雾化合金粉制备ODS钢的组织与性能Microstructure and mechanical properties of ODS steel produced by atomization alloy powders
谢锐,吕铮,石英男,王晴,刘春明
摘要(Abstract):
首先采用气体雾化方式制备氧化物弥散强化(Oxide dispersion strengthened,ODS)钢的合金粉,然后经短时球磨及热等静压烧结成形方法制备了氧化物弥散强化钢9Cr-ODS。采用电子背散射衍射(EBSD)、透射电镜(TEM),三维原子探针(APT)和万能拉伸实验机等研究了9Cr-ODS钢的组织结构和力学性能。实验结果表明:9Cr-ODS氧化物弥散强化钢的组织为铁素体和马氏体的双相组织,组织中弥散分布着极高密度的纳米析出相。三维原子探针的结果表明9Cr-ODS钢中这些纳米析出相的尺寸小于5 nm、分布密度可以达到3.5×10~(22)/m~3,其中Y_2Ti_2O_7相分布密度达到1.57×10~(20)/m~3,同时在其析出相中还发现一些尺寸稍大的CrTi_2O_5氧化物相。与典型的低活化铁素体/马氏体钢、ODS钢相比较,雾化合金粉制备的9Cr-ODS钢表现出更加优异的力学性能。
关键词(KeyWords): 氧化物弥散强化钢;金属雾化;热等静压;抗拉强度;纳米析出相
基金项目(Foundation): 国家自然科学基金/青年科学基金资助项目(51601031);; 辽宁省自然科学基金面上项目(2017540306)
作者(Author): 谢锐,吕铮,石英男,王晴,刘春明
DOI: 10.13289/j.issn.1009-6264.2018-0166
参考文献(References):
- [1]吕铮.聚变堆第一壁用纳米结构ODS钢的发展与前瞻[J].原子能科学技术,2011,9(45):1105-1111.LZheng.Development and prospect of nano-structured ODS steels for fusion reactor first wall application[J].Atomic Energy Science and Technology,2011,9(45):1105-1111.
- [2]Eiselta C C,Schendzielorza H,Seubert A,et al.ODS-materials for high temperature applications in advanced nuclear systems[J].Nuclear Materials and Energy,2016,9(C):22-28.
- [3]Kim T K,Noh S,Kang S H,et al.Current status and future prospective of advanced radiation resistant oxide dispersion strengthened steel(ARROS)development for nuclear reactor system applications[J].Nuclear Engineering and Technology,2016,48:572-594.
- [4]Hirata A,Fujita T,Wen Y R,et al.Atomic structure of nanoclusters in oxide-dispersion-strengthened steels[J].Nature Materials,2011,10(12):922-926.
- [5]Lu C Y,Lu Z,Xie R,et al.Effect of Y/Ti atomic ratio on microstructure of oxide dispersion strengthened alloys[J].Materials Characterization,2017,134:35-40.
- [6]Xie R,Lu Z,Lu C Y,et al.Microstructures and mechanical properties of 9Cr oxide dispersion strengthened steel produced by spark plasma sintering[J].Fusion Engineering and Design,2017,115:67-73.
- [7]Odette G R,Alinger M J,Wirth B D.Recent developments in irradiation-resistant steels[J].Annual Review of Materials Research,2008,38:471-503.
- [8]Robertson C,Panigrahi B K,Balaji S,et al.Particle stability in model ODS steel irradiated up to 100 dpa at 600℃:TEM and nano-indentation investigation[J].Journal of Nuclear Materials,2012,426(1/3):240-246.
- [9]Kim J H,Byun T S,Hoelzer D T,et al.Temperature dependence of strengthening mechanisms in the nanostructured ferritic alloy14YWT:Part II-Mechanistic models and predictions[J].Materials Science and Engineering A,2013,559:111-118.
- [10]Sawazaki Y,Ukai S,Sugino Y,et al.Development of 15Cr ODS ferritic steels for over 1273 K service[J].Journal of Nuclear Materials,2013,442(1/3):S169-S172.
- [11]Iwata N Y,Kasada R,Kimura A,Okuda T.Effects of milling parameters on the microstructure and Charpy impact properties of MA/ODS ferritic steels[J].Fusion Engineering and Design,2018,126:24-28.
- [12]Li Z,Lu Z,Xie R,et al.Effect of spark plasma sintering temperature on microstructure and mechanical properties of 14Cr-ODS ferritic steels[J].Materials Science and Engineering A,2016,660:52-60.
- [13]Shibata H,Ukai S,Oono N H,et al.Development of accident tolerant Fe Cr Al-ODS steels utilizing Ce-oxide particles dispersion[J].Journal of Nuclear Materials,2018,502:228-235.
- [14]Iwata N Y,Kimura A,Fujiwara M,et al.Effect of milling on morphologies and microstructural properties of powder particles for high-Cr oxide dispersion strengthened ferritic steels[J].Journal of Nuclear Materials,2007,367-370:191-195.
- [15]Laurent-Brocq M,Legendre F,Mathon M H,et al.Influence of ball-milling and annealing conditions on nanocluster characteristics in oxide dispersion strengthened steels[J].Acta Materialia,2012,60(20):7150-7159.
- [16]Jones H.A perspective on the development of rapid solidification and non-equilibrium processing and its future[J].Materials Science and Engineering A,2001,304-306:11-19.
- [17]Magee C L.The nucleation of martensite[J].Phase Transformation,1970:115-156.
- [18]Ukai S,Harada M,Okada H,et al.Alloying design of oxide dispersion strengthened ferritic steel for long life FBRs core materials[J].Journal of Nuclear Materials,1993,204:65-73.
- [19]Lu C Y,Lu Z,Xie R et al.Microstructure of a 14Cr-ODS ferritic steel before and after helium ion implantation[J].Journal of Nuclear Materials,2014,455(1/3):366-370.
- [20]Bhattacharyya D,Dickerson P,Odette G R,et al.On the structure and chemistry of complex oxide nanofeatures in nanostructured ferritic alloy U14YWT[J].Philosophical Magazine,2012,92(16):2089-2107.
- [21]Oksiuta Z,Olier P,Carlan Y de,Baluc N.Development and characterisation of a new ODS ferritic steel for fusion reactor application[J].Journal of Nuclear Materials,2009,393(1):114-119.
- [22]Praud M,Mompiou F,Malaplate J,et al.Study of the deformation mechanisms in a Fe-14%Cr ODS alloy[J].Journal of Nuclear Materials,2012,428(1/3):90-97.
- [23]Steckmeyer A,Praud M,Fournier B,et al.Tensile properties and deformation mechanisms of a 14Cr ODS ferritic steel[J].Journal of Nuclear Materials,2010,405(2):95-100.
- [24]Ramar A,Sptig P,Schublin R.Analysis of high temperature deformation mechanism in ODS EUROFER97 alloy[J].Journal of Nuclear Materials,2008,382(2/3):210-216.
- [25]王磊.材料的力学性能[M].沈阳:东北大学出版社,2009:74-79.
- [26]Lindau R,M9slang A,Schirra M,et al.Mechanical and microstructural properties of a hipped RAFM ODS-steel[J].Journal of Nuclear Materials,2002,307-311:769-772.
- [27]Klueh R L,Shingledecker J P,Swindeman R W,et al.Oxide dispersion strengthened steels:A comparison of some commercial and experimental alloys[J].Journal of Nuclear Materials,2005,341(2/3):103-114.
- [28]Lindau R,M9slang A,Rieth M,et al.Present development status of EUROFER and ODS-EUROFER for application in blanket concepts[J].Fusion Engineering and Design,2005,75(11):989-996.
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