TC4钛合金在不同固溶温度下的微观结构及动态力学行为Microstructure and dynamic mechanical behavior of TC4 titanium alloy at different solution treatment temperatures
刘涛,史正宏,雷经发,王璐,柏威
摘要(Abstract):
首先对TC4钛合金进行了不同温度(850、900、920、960和1000℃)的固溶处理,采用X射线衍射(XRD)、扫描电镜(SEM)和电子背散射衍射(EBSD)技术研究了不同温度固溶处理后TC4钛合金试样的显微组织和物相,采用分离式霍普金森拉杆(SHTB)实验装置测试了其动态拉伸力学性能,并对断口形貌进行分析。结果表明:随着固溶温度的升高,TC4钛合金的初生α相含量降低,针状α′相含量升高,晶粒细化、小角度晶界占比增加且择优取向强度增大;在高应变率拉伸载荷作用下,随固溶温度的升高,TC4钛合金的动态屈服强度增加、断裂伸长率降低;未固溶和固溶处理后的试样动态拉伸断口均表现出韧性断裂特征,固溶温度为850℃时塑性最好。
关键词(KeyWords): TC4钛合金;固溶温度;微观组织;动态力学性能;断口
基金项目(Foundation): 安徽省高等学校自然科学研究重大项目(2023AH040036);; 合肥市自然科学基金项目(2024035);; 安徽高校协同创新项目(GXXT-2023-025)
作者(Author): 刘涛,史正宏,雷经发,王璐,柏威
DOI: 10.13289/j.issn.1009-6264.2024-0423
参考文献(References):
- [1] Han X,Ma J,Tian A,et al.Surface modification techniques of titanium and titanium alloys for biomedical orthopaedics applications:A review[J].Colloids and Surfaces B:Biointerfaces,2023,227:113339.
- [2] Li Y,Zhou Z,He Y.Tribocorrosion and surface protection technology of titanium alloys:A review[J].Materials,2023,17(1):65.
- [3] Gao K,Zhang Y,Yi J,et al.Overview of surface modification techniques for titanium alloys in modern material science:A comprehensive analysis[J].Coatings,2024,14(1):148.
- [4] Wu J,Shen M,Wang W,et al.High power arc ion plating of thick Cr2N hard coating on Ti-based alloys:Oxidation and wear behaviors[J].Surface and Coatings Technology,2022,448:128924.
- [5] 西禹,张强,张欣钥,等.增材制造TC4钛合金的动态力学行为研究[J].力学学报,2022,54(2):425-444.XI Yu,ZHANG Qiang,ZHANG Xin-yue,et al.Dynamic mechanical behavior of additive manufacturing TC4 alloy[J].Chinese Journal of Theoretical and Applied Mechanics,2022,54(2):425-444.
- [6] 朱磊,刘洋,孟锦晖,等.激光选区熔化Ti-6Al-4V合金的动态力学性能及其本构关系[J].爆炸与冲击,2022,42(9):90-99.ZHU Lei,LIU Yang,MENG Jin-hui,et al.Dynamic mechanical properties and constitutive relationship of selective laser melted Ti-6Al-4V alloy[J].Explosion and Shock Waves,2022,42(9):90-99.
- [7] 宁子轩,王琳,程兴旺,等.分离式霍普金森压杆加载下不同组织Ti-6321钛合金的动态响应行为[J].兵工学报,2021,42(4):862-870.NING Zi-xuan,WANG Lin,CHENG Xing-wang,et al.Dynamic response behaviors of Ti-6321 titanium alloys with different microstructures under split hopkinson pressure bar loading[J].Acta Armamentarii,2021,42(4):862-870.
- [8] Lee S W,Park C H,Hong J K,et al.Effect of solution treatment and aging conditions on tensile properties of Ti-Al-Fe-Si alloy[J].Materials Science and Engineering A,2017,697:158-166.
- [9] 张启飞,杨帅,刘书君,等.时效处理对Ti55531钛合金微观组织演变规律及力学性能的影响[J].稀有金属材料与工程,2022,51(7):2645-2653.ZHANG Qi-fei,YANG Shuai,LIU Shu-jun,et al.Effect of aging treatment on microstructure evolution and mechanical properties of Ti55531 titanium alloy[J].Rare Metal Materials and Engineering,2022,51(7):2645-2653.
