回火处理对15Cr12MoVN钢显微组织和冲击吸收能量的影响Effects of tempering on microstructure and impact absorbed energy of 15Cr12MoVN martensitic steel
赵卓
摘要(Abstract):
采用光学显微镜(OM)和扫描电镜(SEM)研究了15Cr12MoVN马氏体钢在回火处理过程中的组织转变规律及回火处理对冲击吸收功的影响。结果表明:回火处理后15Cr12MoVN马氏体钢中的主要析出相是M23C6碳化物,分布在原奥氏体晶界和板条界上。当回火温度由700℃增加到800℃时,碳化物析出数量增加,颗粒尺寸增大,分布均匀性得到显著改善;原奥氏体晶界上的碳化物形貌由细小、离散的颗粒状向粗大、连续的颗粒状转变,而板条界上的碳化物形貌均保持细小的颗粒状或短棒状。随回火温度增加,15Cr12MoVN马氏体钢韧脆转变温度(DBTT)降低,在750~800℃范围内达到最低值,冲击断口结晶状区由完全解理断裂向塑性撕裂和局部韧窝转变。
关键词(KeyWords): 15Cr12MoVN钢;回火处理;碳化物;冲击吸收能量
基金项目(Foundation):
作者(Author): 赵卓
DOI: 10.13289/j.issn.1009-6264.2017-0363
参考文献(References):
- [1]Klueh R L,Alexander D J,Kenik E A.Development of low-Cr,Cr-W steels for fusion[J].Journal of Nuclear Materials,1995,227(1):11-23.
- [2]Kohyama A,Hishinuma A,Gelles D S,et al.Low-activation ferritic and martensitic steels for fusion application[J].Journal of Nuclear Materials,1996,233/237:138-147.
- [3]Rosenwasser S N,Miller P,Dalessandro J A,et al.The application of martensitic stainless steels in long lifetime fusion first wall/blankets[J].Journal of Nuclear Materials,1979,85/86:177-182.
- [4]Hamada K,Gold R E,Jacko R J.Effects of precipitate shape on high temperature strength of modified 9Cr-1Mo steels[J].ISIJ International,1995,35(1):335-342.
- [5]Yokoyama T,Masuyama F.Application of boiler materials for ultra-high temperature and high pressure power plants[J].The Thermal and Nuclear Power,1994,45(11):43-54.
- [6]Lucon E,Chaouadi R,Decreton M.Mechanical properties of the European reference RAFM steel(Eurofer 97)before and after irradiation at 300℃[J].Journal of Nuclear Materials,2004,329/333:1078-1082.
- [7]Chatterjee A,Moitra A,Bhaduri A K,et al.Effect of heat treatment on ductile-brittle transition behavior of 9Cr-1Mo steel[J].Procedia Engineering,2014,86(1):287-294.
- [8]Cardoso P H S,Kwietniewski C,Porto J P,et al.The influence of delta ferrite in the AISI 416 stainless steel hot workability[J].Materials Science and Engineering A,2003,351(1/2):1-8.
- [9]Hippsley C A,Haworth N P.Hydrogen and temper embrittlement in 9Cr-1Mo steel[J].Materials Science and Technology,1988,4(9):791-802.
- [10]Gelles D S.Microstructural development in reduced activation ferritic alloys irradiated to 200 dpa at 420℃[J].Journal of Nuclear Materials,1994,212/215(1):714-719.
- [11]Sathyanarayanan S,Moitra A,Samuel K G,et al.Evaluation of dynamic fracture toughness based reference temperature of modified 9Cr-1Mo steel in phosphorus embrittled and cold-worked condition[J].Materials Science and Engineering A,2008,488(1):519-528.
- [12]Allen T R,Stoller R E,Yamanaka S.Comprehensive Nuclear Materials,Volume 4:Radiation Effects in Structural Materials[M].Amsterdam,the Netherlands:Elsevier Ltd,2012:97-120.
- [13]Yan W,Wang W,Shan Y,et al.9-12Cr Heat-Resistant Steels[M].Switzerland:Springer International Publishing,2015:47-50.
- [14]Prabhugaukar V G.Role of carbon in embrittlement phenomena of tempered martensitic 12Cr-0.15%C steel[J].Metals Science,1980,32(12):241-252.
- [15]Schinkel J W,Rademakers P L F,Drenth B R,etal.Heat treatment,aging effects and microstructure of 12%Cr steels[J].Journal of Heat Treating,1984,3(3):237-248.
- [16]Miao B H,Northwood D O.Microstructure of tempered AISI 403 stainless steel[J].Materials Science and Engineering A,1993,171(1/2):21-33.
- [17]郝宪朝,陈波,马颖澈,等.热轧态Inconel690合金中碳化物的溶解和析出[J].材料研究学报,2009,23(6):668-672.HAO Xian-chao,CHEN Bo,MA Ying-che,et al.Dissolution and precipitation of carbide in hot-rolled Inconel alloy 690[J].Chinese Journal of Materials Research,2009,23(6):668-672.
- [18]Kalwa G,Schnabel E.Warmebe handlung und eigenschaften dick wandiger bauteil eauswarm festenrohren stahlen[J].VGB Kraftwerkstech,1978,58(8):604-613.
- [19]Santella M L.Influence of chemical compositions on lower ferrite-austenite transformation temperatures in 9%Cr steels[J].Journal of Pressure Vessel Technology,2010,134(2):1-5.
- [20]Abe F,Kern T U,Viswanathan R.Creep-resistant Steels[M].New York:CRC Press,2008:329-349.
- [21]Klueh R L.Elevated-Temperature Ferritic and Martensitic Steels and Their Application to Future Nuclear Reactors[M].Oak Ridge,Tennessee:Oak Ridge National Laboratory,2004:10-32.
- [22]Bhadeshia H K D H,Honeycombe R W K.Steel-Microstructure and Properties,3rd edition[M].London:Linacre House,2006:247-249.
- [23]崔彤,王磊,杨洪才,等.长期时效对一种镍基合金组织及冲击性能的影响[J].有色矿冶,2005,21:33-36.CUI Tong,WANG Lei,YANG Hong-cai,et al.Microstructures and impact toughness of a Ni-based superalloy after long-term aging[J].Non-Ferrous Mining and Metallurgy,2005,21(1):33-36.
- [24]Dahlen M,Fischmeister H.Carbide precipitation in superalloys[C]//Superalloys 1980.Metals Park,Ohio:ASM,1980:449-454.
- [25]Rolfest B.The dependence of fatigue crack propagation on strain energy release rate and crack opening displacement[J].ASTM STP,1970,446:281-288.
- [26]郝宪朝,高明,张龙,等.退火态12Cr13不锈钢显微组织及其对冲击韧性的影响[J].金属学报,2011,47(7):912-916.HAO Xian-chao,GAO Ming,ZHANG Long,et al.Microstructure of annealed 12Cr13 stainless steel and its effect on the impact toughness[J].Acta Metallurgica Sinica,2011,47(7):912-916.
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