固溶处理冷却方式对近α型高温钛合金显微组织及力学性能的影响Effect of solution treatment cooling methods on microstructure and mechanical properties of near-α type high-temperature titanium alloy
李钢,贾蔚菊,毛新平,彭文雅,强菲,连智伟,涂兴洋,方红琳,赵宇,李奎
摘要(Abstract):
研究了3种固溶冷却方式对近α型高温钛合金(IMI 834)显微组织和力学性能的影响。采用光学显微镜和电子背散射衍射技术对IMI 834钛合金的显微组织及晶体取向特征进行观察和分析,测试了其室温、高温拉伸性能和热稳定性。结果表明:随着固溶后冷却速率的增大,IMI 834合金中的β转变组织逐渐减小,次生α相片层宽度逐渐细化;相较于空冷和油冷,固溶后采用水冷的IMI 834合金中的β转变基体中~63°晶界占比增加,其晶界类型主要以Type 5为主;固溶后水冷将增大显微组织中的位错密度,同时促使IMI 834合金在塑性变形时最易开动的滑移系为锥面滑移■,两种效应同时提升了合金的强度和塑性;IMI 834钛合金经1035℃×2 h/水冷+700℃×2 h/空冷处理,可获得最佳的强塑性匹配,同时具有良好的热稳定性。
关键词(KeyWords): IMI 834钛合金;热处理;冷却方式;组织形貌
基金项目(Foundation):
作者(Author): 李钢,贾蔚菊,毛新平,彭文雅,强菲,连智伟,涂兴洋,方红琳,赵宇,李奎
DOI: 10.13289/j.issn.1009-6264.2024-0496
参考文献(References):
- [1] Williams J C,Starke Jr E A. Progress in structural materials for aerospace systems[J]. Acta Materialia,2003,51(19):5775-5799.
- [2] Parveez B,Kittur M I,Badruddin I A,et al. Scientific advancements in composite materials for aircraft applications:A review[J].Polymers,2022,14(22):5007.
- [3] Cai J M,Huang X,Cao C X,et al. Thermal stability of TG6 titanium alloy and its partial resumption at high temperature[J]. Rare Metal Materials and Engineering,2010,39(11):1893-1898.
- [4] Li G,Sun C. High-temperature failure mechanism and defect sensitivity of TC17 titanium alloy in high cycle fatigue[J]. Journal of Materials Science&Technology,2022,122:128-140.
- [5] Qiang F,Xin S,Tu X,et al. Low-temperature superplastic deformation mechanism of ultra-fine grain Ti-6Al-4V alloy by friction stir processing[J]. Journal of Materials Research and Technology,2024,30:7413-7419.
- [6]武宏让.航空用钛合金[J].钛工业进展,2000(2):30-31.WU Hong-rang. Aerospace titanium alloy[J]. Titanium Industry Progress,2000(2):30-31.
- [7] Sakamoto T,Akiyama H,Tange S,et al. Age hardening of Si-bearing near-α titanium alloy Ti-6Al-2. 75Sn-4Zr-0. 4Mo-0. 45Si(Ti-1100)with two kinds of initial phases[J]. Materials Transactions,2023,64(9):2246-2253.
- [8]蔡建明,郝孟一,李学明,等. BT36高温钛合金的成分特点及组织研究[J].材料工程,2000(2):10-12.CAI Jian-ming,HAO Meng-yi,LI Xue-ming,et al. Study on composition character and microstructure of BT36 high temperature Ti alloy[J]. Journal of Materials Engineering,2000(2):10-12.
- [9]贾蔚菊,曾卫东,刘建荣,等. Ti60高温钛合金氧化行为研究[J].稀有金属材料与工程,2010,39(5):781-786.JIA Wei-ju,ZENG Wei-dong,LIU Jian-rong,et al. Oxidation behavior of near α-titanium alloy Ti60[J]. Rare Metal Materials and Engineering,2010,39(5):781-786.
- [10] Zhang J,Li H,Zhang Y,et al. Microstructure and deformation mechanism of dissimilar titanium alloy Ti600/Ti22Al25Nb weld joints strengthened by isothermal forging[J]. Materials Science and Engineering A,2023,869:144807.
- [11] Wang T,Guo H,Wang Y,et al. The effect of microstructure on tensile properties,deformation mechanisms and fracture models of TG6 high temperature titanium alloy[J]. Materials Science and Engineering A,2011,528(6):2370-2379.
- [12] Yazar K U,Bahl S,Mishra S,et al. Microcrack formation under normal and dwell fatigue of IMI 834[J]. International Journal of Fatigue,2023,175:107724.
