变形工艺对纯Mo棒组织和横向弯曲性能的影响Effect of forging process on microstructure and transverse bending properties of pure molybdenum bars
谭望,郭明星,汪明朴,金鹏,曹玲飞,陈畅
摘要(Abstract):
通过弯曲性能测量、金相、SEM以及TEM观察对不同工艺锻造的纯Mo棒横向弯曲性能及组织进行了研究。结果表明:纯Mo棒直接拔长时,随着变形量的增加,其横向塑性变化不大,纵向晶粒逐渐被拉长,当变形量达到96%时,出现明显的纤维组织,断口呈冰糖状。若纯Mo棒在1100℃镦粗50%再拔长到Φ45mm,这样反复进行三次,随后在此温度下从Φ45mm直接拔长到Φ18mm,其横向组织与直接拔长后的相比变化不大,纵向晶粒虽有拉长,但较直接拔长的晶粒长宽比要小,且晶粒不规则程度增加,此锻造工艺仍然不能有效改善其横向塑性。若纯Mo棒在1100℃先镦粗50%再拔长到Φ45mm,反复进行三次后,再将在此温度下从Φ45mm直接拔长到Φ18mm的纯Mo棒镦粗50%后,其横向塑性可得到大幅度提高,弯曲变形量>5%;金相观察表明,其横向晶粒边界变得不很明晰,扭曲程度加重;而纵向晶粒之间晶界相互穿插程度较为严重;其弯曲断口以穿晶断裂为主,断口上有大量的解理面,具有明显的河流状花样和解理台阶;TEM观察表明,其大部分区域以亚晶组织为主,部分区域存在位错胞组织且缠结有大量位错线。
关键词(KeyWords): 纯Mo棒;横向塑性;纤维组织;沿晶断裂;穿晶断裂
基金项目(Foundation): 国家高新技术发展“863”计划资助项目(2002AA302505);; 湖南省自然科学基金(05JJ30095)
作者(Author): 谭望,郭明星,汪明朴,金鹏,曹玲飞,陈畅
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