时效态Mg-4Y-2Sm-xGd-0.5Zr合金组织与力学性能Microstructure and mechanical properties of aged Mg-4Y-2Sm-xGd-0.5Zr alloy
李志涛,李全安,陈晓亚
摘要(Abstract):
采用光学显微镜、X射线衍射仪、扫描电镜对时效态Mg-4Y-2Sm-xGd-0.5Zr(x=0, 0.5, 1, 1.5 mass%)合金进行了微观组织及物相分析,并采用拉伸实验机在室温至250℃下对其进行了力学性能测试。结果表明:时效态Mg-4Y-2Sm-0.5Zr合金组织主要由α-Mg基体与Mg_(24)Y_5和Mg_(41)Sm_5析出相组成;加入Gd元素后,合金组织中有新相Mg_5Gd形成;随着Gd添加量的增加,Mg_5Gd析出相的数量增加,合金的晶粒得到细化;同一温度拉伸时,合金的抗拉强度在Gd添加量为1.0 mass%时达到峰值,其中室温拉伸时含1.0 mass%Gd的合金的抗拉强度为223.6 MPa;同一成分合金的抗拉强度随着拉伸温度的升高呈逐渐降低的趋势;室温拉伸时合金的伸长率在Gd添加量为0.5 mass%时最高,为15.13%;在150~250℃时高温拉伸时,伸长率在Gd添加量为1.0 mass%时达到峰值,并且比较稳定;加入Gd元素后的合金在150~250℃时具有良好的耐高温性能和热稳定性。
关键词(KeyWords): Mg-4Y-2Sm-xGd-0.5Zr合金;显微组织;力学性能
基金项目(Foundation): 国家自然科学基金(51571084,51171059)
作者(Author): 李志涛,李全安,陈晓亚
DOI: 10.13289/j.issn.1009-6264.2019-0254
参考文献(References):
- [1] Wan Y C,Xiao H C,Jiang S N,et al.Microstructure and mechanical properties of semi-continuous cast Mg-Gd-Y-Zr alloy[J].Materials Science and Engineering A,2014,617:243-247.
- [2] Yang Z,Wang Z H,Duan H B,et al.Microstructure evolution of Mg-6Gd-2Y alloy during solid solution and aging process[J].Materials Science and Engineering A,2015,631:160-165.
- [3] 孟波波,李全安,陈晓亚,等.Mg-9Gd-4Y-1Zn-0.5Zr合金组织和性能[J].材料热处理学报,2017,38(8):35-40.MENG Bo-bo,LI Quan-an,CHEN Xiao-ya,et al.Microstructure and mechanical properties of as-cast Mg-9Gd-4Y-1Zn-0.5Zr alloy[J].Transactions of Materials and Heat Treatment,2017,38(8):35-40.
- [4] Sudholz A D,Birbilis N,Berrles C J,et al.Corrosion behaviour of Mg-alloy AZ91E with atypical alloying additions[J].Journal of Alloys and Compounds,2009,471(1):109-115.
- [5] Aghion E,Bronfm B,Von Buch F,et al.Newly developed magnesium alloys for powertrain applications[J].Journal of Metals,2003,55 (11):30-33.
- [6] 杨晓红,彭丽梅,杨晨辉,等.固溶时效Mg-4Y-3Nd合金析出相与基体的微观结构[J].材料热处理学报,2015,36(4):39-43.YANG Xiao-hong,PENG Li-mei,YANG Chen-hui,et al.Microstructure of Mg-4Y-3Nd alloy after solution and aging treatment[J].Transactions of Materials and Heat Treatment,2015,36(4):39-43.
- [7] Li D Q,Wang Q D,Ding W J.Effects of samarium on microstructure and mechanical properties of Mg-Y-Sm-Zr alloys during thermomechanical treatments[J].Journal of Materials Science,2009,44:3049-3056.
- [8] 陈君,李全安,张清.钇对AZ6l镁合金组织和性能的影响[J].中国稀土学报,2015,33(4):449-454.CHEN Jun,LI Quan-an,ZHANG Qing.Effect of Y on microstructure and properties of AZ61 magnesium alloy[J].Journal of the Chinese Society of Rare Earths,2015,33(4):449-454.
- [9] Jono Y,Yamasaki M,Kawamura Y,et al.Quantitative evaluation of creep strain distribution in an extruded Mg-Zn-Gd alloy of multimodal microstructure[J].Acta Materialia,2015,82:198-211.
- [10] Abrukina N R.Microhardness of phases in the systems Mg-Sm-Y and Mg-Sm-Zn[J].Russian metallurgy:Metally,1987,(2):219-221.
- [11] 刘宁远.Mg-Sm-Gd 系合金时效析出相及相变机理研究[D].上海:上海交通大学,2015:35-88.LIU Ning-yuan.Study on precipitates and phase transformation mechanism of Mg-Sm-Gd system alloys[D].Shanghai:Shanghai Jiao Tong University,2015:35-88.
- [12] 付三玲.Mg-Gd(-Y-Sm-Zr)耐热镁合金组织和性能研究[D].西安:西安理工大学,2016:39-51.FU San-ling.Study on the microstructure and mechanical properties of Mg-Gd(-Y-Sm-Zr) heat resistant magnesium alloys[D].Xi’an:Xi’an University of Technology,2016:39-51.
- [13] 董丽君,夏长清,周岩.稀土元素Gd对Mg-Y-Zr合金组织和高温力学性能的影响[J].铸造,2014,63(11):1149-1152.DONG Li-jun,XIA Chang-qing,ZHOU Yan.Effect of Gd on microstructure and high temperature mechanical properties of Mg-Y-Zr alloys[J].Foundry,2014,63(11):1149-1152.
- [14] Gao L,Chen R S,Han E H.Fracture behavior of high strength Mg-Gd-Y-Zr magnesium alloy[J].Transactions of Nonferrous Metals Society of China,2010,20(7):1217-1221.
- [15] Romano E,Passoni R,Romanowski C.Innovations in the process technology for manufacturing magnesium alloy sheet[J].Magnesium Technology,2015,1:485-490.
- [16] 孟波波,Zn对Mg-9Gd-4Y-0.5Zr合金组织和性能影响[D].洛阳:河南科技大学,2018.MENG Bo-bo.Effect of Zn on microstructure and properties of Mg-9Gd-4Y-0.5Zr alloy[D].Luoyang:Henan University of Science and Technology,2018.
- [17] Nussbaum G,Sainfort P,Regazzoni G,et al.Strengthening mechanisms in the rapidly solidified AZ91 magnesium alloy[J].Scripta Metallurgica,1989,23:1079-1084.
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