等离子喷涂纳米FeS-SiC复合涂层的显微结构研究
关耀辉,徐杨,郑仲瑜,佟晓辉
摘要(Abstract):
以自制的纳米FeS-SiC复合粉末为原料,采用等离子喷涂技术制备了纳米结构FeS-SiC复合涂层。纳米粉末及涂层的形貌、成分、结构和物相组成分别由SEM,EDS,XRD表征。实验结果表明,纳米FeS-SiC复合粉末经造粒后的颗粒尺寸分布在20~80μm,流动性好,适于等离子喷涂。等离子喷涂纳米FeS-SiC复合涂层的晶粒呈现两种尺寸分布,一种是30~80nm的小晶粒,另一种是100~200nm的大晶粒。涂层的物相主要由FeS和SiC组成,还含有少量的Fe1-xS和氧化物。涂层的气孔率大约为19%。
关键词(KeyWords): 等离子喷涂;纳米结构;FeS-SiC;复合涂层;显微结构
基金项目(Foundation): 国家自然科学基金资助项目(50375015)
作者(Author): 关耀辉,徐杨,郑仲瑜,佟晓辉
参考文献(References):
- 1 Zhu Ying-chun,Ding Chuan-xian,Yukimurac K,et al.Deposition and characterization of nanostructured WC-Co coating[J].Ceramics International,2001,27:669~674.
- 2 Goberman D,Sohn Y H,Shaw L,et al.Microstructure development of Al2O3-13wt%TiO2plasma sprayed coatings derived from nanocrystalline powders[J].Acta Materialia,2002,50:1141~1152.
- 3 Chen H,Ding C X.Nanostructured zirconia coationg prepared by atmospheric plasma spraying[J].Surface and Coatings Technology,2002,150:31~36.
- 4 Lima R S,Kucuk A,Berndt C C.Evaluation of microhardness and elastic modulus of thermally sprayed nanostructured zirconia coatings[J].Surface andCoatings Technology,2001,135:166~172.
- 5 Wang You,Jiang Stephen,Wang Meidong,et al.Abrasive wear characteristics of plasma sprayed nanostructured alumina/titania coatings[J].Wear,2000,237:176~185.
- 6 Chen Huang,Zhou Xia-ming,Ding Chuan-xian.Investigation of the thermomechanical properties of a plasma-sprayed nanostructured zirconia coating[J].Journal of the European Ceramic Society,2003,23:1449~1455.
- 7 Wang Haidou,Zhuang Daming,Wang Kunlin,et al.Comparison of the tribological properties of an ion sulfurized coating and a plasma sprayed FeS coating[J].Materials Science and Engineering,2003,357(A):321~327.
- 8 Ahmed I,Bergman T L.Thermal modeling of plasma spray deposition of nanostructured ceramics[J].Thermal Spray Technology,1999,8(3):315~322.
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