镀液成分对等离子电沉积镍镀层的影响Effects of composition in plating solution on Ni coatings prepared by plasma electrodeposition
赵广宏,何业东
摘要(Abstract):
通过对镀镍液成分的改变、SEM观察、称重测量和硬度对比等方法确立了在等离子电沉积作用下,主盐和添加剂的种类及含量对镀层的结构、生长速度、表面硬度的影响规律。结果表明,以NiSO4为主盐的镀液,其含量不可过高,在100 g/L为宜,含量过高会导致表面结构疏松,镀层硬度下降;以NiCl2为主盐的镀液主盐含量可维持较大值在150~200 g/L,镀速和镀层硬度随主盐含量增加而增加;以C6H5O7Na3为添加剂的镀液,随C6H5O7Na3的含量增加镀层可逐渐变得致密,镀速先增加后减少,硬度则逐渐得到提升;以C12H25SO4Na为添加剂的镀液,随C12H25SO4Na含量的增加,镀层的生长速度变化不大,硬度却有逐步缓慢下降的趋势。
关键词(KeyWords): 等离子电沉积;主盐;添加剂;表面结构;镀速;表面硬度
基金项目(Foundation): 国家自然科学基金(51171021)
作者(Author): 赵广宏,何业东
DOI: 10.13289/j.issn.1009-6264.2012.09.021
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