徐建林,郭强,康昭,席国强

• 1:兰州理工大学甘肃省有色金属新材料省部共建国家重点实验室
• 2:兰州理工大学温州泵阀工程研究院

摘要(Abstract)：

以250μm大小的锑粉为原料,在添加相同含量蒸馏水和烷基酚聚氧乙烯醚的条件下,采用湿法机械球磨的方式制备出不同类型的锑基粉末。采用XRD、TEM及FT-IR对制备的锑基粉末的结构、形貌及粒径大小进行了表征分析,研究了球磨时间和球磨转速对锑粉制备的影响。结果表明:当锑粉原料中加入1 ml/g蒸馏水和0.2 ml/g OP-10湿磨时,球磨转速为150 r/min、球磨时间为18 h可制备出分散良好、粒径分布均匀、平均粒径约为10 nm的锑粉。

关键词(KeyWords)： 锑;球磨;纳米粉

Abstract:

Keywords:

基金项目(Foundation): 浙江省自然科学基金(LY12E01002);; 甘肃省有色金属新材料省部共建国家重点实验室开放基金(SKL12012)

作者(Author): 徐建林,郭强,康昭,席国强

DOI: 10.13289/j.issn.1009-6264.2013.06.006

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