锆合金表面微弧氧化陶瓷膜制备及特性分析Preparation and properties of ceramic coating formed by microarc oxidation on zirconium alloy
薛文斌,金乾,朱庆振,华铭
摘要(Abstract):
采用交流微弧氧化方法在一种锆合金表面制备出保护性陶瓷膜。采用SEM、EDS、XRD分析了陶瓷膜的表面形貌、截面组织、成分和相组成,并测量了微弧氧化前后锆合金的极化曲线,以评估陶瓷膜的电化学腐蚀特性。结果表明,膜层较为致密,并与锆合金结合良好。陶瓷膜由m-ZrO2、t-ZrO2、S iO2相所组成,其中S iO2相主要分布在外层膜里。微弧氧化处理后,锆合金的腐蚀电位上升,腐蚀电流密度下降,它的抗腐蚀能力得到较大提高。
关键词(KeyWords): 锆合金;微弧氧化;陶瓷膜;电化学腐蚀
基金项目(Foundation): 北京市科技新星计划(9558102500);; 教育部留学回国人员科研启动基金;; 北京市留学人员科技活动项目;; 北京市自然科学基金(2102018)
作者(Author): 薛文斌,金乾,朱庆振,华铭
DOI: 10.13289/j.issn.1009-6264.2010.02.009
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