时效工艺对反应堆压力容器钢中富Cu团簇析出的影响Effect of aging treatments on precipitation of Cu-rich clusters in simulated reactor pressure vessel steels
王伟,王玲,周细应,李忠文,刘继华,刘艳红
摘要(Abstract):
反应堆压力容器(RPV)模拟钢样品经880℃加热0.5 h水淬,再经过660℃加热10 h调质处理,随后在340~400℃进行不同时间的时效处理,测量了维氏硬度,并采用原子探针层析技术(atom probe tomography,APT)研究了富Cu团簇的析出过程。APT分析结果表明,RPV模拟钢淬火后经400℃时效100 h的样品中析出了富Cu团簇,团簇的数量密度为1.69×1023m-3;模拟钢在调质处理后,经400℃时效1000 h时效处理后才析出了富Cu团簇,团簇的数量密度为6×1022m-3。研究结果表明,同调质处理后时效相比,模拟钢淬火后直接时效可以更好地模拟RPV钢经中子辐照后富Cu团簇的析出。
关键词(KeyWords): 反应堆压力容器模拟钢;原子探针层析技术;时效处理;富Cu团簇
基金项目(Foundation): 国家自然科学基金(51271111)
作者(Author): 王伟,王玲,周细应,李忠文,刘继华,刘艳红
DOI: 10.13289/j.issn.1009-6264.2013.12.020
参考文献(References):
- [1]李云良,张汉谦,胡莹,等.核电压力容器用厚钢板SA533B的组织及力学性能[J].材料热处理学报,2012,33(8):84-88.LI Yun-liang,ZHANG Han-qian,HU Ying,et al.Microstructure and mechanical properties of nuclear pressure vessel steel SA533B heavy plate[J].Transactions of Materials and Heat Treatment,2012,33(8):84-88.
- [2]王月香,周平,麻衡,等.热处理工艺对低温压力容器用钢组织性能的影响[J].材料热处理学报,2012,33(s1):77-80.WANG Yue-xiang,ZHOU Ping,MA Heng,et al.Influence of heat treatment process on microstructure and properties of the low-temperature pressure vessel steel[J].Transactions of Materials and Heat Treatment,2012,33(s1):77-80.
- [3]李昌义,刘正东,林肇杰,等.反应堆压力容器用钢的淬透性问题[J].材料热处理学报,2011,32(6):68-72.LI Chang-yi,LIU Zheng-dong,LIN Zhao-jie,et al.Hardenability of nuclear reactor pressure vessel steels[J].Transactions of Materials and Heat Treatment,2011,32(6):68-72.
- [4]Mayoral M H,Briceno D G.Transmission electron microscopy study on neutron irradiated pure and RPV model alloys[J].Journal of Nuclear Materials,2010,399(2-3):146-153.
- [5]Meslin E,Radiguet B,Pareige P,et al.Kinetic of solute clustering in neutron irradiated ferritic model alloys and a french pressure vessel steel investigated by atom probe tomography[J].Journal of Nuclear Materials,2010,399(2-3):137-145.
- [6]Grafutin V,Ilyukhnia O,Krsjak V,et al.Study of PRIMAVERA steel samples by a positron annihilation spectroscopy technique[J].Journal of Nuclear Materials,2010,406(2):257-262.
- [7]Bergner F,Lambrecht M,Ulbricht A,et al.Comparative small-angle neutron scattering study of neutron-irradiated Fe,Fe-based alloys and a pressure vessel steel[J].Journal of Nuclear Materials,2010,399(2-3):129-136.
- [8]Toyama T,Nagai Y,Tang Z,et al.Nanostructural evolution in surveillance test specimens of a commercial nuclear reactor pressure vessel studied by three-dimensional atom probe and positron annihilation[J].Acta Materialia,2007,55(20):6852-6860.
- [9]Kamada Y,Park D G,Takahashi S,et al.The effect of bcc-Cu Precipitation on magnetism in thermally aged Fe-1wt.%Cu model alloys[J].IEEE Transaction on Magnetics,2007,43(6):2701-2703.
- [10]Park D G,Ryu K S,Kobayashi S,et al.Change in magnetic properties of a cold rolled and thermally aged Fe-Cu alloy[J].Journal of Applied Physics,2010,107:09A330-1-09A330-3.
- [11]Minov B,Vandenbossche L P,Konstantinovic M J,et al.Magnetic after-effect study of the Cu-precipitation in thermally aged Fe-1%Cu alloys[J].IEEE Transaction on Magnetics,2010,46(2):521-524.
- [12]Hyde J M,Sha G,Marquis E A,et al.A comparison of the structure of solute clusters formed during thermal ageing and irradiation[J].Ultramicroscopy,2011,111(6):664-671.
- [13]Styman P D,Hyde J M,Wilford K,et al.Precipitation in long term thermally aged high copper,high nickel model RPV steel welds[J].Progress in Nuclear Energy,2012,57:86-92.
- [14]Miller M K,Russell K F,Odette G R.IVNC and IFES 2006-Technical Digest-l9th International Vacuum Nanoelectronics Conference and 50th International Field Emission Symposium[C]∥2006,Guilin,China.
- [15]Miller M K.Atom Probe Tomography:Analysis at the Atomic Level[M].New York:Kluwer academic/plenum publishers,2000.
- [16]刘庆东,褚于良,王泽民,等.Nb-V微合金钢中渗碳体周围元素分布的三维原子探针表征[J].金属学报,2008,44(11):1281-1285.LIU Qing-dong,CHU Yu-liang,WANG Ze-min,et al.3D atom probe characterization of alloying elements partitioning in cementite of Nb-V microalloying steel[J].Acta Metallurgica Sinica,2008,44(11):1281-1285.
- [17]Auger P,Pareige P,Akamatsu M,et al.Microstructural characterization of atom cluster in irradiated pressure vessel steels and model alloys[J].Journal of Nuclear Materials,1994,211:194-201.
- [18]Kimura Y,Takaki S.Phase transformation mechanism of Fe-Cu alloys[J].ISIJ International,1997,37(3):290-295.
- [19]王伟,朱娟娟,林民东,等.核反应堆压力容器模拟钢中富Cu纳米团簇析出早期阶段的研究[J].北京科技大学学报,2010,32(1):39-43.WANG Wei,ZHU Juan-juan,LIN Min-dong,et al.Study on the early-stage of copper-rich nano-clusters precipitation in model nuclear reactor pressure vessel steel[J].Journal of University of Science and Technology Beijing,2010,32(1):39-43.
- [20]徐刚,蔡琳玲,冯柳,等.富Cu团簇的析出对RPV模拟钢韧-脆转变温度的影响[J].金属学报,2012,48(6):753-758.XU Gang,CAI Lin-ling,FENG Liu,et al.Effect of the precipitation of Cu-rich clusters on the DBTT of RPV simulated steel[J].Acta Metallurgica Sinica,2012,48(6):753-758.
文章评论(Comment):
|
||||||||||||||||||
|
||||||||||||||||||