电沉积温度对熔融盐电沉积Ni/W复合层的影响Effect of electrodeposited temperature on properties of Ni/W coating by electrodeposition in molten salt
戴志强,赵丽宏,石伟,刘建涛,李运刚,田薇,齐艳飞
摘要(Abstract):
采用熔盐电沉积法制备了Ni/W复合层,通过扫描电镜,辉光放电光谱仪和电子背散射衍射技术对Ni/W复合层的微观结构、复合层厚度、晶粒尺寸及小角度晶界频率进行了表征。结果表明,Ni/W复合层的断裂方式为解理断裂;当电沉积温度为1073 K时,Ni/W复合层的表面平整光滑,晶粒尺寸大小均匀;随电沉积温度升高,复合层厚度逐渐增加,Ni在钨板中的扩散系数增大,小角度晶界频率增加。
关键词(KeyWords): Ni/W复合层;微观结构;复合层厚度;晶粒尺寸;小角度晶界
基金项目(Foundation): 国家自然科学基金(51274082)
作者(Author): 戴志强,赵丽宏,石伟,刘建涛,李运刚,田薇,齐艳飞
DOI: 10.13289/j.issn.1009-6264.2016.12.023
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