微波无压烧结制备(TiB+TiC)/Ti复合材料的组织及力学性能Microstructure and mechanical properties of (TiB+TiC)/Ti composites prepared by microwave pressureless sintering
宋光远,雷鹰,李雨,陶磊
摘要(Abstract):
采用微波无压烧结技术制备了(TiB+TiC)/Ti复合材料。选用石墨粉和TiB_2作为增强相的C源和B源,通过球磨将其附着到Ti基体表面,烧结时与Ti基体发生反应,原位生成TiC和TiB增强相。为了避免红外测温精确度较低的弊端,使用微波功率和烧结时间作为变量,探索制备(TiB+TiC)/Ti复合材料的最佳条件,研究微波烧结工艺对复合材料微观结构和力学性能的影响。结果表明:1 kW功率下烧结27.5 min制备的复合材料力学性能最佳,极限抗压强度为1633 MPa,应变为34.88%,显微硬度为367 HV0.2;随着微波功率的增加,增强相发生粗化,复合材料的力学性能降低。复合材料的断口表面呈现出韧窝和解理面的混合断裂特征。
关键词(KeyWords): 微波无压烧结;微波功率;烧结时间;微观结构;力学性能
基金项目(Foundation): 钒钛资源综合利用国家重点实验室开放基金课题(2021P4FZG10A)
作者(Author): 宋光远,雷鹰,李雨,陶磊
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