热等静压对Ti65合金包套组织性能的影响Effect of hot isostatic pressing on microstructure and properties of Ti65 alloy capsule
鞠长滨,刘明刚,张晓巍,朱丽,高溪蔓,李冠良,孟凡玲,贾秋月
摘要(Abstract):
在钛基复合材料制备过程中,热等静压工艺使Ti65合金包套性能下降,导致钛基复合材料构件服役性能降低。为优化钛基复合材料性能及制备工艺,采用扫描电镜(SEM)、电子背散射衍射(EBSD)和电子万能试验机等分析了热处理工艺与热等静压对Ti65合金的显微组织及室温、高温拉伸性能的影响,分析了不同状态下Ti65合金的室温和高温拉伸断裂机制。结果表明:Ti65合金的锻态和热等静压态的组织相似,均为典型的双态组织,经过热处理后组织中出现了大量的β转变组织;热等静压处理导致Ti65合金的屈服强度下降,热处理会提升其抗拉强度;热等静压处理后Ti65合金的室温和高温拉伸断裂机制均为韧性断裂;在钛基复合材料热等静压成型前Ti65合金包套无需热处理,成型后适当的热处理可提升Ti65合金包套的性能。
关键词(KeyWords): Ti65合金;钛基复合材料;热等静压;组织性能
基金项目(Foundation): 沈阳市重大科技专项“揭榜挂帅”项目(2023-2836)
作者(Author): 鞠长滨,刘明刚,张晓巍,朱丽,高溪蔓,李冠良,孟凡玲,贾秋月
DOI: 10.13289/j.issn.1009-6264.2025-0138
参考文献(References):
- [1] 金旗.SiC纤维增强Ti基复合材料的制备及微观组织结构研究[D].北京:北京科技大学,2021.JIN Qi.Preparation and microstructure of fiber reinforced Ti matrix composites[D].Beijing:University of Science and Technology Beijing,2021.
- [2] 杨亚政,杨嘉陵,方岱宁.高超声速飞行器热防护材料与结构的研究进展[J].应用数学和力学,2008(1):47-56.YANG Ya-zheng,YANG Jia-ling,FANG Dai-ning.Research progress on the thermal protection materials and structures in hypersonic vehicles[J].Applied Mathematics and Mechanics,2008(1):47-56.
- [3] 崔尔杰.近空间飞行器研究发展现状及关键技术问题[J].力学进展,2009,39(6):658-673.CUI Er-jie.Research statutes,development trends and key technical problems of near space flying vehicles[J].Advances in Mechanics,2009,39(6):658-673.
- [4] 黄伟,罗世彬,王振国.临近空间高超声速飞行器关键技术及展望[J].宇航学报,2010,31(5):1259-1265.HUANG Wei,LUO Shi-bin,WANG Zhen-guo.Key techniques and prospect of near-space hypersonic vehicle[J].Journal of Astronautics,2010,31(5):1259-1265.
- [5] 王超,张旭,王玉敏,等.SiCf/Ti65复合材料界面反应与基体相变机理[J].金属学报,2020,56(9):1275-1285.WANG Chao,ZHANG Xu,WANG Yu-min,et al.Mechanisms of interfacial reaction and matrix phase transition in SiCf/Ti65 composites[J].Acta Metallurgica Sinica,2020 56(9):1275-1285.
- [6] 刘范凯.SiCf/Ti2AlNb复合材料增强Ti65合金力学性能研究[D].沈阳:沈阳理工大学,2023.LIU Fan-kai.Study on mechanical properties of Ti65 alloy with SiCf/Ti2AlNb composite[D].Shenyang:Shenyang Ligong University,2023.
- [7] 王清江,刘建荣,杨锐.高温钛合金的现状与前景[J].航空材料学报,2014,34(4):1-26.WANG Qing-jiang,LIU Jian-rong,YANG Rui.High temperature titanium alloys:status and perspective[J].Journal of Aeronautical Materials,2014,34(4):1-26.
- [8] 王玉敏,张国兴,张旭,等.连续SiC纤维增强钛基复合材料研究进展[J].金属学报,2016,52(10):1153-1170.WANG Yu-min,ZHANG Guo-xing,ZHANG Xu,et al.Adcances in SiC fiber reinforced titanium matrix composites[J].Acta Metallurgica Sinica,2016,52(10):1153-1170.
- [9] Weber C H,Du Z Z,Zok F W,et al.High temperature deformation and fracture of a fiber reinforced titanium matrix composite[J].Acta Materialia,1996,44(2):683-695.