- [13] Liu X,Li H,Mei Z,et al. Quantitative characterization of lamellar α precipitation behavior of IMI 834 Ti-alloy in isothermal and non-isothermal heat treatments[J]. Transactions of Nonferrous Metals Society of China,2022,32(1):162-174.
- [14] Singh A,Balasundar I,Gautam J P,et al. Effect of primary α phase fraction on tensile behavior of IMI 834 alloy[J]. Procedia Structural Integrity,2019,14:78-88.
- [15]张雪敏,陈秉刚,李巍,等.固溶温度对Ti150合金棒材组织及力学性能的影响[J].钛工业进展,2019,36(3):31-34.ZHANG Xue-min,CHEN Bing-gang,LI Wei,et al. Effect of solution temperature on microstructures and mechanical properties of Ti150 alloy bar[J]. Titanium Industry Progress,2019,36(3):31-34.
- [16]李四清,王旭,邓雨亭,等.固溶温度对IMI 834钛合金锻件组织和性能的影响[J].航空制造技术,2019,62(19):47-52.LI Si-qing,WANG Xu,DENG Yu-ting,et al. Effect of solid solution temperature on microstructure and properties of IMI 834titanium alloy forging[J]. Aeronautical Manufacturing Technology,2019,62(19):47-52.
- [17]史蒲英,张永强,孙峰,等.固溶时效温度对IMI 834钛合金组织和性能的影响[J].特种铸造及有色合金,2017,37(9):936-939.SHI Pu-ying,ZHANG Yong-qiang,SUN Feng,et al. Influences of solution and aging temperature on microstructure and mechanical properties of the IMI 834 alloy[J]. Special Casting&Nonferrous Alloys,2017,37(9):936-939.
- [18]郭建忠,刘小花,刘娣,等.热处理对IMI 834铸造用高温钛合金组织与性能的影响[J].世界有色金属,2019(18):1-3.GUO Jian-zhong,LIU Xiao-hua,LIU Ti,et al. Effects of heat treatment on microstructures and properties of cast IMI 834 hightemperature titanium alloy[J]. World Nonferrous Metals,2019(18):1-3.
- [19]孙峰. Ti60钛合金相变动力学及组织演变研究[D].西安:西北工业大学,2015.SUN Feng. Investigation of phase transformation kinetics and microstructure evolution in Ti60 alloy[D]. Xi’ an:Northwestern Polytechnical University,2015.
- [20] Sun F,Li J,Wang T,et al. Effect of solution and cooling methods on the high-temperature mechanical behavior of Ti60 alloy[J].Journal of Alloys and Compounds,2024,1009:176985.
- [21] Fu Y,Guo N,Cheng Q,et al. In-situ formation of laser-cladded layer on Ti-6Al-4V titanium alloy in underwater environment[J].Optics and Lasers in Engineering,2020,131:106104.
- [22] Lei L,Zhao Q,Wu C,et al. Variant selection,coarsening behavior of α phase and associated tensile properties in an α+β titanium alloy[J]. Journal of Materials Science&Technology,2022,99:101-113.
- [23] Ke W,Wu M,Zhao R E N,et al. Static globularization and grain morphology evolution of α and β phases during annealing of hotrolled TC21 titanium alloy[J]. Transactions of Nonferrous Metals Society of China,2021,31(9):2664-2676.
- [24] Yazar K U,Bhattacharjee A,Suwas S. Effect of thermomechanical processing on the dwell fatigue behaviour of near alpha titanium alloy IMI 834[J]. JOM,2023,75(1):218-231.
- [25] Wang J,Ji X,Ouyang B,et al. Post-dynamic transformation from α to β phase and reverse transformation in Ti-10V-2Fe-3Al alloy during interrupted hot deformation[J]. Journal of Alloys and Compounds,2024,997:174884.
- [26]罗安,邓运来,官立群.织构对Mg-Gd-Y-Nd-Zr合金疲劳性能的影响[J].材料科学,2021,11(5):554-561.LUO An,DENG Yun-lai,GUAN Li-qun. Effect of texture on fatigue properties of Mg-Gd-Y-Nd-Zr alloy[J]. Material Sciences,2021,11(5):554-561.
- [27] Zhang K,Jiang J. Effects of grain size and temperature on slip and twinning activity in a magnesium-rare earth alloy[J]. Materials Science and Engineering A,2024,891:145974.
- [28]王瑞琴,葛鹏,侯鹏,等.固溶和时效温度对IMI 834钛合金板材组织和性能的影响[J].金属热处理,2021,46(3):96-100.WANG Rui-qin,GE Peng,HOU Peng,et al. Effects of solution treatment and aging temperature on microstructure and mechanical properties of IMI 834 titanium alloy plate[J]. Heat Treatment of Metals,2021,46(3):96-100.
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