- [10] Zhou C,Zhan L H,Li H,et al.Influence of temperature on creep behavior,mechanical properties and microstructural evolution of an Al-Cu-Li alloy during creep age forming[J].Journal of Central South University,2021,28(8):2285-2294.
- [11] Wei K,Xiao L,Gao B,et al.Effect of aging temperature on the hardening behavior and precipitation evolution of Mg-10Gd alloy[J].Materials Characterization,2023,196:112580.
- [12] 徐铁伟,李金山,张丰收,等.TB8钛合金双级时效过程中的组织演变及时效响应[J].材料热处理学报,2016,37(2):58-64.XU Tie-wei,LI Jin-shan,ZHANG Feng-shou,et al.Microstructure evolution and aging response during duplex aging of TB8 titanium alloy[J].Transactions of Materials and Heat Treatment,2016,37(2):58-64.
- [13] 马权,曹迪.双级时效处理对TB8合金组织和性能的影响[J].材料热处理学报,2017,38(10):41-45.MA Quan,CAO Di.Effect of double aging treatment on microstructure and mechanical property of TB8 titanium alloy[J].Transactions of Materials and Heat Treatment,2017,38(10):41-45.
- [14] 吴晨,马宝飞,肖松涛,等.航天紧固件用TC4钛合金棒材固溶时效后的组织与性能[J].金属热处理,2021,46(11):166-169.WU Chen,MA Bao-fei,XIAO Song-tao,et al.Microstructure and properties of TC4 titanium alloy bar for aerospace fasteners after solid solution treatment and aging[J].Heat Treatment of Metals,2021,46(11):166-169.
- [15] 覃佳栋,马雄,史晓强,等.固溶处理对Ti-22Al-25Nb合金棒材组织与拉伸性能的影响[J].热加工工艺,2020,49(18):144-147.QIN Jia-dong,MA Xiong,SHI Xiao-qiang,et al.Effects of solution treatment on microstructure and tensile properties of Ti-22Al-25Nb alloy bar[J].Hot Working Technology,2020,49(18):144-147.
- [16] 高鹏,刘玲玉.固溶工艺对Ti-6Al-4V铸造合金力学性能的影响[J].材料热处理学报,2019,40(9):39-43.GAO Peng,LIU Ling-yu.Effect of solid solution treatment on mechanical properties of Ti-6Al-4V casting alloy[J].Transactions of Materials and Heat Treatment,2019,40(9):39-43.
- [17] Peng X N,Guo H Z,Shi Z F,et al.Microstructure characterization and mechanical properties of TC4-DT titanium alloy after thermomechanical treatment[J].Transactions of Nonferrous Metals Society of China,2014,24(3):682-689.
- [18] 丁灿,汪常亮,李峰,等.固溶-冷速-时效对TC4-DT合金显微组织和力学性能的影响[J].稀有金属材料与工程,2020,49(3):962-967.DING Can,WANG Chang-liang,LI Feng,et al.Effects of solid solution,cooling rates and aging treatments on microstructure and mechanical properties of TC4-DT alloy[J].Rare Metal Materials and Engineering,2020,49(3):962-967.
- [19] 鲁媛媛,张怡,郭帅,等.固溶温度对3D打印TC4钛合金显微组织和力学性能的影响[J].金属热处理,2020,45(11):171-176.LU Yuan-yuan,ZHANG Yi,GUO Shuai,et al.Influence of solution treatment temperature on microstructure and mechanical properties of TC4 titanium alloy prepared by 3D printing[J].Heat Treatment of Metals,2020,45(11):171-176.
- [20] 杨光,邵帅,王超,等.固溶温度对激光沉积制造Ti-6Al-2Mo-2Sn-2Zr-2Cr-2V钛合金组织及力学行为影响[J].稀有金属,2021,45(3):264-271.YANG Guang,SHAO Shuai,WANG Chao,et al.Microstructure and mechanical behavior of Ti-6Al-2Mo-2Sn-2Zr-2Cr-2V titanium alloy fabricated by laser deposition with change of solution temperature[J].Chinese Journal of Rare Metals,2021,45(3):264-271.
- [21] 刘全明,张朝晖,刘世锋,等.固溶处理对TC16钛合金显微组织和拉伸性能的影响[J].四川大学学报(自然科学版),2015,52(2):377-382.LIU Quan-ming,ZHANG Zhao-hui,LIU Shi-feng,et al.Effects of solution treatment on the microstructures and tensile properties of TC16 titanium alloy[J].Journal of Sichuan University (Natural Science Edition),2015,52(2):377-382.