- [10] 罗国珍.钛基复合材料的研究与发展[J].稀有金属材料与工程,1997(2):1-7.LUO Guo-zhen.Recent development of titanium metallic matrix composites[J].Rare Metal Materials and Engineering,1997(2):1-7.
- [11] Jia Q Y,Wang Y M,Zhang X,et al.Failure mechanism of continuous fiber-reinforced titanium matrix composite bling under rotational loading[J].Journal of Materials Research and Technology,2022,18:788-799.
- [12] 张旭.SiCf/TC17复合材料界面反应、残余应力及力学性能研究[D].沈阳:中国科学院金属研究所,2012.ZHANG Xu.Study on interface reaction,redidual stress and mechanical properties of SiCf/TC17 composite[D].Shenyang:Institute of Metal Research,Chinese Academy of Sciences,2012.
- [13] 杨青.SiCf/BT25复合材料制备工艺及其拉伸性能研究[D].沈阳:中国科学院金属研究所,2018.YANG Qing.Preparation process and tensile properties of SiCf/BT25 composites[D].Shenyang:Institute of Metal Research,Chinese Academy of Sciences,2018.
- [14] 吴汐玥,陈志勇,程超,等.热处理对Ti65钛合金板材的显微组织、织构及拉伸性能的影响[J].材料研究学报,2019,33(10):785-793.WU Xi-yue,CHEN Zhi-yong,CHENG Chao,et al.Effects of heat treatment on microstructure,texture and tensile properties of Ti65 alloy[J].Chinese Journal of Materials Research,2019,33(10):785-793.
- [15] 谭海兵,臧健,梁弼宁,等.中温热处理对Ti65合金淬火组织及室温拉伸性能的影响[J].材料研究学报,2023,37(12):881-888.TAN Hai-bing,ZANG Jian,LIANG Bi-ning,et al.Effect of medium heat treatmengt on quenched microstructure and tensile properties of Ti65 alloy[J].Chinese Journal of Materials Research,2023,37(12):881-888.
- [16] Liu X Y,Li H W,Zhan M,et al.Quantitative characterization of lamellar α precipitation behavior of IMI834 Ti-alloy in isothermal and non-isothermal heat treatments[J].Transactions of Nonferrous Metals Society of China,2022,32(1):162-174.
- [17] Ke Y,Liu J R,Zhang H J,et al.Precipitates and alloying elements distribution in near α titanium alloy Ti65[J].Journal of Materials Science & Technology,2020,36:91-96.
- [18] Yan Z B,Wang K,Zhou Y,et al.Crystallographic orientation dependent crack nucleation during the compression of a widmannstatten-structure α/β titanium alloy[J].Scripta Materialia,2018,156:110-114.
- [19] Zhou Y,Wang K,Yan Z B,et al.Ex-situ study on mechanical properties and deformation mechanism of three typical microstructures in TA19 titanium alloy[J].Materials Characterization,2020,167:110521.
- [20] Tan C S,Sun Q Y,Lin X,et al.Characterization of deformation in primary α phase and crack initiation and propagation of TC21 alloy using in-situ SEM experiments[J].Materials Science and Engineering A,2018,725:33-42.
- [21] Guo Y,Britton T B,Wilkinson A J,et al.Slip band-grain boundary interactions in commercial-purity Titanium[J].Acta Materialia,2014,76:1-12.
- [22] 何东.双相多晶钛合金微观塑性变形机理与组织演化的定量研究[D].哈尔滨:哈尔滨工业大学,2012.HE Dong.Quantitative research on micro-plastic deformation mechanism and microstructure evolution of polycrystal-dual phase titanium alloy[D].Harbin:Harbin Institute of Technology,2012.
- [23] 唐泽,杨合,孙志超,等.TA15钛合金高温变形微观组织演变分析与数值模拟[J].中国有色金属学报,2008(4):722-727.TANG Ze,YANG He,SUN Zhi-chao,et al.Microstructure evolution and numerical simulation of TA15 titanium alloy during hot compressive deformation[J].The Chinese Journal of Nonferrous Metals,2008(4):722-727.
- [24] Jeoung H K,Semiatin S L,Lee C S.Constitutive analysis of the high-temperature deformation of Ti-6Al-4V with a transformed microstructure[J].Acta Materialia,2003 51:5613-5626.
- [25] 陈慧琴,林好转,郭灵,等.钛合金热变形机制及微观组织演变规律的研究进展[J].材料工程,2007(1):60-64.CHEN Hui-qin,LIN Hao-zhuan,GUO Ling,et al.Progress on hot deformation mechanisms and microstructure evolution of titanium alloys[J].Journal of Materials Engineering,2007(1):60-64.
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