氧化物粒子;弥散强化;显微组织;时效处理
基金项目(Foundation): 科技部国际热核聚变实验堆计划专项(2015GB121006);; 国家自然科学基金(51801202)
作者(Author): 陈灵芝,李少夫,廖璐,董浩,车洪艳,周张健
DOI: 10.13289/j.issn.1009-6264.2019-0308
参考文献(References):
- [1] Hosemann P,Frazer D,Fratoni M,et al.Materials selection for nuclear applications:challenges and opportunities[J].Scripta Materialia,2018,143:181-187.
- [2] Zinkle S J,Snead L L.Designing radiation resistance in materials for fusion energy[J].Annual Review of Materials Research,2014,44:241-267.
- [3] Klueh R L Elevated temperature ferritic and martensitic steels and their application to future nuclear reactors[J].International Materials Reviews,2005,50(5):287-310.
- [4] Bremaecker A D.Past research and fabrication conducted at SCKCEN on ferritic ODS alloys used as cladding for FBR’s fuel pins[J].Journal of Nuclear Materials,2012,428(1/3):13-30.
- [5] Bischoff J,Motta A.Oxidation behavior of ferritic-martensitic and ODS steels in supercritical water[J].Journal of Nuclear Materials,2012,424(1/3):261-276.
- [6] Hosemann P,Thau H T,Johnson A L,et al.Corrosion of ODS steels in lead-bismuth eutectic[J].Journal of Nuclear Materials,2008,373(1/3):246-253.
- [7] Ricci E,Giuranno D,Canu G,et al.Corrosion behaviour of oxide dispersion strengthened iron-chromium steels in liquid lead at 973 K[J].Materials and Corrosion,2018,69(11):1584-1596.
- [8] Zinkle S J,Boutard J L,Hoelzer D T,et al.Development of next generation tempered and ODS reduced activation ferritic/martensitic steels for fusion energy applications[J].Nuclear Fusion,2017,57(9):092005
- [9] Klueh R L,Shingledecker J P,Swindeman R W,et al.Oxide dispersion-strengthened steels:A comparison of some commercial and experimental alloys[J].Journal of Nuclear Materials,2005,341(2/3):103-114.
- [10] Schneibel J H,Liu C T,Miller M K,et al.Ultrafine-grained nanocluster-strengthened alloys with unusually high creep strength[J].Scripta Materialia,2009,61(8):793-796.
- [11] He P,Klimenkov M,Moeslang A,et al.Correlation of microstructure and low cycle fatigue properties for 13.5Cr1.1W0.3Ti ODS steel[J].Journal of Nuclear Materials,2014,455(1/3):167-173.
- [12] Odette G R.Recent progress in developing and qualifying nanostructured ferritic alloys for advanced fission and fusion applications[J].JOM,2014,66(12):2427-2441.
- [13] Ukai S,Ohtsuka S,Kaito T,et al.10-oxide Dispersion-strengthened/Ferrite-martensite Steels as Core Materials for Generation iv Nuclear Reactors[M].S.l.:Elsevier Ltd,2017:357-414.
- [14] Odette G R.On the status and prospects for nanostructured ferritic alloys for nuclear fission and fusion application with emphasis on the underlying science[J].Scripta Materialia,2018,143:142-148.
- [15] Li S F,Zhou Z J,Wang P H et al.Long-term thermal-aging stability of a 16Cr-oxide dispersion strengthened ferritic steel at 973 K[J].Materials and Design,2016,90:318-329.
- [16] Zilnyk K D,Pradeep K G,Choi,P,et al.Long-term thermal stability of nanoclusters in ODS-Eurofer steel:An atom probe tomography study[J].Journal of Nuclear Materials,2017,492:142-147.
- [17] Li Y F,Abe H,Li F,et al.Grain structural characterization of 9Cr-ODS steel aged at 973 K up to 10,000 h by electron backscatter diffraction[J].Journal of Nuclear.Materials,2014,455:568-572.
- [18] Mao X D,Kim T K,Kim S S,et al.Thermal stability of oxide particles in 12Cr ODS steel[J].Journal of Nuclear Materials,2012,428(1/3):82-89.
- [19] Mohammad A G,Mohsen M.Effect of long-term service exposure on microstructure and mechanical properties of alloy 617[J].Materials and Design,2011,32:2695-2700.
- [20] Larson F R,Miller J.A time temperature relationship for rupture and creep stresses[J].Transactions of the ASME,1952,74:765-775.
文章评论(Comment):
|
||||||||||||||||||
|
||||||||||||||||||