热机械加工对Al-13.0Zn-3.16Mg-2.8Cu-0.2Zr-0.07Sr合金组织与性能的影响Effect of thermo-mechanical processing on microstructure and properties of Al-13.01Zn-3.16Mg-2.8Cu-0.204Zr-0.0757Sr aluminum alloy
徐驰,许晓静,郭云飞,马文海,王子路,陈洋
摘要(Abstract):
采用X射线衍射分析(XRD)、电子背散射衍射分析(EBSD)、电导率测试、硬度测试、晶间腐蚀试验和剥落腐蚀试验,研究了预回复固溶时效处理前的热机械加工(Thermo-mechanical processing,TMP)对超高强铝合金Al-13.01Zn-3.16Mg-2.8Cu-0.2Zr-0.07Sr组织及性能的影响。结果表明,TMP(450℃/2 h+460℃/2 h+470℃/2 h(水淬)固溶、400℃/24 h过时效、约45%压缩量)处理后降低了合金的位错密度(0.150→0),减小了平均晶粒尺寸(6.256μm→5.012μm)和平均晶界角度,显著提高了低角度晶界数目百分比(0.618→0.700),电导率(25.3%IACS→27.2%IACS)和伸长率(8.1%→8.2%)基本未发生变化,降低了硬度(229.6 HV→221.0 HV)、屈服强度(653.8 MPa→599.5 MPa)、抗拉强度(701.9 MPa→646.3 MPa),提高了抗晶间腐蚀和抗剥落腐蚀性能。定量分析显示,热机械加工轻微提高了合金位错强化、低角度晶界强化和高角度晶界强化的总强化,合金强度的降低主要归因于合金固溶强化和时效沉淀析出相强化的总强化的降低。抗腐蚀性能的提高可以归因于合金低角度晶界数目百分比的提高。
关键词(KeyWords): Al-Zn-Mg-Cu合金;热机械加工;高/低角度晶界;电导率;腐蚀性能
基金项目(Foundation): 江苏大学研究生科研创新计划项目(KYXX_0031);; 江苏省优势学科资助
作者(Author): 徐驰,许晓静,郭云飞,马文海,王子路,陈洋
DOI: 10.13289/j.issn.1009-6264.2016.02.010
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