后处理对电子束熔化成形Ti48Al2Cr2Nb合金组织及性能的影响Effect of post-treatment on microstructure and properties of Ti48Al2Cr2Nb alloy prepared by electron beam melting
高宇翔,李忠文,刘凯,杨东野
摘要(Abstract):
采用电子束熔化成形(EBM)技术制备了Ti48Al2Cr2Nb合金试棒,并对其进行后处理。采用X射线衍射仪(XRD)、扫描电镜(SEM)、显微硬度计及万能材料试验机等研究了未处理、热等静压(HIP)及热处理后合金的显微组织及力学性能。结果表明:EBM制备的Ti48Al2Cr2Nb合金组织以γ相和α_2相为主。热等静压处理后,合金的致密度由3.1441 g/cm~3增加至3.5343 g/cm~3,显微硬度由257 HV0.1增加至315 HV0.1。热处理后,合金的晶粒发生明显长大,随着保温温度由1220℃升高至1280℃,等轴γ组织的体积分数由50.12%降低至19.37%。热处理后合金的拉伸强度相较于未处理试样(403 MPa)均有一定下降,1260℃保温120 min后合金的拉伸强度降低至268 MPa。
关键词(KeyWords): TiAl合金;电子束熔化成形(EBM);热处理;热等静压
基金项目(Foundation): 上海市Ⅲ类高峰学科-材料科学与工程(高能束智能加工与绿色制造)
作者(Author): 高宇翔,李忠文,刘凯,杨东野
DOI: 10.13289/j.issn.1009-6264.2023-0145
参考文献(References):
- [1] Xu R R,Li M Q,Zhao Y H.A review of microstructure control and mechanical performance optimization of γ-TiAl alloys[J].Journal of Alloys and Compounds,2023,932:167611.
- [2] Xi X X,Ding W F,Wu Z X,et al.Performance evaluation of creep feed grinding of γ-TiAl intermetallics with electroplated diamond wheels[J].Chinese Journal of Aeronautics,2021,34(6):100-109.
- [3] 寇宏超,程亮,唐斌,等.高温TiAl合金热成形技术研究进展[J].航空制造技术,2016,59(21):24-31.KOU Hong-chao,CHENG Liang,TANG Bin,et al.Progress on hot-forming techniques of high temperature TiAl alloys[J].Aeronautical Manufacturing Technology,2016,59(21):24-31.
- [4] 张琛,杨森,颜银标.TiAl基合金成形技术的研究现状[J].兵器材料科学与工程,2017,40(4):126-132.ZHANG Chen,YANG Sen,YAN Yin-biao.Research progress in manufacturing of TiAl alloys[J].Ordnance Material Science and Engineering,2017,40(4):126-132.
- [5] 汤慧萍,李会霞,车倩颖,等.电子束粉床3D打印TiAl金属间化合物研究进展[J].精密成形工程,2022,14(11):30-46.TANG Hui-ping,LI Hui-xia,CHE Qian-ying,et al.Research progress of TiAl intermetallics fabricated by electron beam-powder bed fusion[J].Journal of Netshape Forming Engineering,2022,14(11):30-46.
- [6] 车倩颖,李会霞,贺卫卫,等.TiAl合金粉床电子束选区熔化成形研究进展[J].航空制造技术,2021,64(3):52-60.CHE Qian-ying,LI Hui-xia,HE Wei-wei,et al.Research progress in TiAl alloys prepared by powder selective electron beam melting[J].Aeronautical Manufacturing Technology,2021,64(3):52-60.
- [7] Todai M,Nakano T,Liu T Q,et al.Effect of building direction on the microstructure and tensile properties of Ti-48Al-2Cr-2Nb alloy additively manufactured by electron beam melting[J].Additive Manufacturing,2017,13:61-70.
- [8] 王茂松,杜宇雷.增材制造钛铝合金研究进展[J].航空学报,2021,42(7):8-31.WANG Mao-song,DU Yu-lei.Research progress of additive manufacturing of TiAl alloys[J].Acta Aeronautica et Astronautica Sinica,2021,42(7):8-31.
- [9] 梁啸宇,张磊,林峰.电子束粉末床熔融制备钛铝基金属间化合物研究进展[J].精密成形工程,2022,14(11):81-97.LIANG Xiao-yu,ZHANG Lei,LIN Feng.Research progress of TiAl intermetallic fabricated by electron beam powder bed fusion[J].Journal of Netshape Forming Engineering,2022,14(11):81-97.
