时效温度对00Cr11Ni8Co7Mo3马氏体钢显微组织和力学性能的影响Effect of aging temperature on microstructure and mechanical properties of 00Cr11Ni8Co7Mo3 martensitic steel
孙世豪,李洲,邓想涛,石如星,徐流杰
摘要(Abstract):
采用真空冶炼技术制备了00Cr11Ni8Co7Mo3马氏体钢,经过锻造、1000℃固溶处理和800℃二次固溶处理后,研究了不同温度(300~600℃)时效处理对其微观组织和力学性能的影响。结果表明:当时效温度为500℃时,试验钢中的马氏体板条的平均宽度为8.34μm,在马氏体板条之间生成了5.9 vol%薄膜状的逆转变奥氏体,此时试验钢的力学性能表现出最佳的强韧性匹配,室温和低温(-196℃)屈服强度分别为1251.6和1508.1 MPa,室温和低温(-196℃)冲击吸收能量分别为96.2和43.1 J;当时效温度为400℃时,马氏体板条宽度增加至9.65μm,且基体中无明显逆转变奥氏体生成,室温以及低温(-196℃)冲击吸收能量最低,分别为66.2和25.2 J;当时效温度升高至600℃时,马氏体板条平均宽度降低至5.10μm,逆转变奥氏体相体积分数增至13.8 vol%,由于部分逆转变奥氏体出现了较大的块状结构,无法有效抑制裂纹扩展,导致试验钢的冲击韧性下降,室温和低温(-196℃)冲击韧性分别下降至90.4和33.8 J。
关键词(KeyWords): 马氏体时效不锈钢;热处理;微观组织;力学性能
基金项目(Foundation): 国家重点研发计划(2022YFB3705300);; 河南省重点研发专项(231111230400)
作者(Author): 孙世豪,李洲,邓想涛,石如星,徐流杰
DOI: 10.13289/j.issn.1009-6264.2024-0536
参考文献(References):
- [1] Man C,Dong C,Kong D,et al.Beneficial effect of reversed austenite on the intergranular corrosion resistance of martensitic stainless steel[J].Corrosion Science,2019,151:108-121.
- [2] Cheng Z,Sun S,Du X,et al.Microstructural evolution of a FeCo15Cr14Ni4Mo3 maraging steel with high ductility prepared by selective laser melting[J].Materials Today Communications,2022,31:103243.
- [3] Zhan L,Xie H,Yang Y,et al.Investigation on creep deformation and age strengthening behavior of 304 stainless steel under high stress levels[J].Materials,2024,17(3):642.
- [4] Lin Q E,Wu C D,Zhang Y W,et al.Enhancement of the compressive performances of additive manufactured Corrax maraging stainless steel lattice by heat treatment[J].Journal of Materials Research and Technology,2024,33:1640-1653.
- [5] 潘钱付,牛犇,贾玉振,等.热处理工艺对Fe-12Cr马氏体钢组织与力学性能的影响[J].材料热处理学报,2020,41(5):102-109.PAN Qian-fu,NIU Ben,JIA Yu-zhen,et al.Effect of heat treatment on microstructure and mechanical properties of Fe-12Cr martensitic steel[J].Transactions of Materials and Heat Treatment,2020,41(5):102-109.
- [6] Galindo-Nava E I,Rainforth W M,Rivera-Díaz-del-Castillo P E J.Predicting microstructure and strength of maraging steels:Elemental optimisation[J].Acta Materialia,2016,117:270-285.
- [7] Zhang H,Ji X,Ma D,et al.Effect of aging temperature on the austenite reversion and mechanical properties of a Fe-10Cr-10Ni cryogenic maraging steel[J].Journal of Materials Research and Technology,2021,11:98-111.
- [8] Raabe D,Sandl?bes S,Millán J,et al.Segregation engineering enables nanoscale martensite to austenite phase transformation at grain boundaries:A pathway to ductile martensite[J].Acta Materialia,2013,61(16):6132-6152.
- [9] Wang M M,Tasan C C,Ponge D,et al.Smaller is less stable:Size effects on twinning vs.transformation of reverted austenite in TRIP-maraging steels[J].Acta Materialia,2014,79:268-281.
- [10] 周海萍,王中伟,张弘斌,等热处理对选区激光熔化马氏体不锈钢腐蚀行为及组织的影响[J].材料热处理学报,2024,45(2):102-111.ZHOU Hai-ping,WANG Zhong-wei,ZHANG Hong-bin,et al.Effect of heat treatment on corrosion behavior and microstructure of martensitic stainless steel prepared by selective laser melting[J].Transactions of Materials and Heat Treatment,2024,45(2):102-111.
- [11] 白璇,赵昆渝,姜雯,等冷处理对超级马氏体不锈钢组织及逆变奥氏体的影响[J].材料热处理学报,2015,36(3):96-100.BAI Xuan,ZHAO Kun-yu,JIANG Wen,et al.Effect of cold treatment on microstructure and reversed austenite of super martensitic stainless steel[J].Transactions of Materials and Heat Treatment,2015,36(3):96-100.
- [12] 黄玉山,谭超林,马文有,等.热处理对选区激光熔化马氏体时效钢组织和性能的影响[J].材料热处理学报,2017,38(11):59-64.HUANG Yu-shan,TAN Chao-lin,MA Wen-you,et al.Effect of heat treatment on microstructure and properties of selective laser melting maraging steel[J].Transactions of Materials and Heat Treatment,2017,38(11):59-64.
