物理分析法与金相法测定BT25钛合金相变点Measurement of beta transus temperature of BT25 titanium alloy by physical analysis and metallographic observation methods
田飞,曾卫东,马雄,孙宇,周义刚
摘要(Abstract):
针对BT25两相钛合金,对比研究了计算法、热膨胀法、差示扫描量热法和连续升温金相法4种方法测定(α+β)/β相变点的一致性问题。计算法根据各合金元素及杂质含量对钛合金相变点的影响值,推算出公式,得出BT25合金的相变点约为1023℃;热膨胀法和差示扫描量热法根据钛合金发生(α+β)→β转变时体积和热量的变化,测得BT25合金的相变点约分别为1029.2和1029.85℃;而连续升温金相法通过观察不同淬火温度的试样在光学显微镜下的显微组织变化,确定升温过程中初生α相完全消失的温度即为相变温度,约为1029℃。结果表明采用计算法、热膨胀法和差示扫描量热法与金相法测定BT25钛合金的(α+β)/β相变点一致,基于多种测定方法的综合运用对于钛合金相变点的准确测定具有重要意义。
关键词(KeyWords): BT25;相变点;计算法;热膨胀法;差示扫描量热法
基金项目(Foundation): 国家“973”计划(2007CB613807);; 新世纪优秀人才支持计划(NCET-07-0696);; 凝固技术国家重点实验室开放课题(35-TP-2009)
作者(Author): 田飞,曾卫东,马雄,孙宇,周义刚
DOI: 10.13289/j.issn.1009-6264.2011.05.002
参考文献(References):
- [1]袁绍冲,毛小南,张鹏省,等.热强钛合金BT25的组织与性能[J].钛工业进展,2006,23(3):19-22.YUAN Shao-chong,MAO Xiao-nan,ZHANG Peng-sheng,et al.Microstructure and property of heat strong titanium alloy BT25[J].Titanium IndustryProgress,2006,23(3):19-22.
- [2]白晓环,吕平,徐庆.热处理工艺对BT25钛合金锻件的组织与性能的影响[J].钛工业进展,2008,25(5):20-22.BAI Xiao-huan,LPing,XU Qing.Influence of treatment process on the structure and performance of forgings of titanium alloy BT25[J].TitaniumIndustry Progress,2008,25(5):20-22.
- [3]王金友.航空用钛合金[M].上海:上海科学技术出版社,1985.
- [4]李明怡.航空用钛合金结构材料[J].世界有色金属,2000,(6):17-20.LI Ming-yi.Titanium structure material using in airplane[J].World Nonferrous Metals,2000,(6):17-20.
- [5]Shang Shun li,Shen Jian yun,Wang Xi zhe.Transformation textures in anα+βtitanium alloy thin sheet[J].Materials Science and Engineering A,2002,326:249-254.
- [6]鲍利索娃(苏).钛合金金相学[M].北京:国防工业出版社,1986.
- [7]Zhou Y G,Zeng W D,Yu H Q.An investigation of a new near-beta forging process for titanium alloys and its application in aviation components[J].Materials Science and Engineering A,2005,393:204-212.
- [8]李晓芹,周义刚,俞汉清,等.钛合金完全相变温度的检测方法[J].热加工工艺,1990,(3):35-38.LI Xiao-qing,ZHOU Yi-gang,YU Han-qing,et al.Measuring method about complete transformation temperature of titanium alloy[J].Hot WorkingTechnology,1990,(3):35-38.
- [9]唐普放.钛及钛合金相变温度与测定[J].钛工业进展,1999,(3):34-37.TANG Pu-fang.The measurement of transformation temperature of titanium and titanium alloy[J].Titanium Industry Progress,1999,(3):34-37.
- [10]《稀有金属材料加工手册》编写组.稀有金属材料加工手册[M].北京:冶金工业出版社,1984.
- [11]孙宇,曾卫东,赵永庆,等.应用人工神经网络研究化学元素对钛合金相变点的影响[J].稀有金属材料与工程,2010,39(6):1031-1035.SUN Yu,ZENG Wei-dong,ZHAO Yong-qing,et al.Study on effects of alloying elements onβtransus temperature of titanium alloys using artificialneural network[J].Rare Metal Materials and Engineering,2010,39(6):1031-1035.
- [12]张东,李凯莉.相变材料热物性测试方法[J].材料导报,2007,21(12):103-114.ZHANG Dong,LI Kai-li.Testing methods of thermal property of phase change materials[J].Materials Review,2007,21(12):103-114.
- [13]Filip R,Kubiak K,Ziaja W,et al.The effect of microstructure on the mechanical properties of two-phase titanium alloys[J].Journal of MaterialsProcessing Technology,2003,133(1-2):84-89.
- [14]陈绍楷,田弋纬,常璐,等.钛合金(α+β)/β转变温度测定的金相法与差热分析法对比研究[J].稀有金属材料与工程,2009,38(11):1916-1919.CHEN Shao-kai,TIAN Yi-wei,CHANG Lu,et al.A Comparative study of differential thermal analysis method and metallographic observation methodfor theα+β/βtransformation temperature of titanium alloys[J].Rare Metal Materials and Engineering,2009,38(11):1916-1919.
- [15]潘洪波,唐荻,胡水平,等.热分析法测量相变温度的研究[J].物理测试,2008,26(6):43-46.PAN Hong-bo,TANG Di,HU Shui-ping,et al.Development of measuring transformation temperature by thermal analysis method[J].PhysicsExamination and Testing,2008,26(6):43-46.
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