- [10] Schwerdtfeger J,K?rner C.Selective electron beam melting of Ti-48Al-2Nb-2Cr:Microstructure and aluminium loss[J].Intermetallics,2014,49:29-35.
- [11] Juechter V,Franke M M,Merenda T,et al.Additive manufacturing of Ti-45Al-4Nb-C by selective electron beam melting for automotive applications[J].Additive Manufacturing,2018,22:118-126.
- [12] Tang H P,Yang G Y,Jia W P,et al.Additive manufacturing of a high niobium-containing titanium aluminide alloy by selective electron beam melting[J].Materials Science and Engineering A,2015,636:103-107.
- [13] Kan W B,Liang Y F,Peng H,et al.Microstructural degradation of Ti-45Al-8Nb alloy during the fabrication process by electron beam melting[J].JOM,2017,69:2596-2601.
- [14] Wang J,Yang K,Liu N,et al.Microstructure and tensile properties of Ti-48Al-2Cr-2Nb rods additively manufactured by selective electron beam melting[J].JOM,2017,69:2751-2755.
- [15] Zhou J,Li H X,Yu Y F,et al.Research on aluminum component change and phase transformation of TiAl-based alloy in electron beam selective melting process under multiple scan[J].Intermetallics,2019,113:106575.
- [16] 冉江涛,赵鸿,高华兵,等.电子束选区熔化成形技术及应用[J].航空制造技术,2019,62(Z1):46-57.RAN Jiang-tao,ZHAO Hong,GAO Hua-bing,et al.Selective electron beam melting technique and its application[J].Aeronautical Manufacturing Technology,2019,62(Z1):46-57.
- [17] Laleh M,Sadeghi E,Revilla R I,et al.Heat treatment for metal additive manufacturing[J].Progress in Materials Science,2023,133:101051.
- [18] Biamino S,Penna A,Ackelid U,et al.Electron beam melting of Ti-48Al-2Cr-2Nb alloy:Microstructure and mechanical properties investigation[J].Intermetallics,2011,19(6):776-781.
- [19] Tebaldo V,Faga M G.Influence of the heat treatment on the microstructure and machinability of titanium aluminides produced by electron beam melting[J].Journal of Materials Processing Technology,2017,244:289-303.
- [20] Yue H Y,Chen Y Y,Wang X P,et al.Effect of beam current on microstructure,phase,grain characteristic and mechanical properties of Ti-47Al-2Cr-2Nb alloy fabricated by selective electron beam melting[J].Journal of Alloys and Compounds,2018,750:617-625.
- [21] Schloffer M,Iqbal F,Gabrisch H,et al.Microstructure development and hardness of a powder metallurgical multi phase γ-TiAl based alloy[J].Intermetallics,2012,22:231-240.
- [22] Li W,Li M,Yang Y,et al.Enhanced compressive strength and tailored microstructure of selective laser melted Ti-46.5 Al-2.5 Cr-2Nb-0.5 Y alloy with different boron addition[J].Materials Science and Engineering A,2018,731:209-219.
- [23] 王敏智.热处理对TiAl基合金组织与性能的影响[D].南京:南京理工大学,2016.WANG Min-zhi.Effects of heat treatment on the microstructure and mechanical property of TiAl alloy[D].Nanjing:Nanjing University of Science and Technology,2016.
- [24] 陈玮,杨洋,刘亮亮,等.电子束增材制造γ-TiAl显微组织调控与拉伸性能研究[J].航空制造技术,2017,60(Z1):37-41.CHEN Wei,YANG Yang,LIU Liang-liang,et al.Microstructure control and tensile properties of EBM γ-TiAl[J].Aeronautical Manufacturing Technology,2017,60(Z1):37-41.
- [25] 岳航宇.电子束选区熔化成形Ti-47Al-2Cr-2Nb合金的组织及力学性能研究[D].哈尔滨:哈尔滨工业大学,2019.YUE Hang-yu.Study on the microstructure and mechanical property of Ti-47Al-2Cr-2Nb alloy fabricated by selective electron beam melting[D].Harbin:Harbin Institute of Technology,2019.
- [26] Wang Y,Wang Y T,Li R D,et al.Hall-Petch relationship in selective laser melting additively manufactured metals:using grain or cell size?[J].Journal of Central South University,2021,28(4):1043-1057.
文章评论(Comment):
|
||||||||||||||||||
|
||||||||||||||||||