- [13] Cao H,Luo X,Zhan G,et al.Effect of intercritical quenching on the microstructure and cryogenic mechanical properties of a 7 pct Ni steel[J].Metallurgical and Materials Transactions A,2017,48(9):4403-4410.
- [14] Yang M,Zhang D,Yao Z,et al.Precipitation behavior of the G-phase strengthened 7Ni maraging steels[J].Journal of Materials Research and Technology,2023,26:9261-9275.
- [15] Hou W,Liu Q,Gu J.Martensitic transformation of reversed austenite in a low-carbon 7Ni steel[J].Philosophical Magazine Letters,2024,104(1):2393615.
- [16] Sun C,Liu S L,Misra R D K,et al.Influence of intercritical tempering temperature on impact toughness of a quenched and tempered medium-Mn steel:Intercritical tempering versus traditional tempering[J].Materials Science and Engineering A,2018,711:484-491.
- [17] Anoop C R,Prakash A,Narayana Murty S V S,et al.Origin of low temperature toughness in a 12Cr-10Ni martensitic precipitation hardenable stainless steel[J].Materials Science and Engineering A,2018,709:1-8.
- [18] Kolomy S,Sedlak J,Zouhar J,et al.Influence of aging temperature on mechanical properties and structure of M300 maraging steel produced by selective laser melting[J].Materials,2023,16(3):977.
- [19] Afshari E,Ghaffari M,Vahedi Nemani A,et al.Effect of heat treatment on microstructure and tribological performance of PH 13-8Mo stainless steel fabricated via wire arc additive manufacturing[J].Wear,2023,526-527:204947.
- [20] Hou H,Li H,Jin Y,et al.Effect of heat treatment temperature on the mechanical properties of low-temperature high strength maraging steel[J].Materials Science and Engineering A,2014,601:1-6.
- [21] Shen L C,Yang X H,Ho J R,et al.Effects of build direction on the mechanical properties of a martensitic stainless steel fabricated by selective laser melting[J].Materials,2020,13(12):5142.
- [22] Wang C,Ma R,Zhou Y,et al.Effects of rare earth modifying inclusions on the pitting corrosion of 13Cr4Ni martensitic stainless steel[J].Journal of Materials Science & Technology,2021,93:232-243.
- [23] Lian Y,Zhang J,Ji P,et al.Effect of tempering treatment on atmospheric corrosion behavior of 3Cr13 martensitic stainless steel in marine environment[J].Journal of Materials Engineering and Performance,2022,31(6):4963-4973.
- [24] Foroozmehr F,Bocher P J F.An investigation on fracture toughness of the heat-affected zone in the welded joints of 13 % Cr-4 % Ni martensitic stainless steels[J].Fatigue and Fracture of Engineering Materials and Structures,2021,44(12):3416-3430.
- [25] Yang T,Xue S,Zheng L,et al.Crack investigation of martensitic stainless steel turbine blade in thermal power plant[J].Engineering Failure Analysis,2021,127:105553.
- [26] 王明明,魏晨阳,郭广顺,等.超高强度马氏体基钢强韧化及疲劳性能研究进展[J].材料热处理学报,2023,44(3):17-27.WANG Ming-ming,WEl Chen-yang,GUO Guang-shun,et al.Research progress on strengthening,toughening and fatigue properties of ultra-high-strength martensitic-based steel[J].Transactions of Materials and Heat Treatment,2023,44(3):17-27.
- [27] Hou H,Qi L,Zhao Y H.Effect of austenitizing temperature on the mechanical properties of high-strength maraging steel[J].Materials Science and Engineering A,2013,587:209-212.
- [28] Markfeld A,Rosen A.The effect of reverted austenite on the plastic deformation of maraging steel[J].Materials Science and Engineering A,1980,46(2):151-157.
- [29] Xie Z J,Ren Y Q,Zhou W H,et al.Stability of retained austenite in multi-phase microstructure during austempering and its effect on the ductility of a low carbon steel[J].Materials Science and Engineering A,2014,603:69-75.
- [30] Song Y Y,Ping D H,Yin F X,et al.Microstructural evolution and low temperature impact toughness of a Fe-13 %Cr-4%Ni-Mo martensitic stainless steel[J].Materials Science and Engineering A,2010,527(3):614-618.
- [31] Ghasemi-Nanesa H,Nili-Ahmadabadi M,Koohdar H R,et al.Strain-induced martensite to austenite reverse transformation in an ultrafine-grained Fe-Ni-Mn martensitic steel[J].Philosophical Magazine,2014,94(13):14931507.
- [32] Wang M,Huang M X.Abnormal TRIP effect on the work hardening behavior of a quenching and partitioning steel at high strain rate[J].Acta Materialia,2020,188:551-559.
- [33] Yuan L,Ponge D,Wittig J,et al.Nanoscale austenite reversion through partitioning,segregation and kinetic freezing:Example of a ductile 2GPa Fe-Cr-C steel[J].Acta Materialia,2012,60(6):2790-2804.
文章评论(Comment):
|
||||||||||||||||||
|
||||||||||||||||||