- [22] 商国强,张晓泳,王新南,等.冷却速率对TB17钛合金显微组织和力学性能的影响[J].中国有色金属学报,2023,33(6):1758-1768.SHANG Guo-qiang,ZHANG Xiao-yong,WANG Xin-nan,et al.Effect of cooling rate on microstructure and properties of TB17 titanium alloy[J].The Chinese Journal of Nonferrous Metals,2023,33(6):1758-1768.
- [23] 张志强,董利民,胡明,等.冷却速率对TC16钛合金显微组织和力学性能的影响[J].中国有色金属学报,2019,29(7):1391-1398.ZHANG Zhi-qiang,DONG Li-min,HU Ming,et al.Effect of cooling rate on microstructure and mechanical properties of TC16 titanium alloy[J] The Chinese Journal of Nonferrous Metals,2019,29(7):1391-1398.
- [24] Lu B,Li Y,Wang H Y,et al.Effects of cooling rates on the solidification behavior,microstructural evolution and mechanical properties of Al-Zn-Mg-Cu alloys[J].Journal of Materials Research and Technology,2023,22:2532-2548.
- [25] Xu K H,Xue Y,Zhang Z M,et al.The effect of heat treatment on α/β phases evolution of TC4 titanium alloy fabricated by spark plasma sintering[J].Procedia Manufacturing,2020,50:713-718.
- [26] 彭美旗,程兴旺,郑超,等.转变β区体积分数对双态组织TC4钛合金动态压缩性能及其绝热剪切敏感性的影响规律[J].稀有金属材料工程,2017,46(8):2227-2233.PENG Mei-qi,CHENG Xing-wang,ZHENG Chao,et al.Effects of volume fraction of transformed β matrix on dynamic mechanical properties and sensitivity of adiabatic shear banding in bimodal microstructures of TC4 alloy[J].Rare Metal Materials and Engineering,2017,46(8):2227-2233.
- [27] 翟大军,税玥,袁满,等.α相含量及形态对TC4钛合金组织和力学性能的影响[J].金属热处理,2019,44(10):129-134.ZHAI Da-jun,SHUI Yue,YUAN Man,et al.Effects of content and morphology of α phase on microstructure and mechanical properties of TC4 alloy[J].Heat Treatment of Metals,2019,44(10):129-134.
- [28] 詹奇云,靳刚,韩进,等.TC4钛合金低温拉伸行为与本构建模[J].塑性工程学报,2024,31(1):204-215.ZHAN Qi-yun,JIN Gang,HAN Jin,et al.Low temperature tensile behavior and constitutive modeling of TC4 titanium alloy[J].Journal of Plasticity Engineering,2024,31(1) :204-215.
- [29] 张昭,郭保桥,冉春,等.固溶温度对TB6钛合金动态力学性能和微观组织的影响[J].高压物理学报,2021,35(6):107-113.ZHANG Zhao,GUO Bao-qiao,RAN Chun,et al.Effect of solution temperature on dynamic mechanical properties and microstructure of TB6 titanium alloy[J].Chinese Journal of High Pressure Physics,2021,35(6):107-113.
- [30] 陈稳,郭保桥,郭岩松,等.时效温度对TB8钛合金动态力学性能的影响[J].高压物理学报,2022,36(5):66-76.CHEN Wen,GUO Bao-qiao,GUO Yan-song,et al.Effect of aging temperature on dynamic mechanical properties of TB8 titanium alloy[J].Chinese Journal of High Pressure Physics,2022,36(5):66-76.
- [31] 冯恩昊,陈蓉,邸士雄,等.热处理对选区激光熔化TC4合金微观组织及力学性能的影响规律研究[J].中国激光,2024,51(10):298-309.FENG En-hao,CHEN Rong,DI Shi-xiong,et al.Effect of heat treatment on microstructure and mechanical properties of TC4 alloy by selective laser melting[J].Chinese Journal of Lasers,2024,51(10):298-309.
- [32] 刘涛,邵博,雷经发,等.固溶温度对TC4钛合金微观组织和动态拉伸力学性能的影响[J].稀有金属材料与工程,2023,52(12):4133-4140.LIU Tao,SHAO Bo,LEI Jing-fa,et al.Effect of solid solution temperature on microstructure and dynamic tensile mechanical properties of TC4 titanium alloy[J].Rare Metal Materials and Engineering,2023,52(12):4133-4140.
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