选区激光熔化制造Inconel 718合金的氢脆行为Hydrogen embrittlement behavior of Inconel 718 alloy prepared by selective laser melting
曾强,吴颖,夏林,朱绍维
摘要(Abstract):
后热处理可以有效改善选区激光熔化(SLM)制造的Inconel 718合金的强塑性匹配,但其氢脆断裂行为目前还尚不明确。为此,对SLM制造的Inconel 718合金进行了高温固溶+单级时效热处理,并采用扫描电镜的电子背散射衍射(EBSD)和背散射电子(BSE)成像对其显微组织进行了分析,通过预充氢前后的拉伸实验对合金的氢脆敏感性进行了评估,并采用EBSD和BSE对拉伸试样的断口表面形貌和裂纹扩展路径进行了分析。结果表明:热处理后,SLM制造的Inconel 718合金的抗拉强度可达1341 MPa,并保持24.5%的断后伸长率,但也具有较高的氢脆敏感性,充氢96 h后合金的强度损伤和塑性损失分别达到18.5%和52.3%。拉伸过程中晶界上由于δ相以及滑移带引起的应力集中促进了晶界上氢的局部富集,从而诱发沿晶氢脆裂纹的萌生及扩展。
关键词(KeyWords): Inconel 718合金;选区激光熔化;氢脆;裂纹扩展路径
基金项目(Foundation): 达州市智能制造产业技术研究院2022年度开放基金项目(ZNZZ2214)
作者(Author): 曾强,吴颖,夏林,朱绍维
DOI: 10.13289/j.issn.1009-6264.2023-0596
参考文献(References):
- [1] Diltemiz S F,Zhang S.Superalloys for Super Jobs[M].Aerospace Materials Handbook,2013.
- [2] 曾强,吴颖,肖辉进,等.油气工程用Inconel 718合金激光焊接头的氢脆行为[J].金属热处理,2020,45(8):50-55.ZENG Qiang,WU Ying,XIAO Hui-jin,et al.Hydrogen embrittlement behavior of oilfield-grade Inconel 718 alloy laser welded joint[J].Heat Treatment of Metals,2020,45(8):50-55.
- [3] 郑凯元,罗耀恩,张屹,等.Inconel 718合金激光直接沉积工艺研究进展[J].激光与光电子学进展,2022,59(23):9-24.ZHENG Kai-yuan,LUO Yao-en,ZHANG Yi,et al.Progress in laser direct deposition of Inconel 718 alloy[J].Laser & Optoelectronics Progress,2022,59(23):9-24.
- [4] 石寅晖,李洁,刘坤,等.铝合金电弧熔丝增材制造的冶金缺陷研究现状与展望[J].材料热处理学报,2023,44(6):1-10.SHI Yin-hui,LI Jie,LIU Kun,et al.Research progress and prospect of metallurgical defects in wire arc additive manufacturing of aluminumalloys[J].Transactions of Materials and Heat Treatment,2023,44(6):1-10.
- [5] Ma X F,Zhai H L,Zuo L,et al.Fatigue short crack propagation behavior of selective laser melted Inconel 718 alloy by in-situ SEM study:Influence of orientation and temperature[J].International Journal of Fatigue,2020,139:105739.
- [6] 杨思瑞,白海清,李超凡,等.镍基高温合金激光熔覆数值模拟及回归正交试验优化[J].激光与光电子学进展,2023,60(5):190-199.YANG Si-rui,BAI Hai-qing,LI Chao-fan,et al.Numerical simulation and regression orthogonal experiment optimization of laser cladding of nickel-based superalloy[J].Laser & Optoelectronics Progress,2023,60(5):190-199.
- [7] Tarzimoghadam Z,Ponge D,Kl?wer J,et al.Hydrogen-assisted failure in Ni-based superalloy 718 studied under in situ hydrogen charging:The role of localized deformation in crack propagation[J].Acta Materialia,2017,128:365-374.
- [8] Tarzimoghadam Z,Rohwerder M,Merzlikin S V,et al.Multi-scale and spatially resolved hydrogen mapping in a Ni-Nb model alloy reveals the role of the δ phase in hydrogen embrittlement of alloy 718[J].Acta Materialia,2016,109:69-81.
- [9] Zhang Z B,Obasi G,Morana R,et al.Hydrogen assisted crack initiation and propagation in a nickel-based superalloy[J].Acta Materialia,2016,113:272-283.
- [10] Ogawa Y,Takakuwa O,Okazaki S,et al.Pronounced transition of crack initiation and propagation modes in the hydrogen-related failure of a Ni-based superalloy 718 under internal and external hydrogen conditions[J].Corrosion Science,2019,161:108186.
- [11] Li X F,Li Q Z,Wang T,et al.Hydrogen-assisted failure of laser melting additive manufactured IN718 superalloy[J].Corrosion Science,2019,160:108171.
- [12] Kevinsanny,Okazaki S,Takakuwa O,et al.Defect tolerance and hydrogen susceptibility of the fatigue limit of an additively manufactured Ni-based superalloy 718[J].International Journal of Fatigue,2020,139:105740.
- [13] Yoo J,Kim S,Jo M C,et al.Investigation of hydrogen embrittlement properties of Ni-based alloy 718 fabricated via laser powder bed fusion[J].International Journal of Hydrogen Energy,2022,47(43):18892-18910.
- [14] Lee D H,Zhao K,Lee S Y,et al.Hydrogen-assisted failure in Inconel 718 fabricated by laser powder bed fusion:The role of solidification substructure in the embrittlement[J].Scripta Materialia,2022,207:114308.
- [15] 唐瑞,刘海定,王东哲,等.油气工程用镍基耐蚀合金718的研究进展[J].金属热处理,2018,43(7):54-59.TANG Rui,LIU Hai-ding,WANG Dong-zhe,et al.Developing progress of oilfield-grade corrosion resistant alloy 718[J].Heat Treatment of Metals,2018,43(7):54-59.
- [16] Han C,Fang Q,Shi Y,et al.Recent advances on high-entropy alloys for 3D printing[J].Advanced Materials,2020,32(26):1903855.
- [17] Li X,Shi J J,Wang C H,et al.Effect of heat treatment on microstructure evolution of Inconel 718 alloy fabricated by selective laser melting[J].Journal of Alloys and Compounds,2018,764:639-649.
- [18] Deng D Y,Peng R L,Brodin H,et al.Microstructure and mechanical properties of Inconel 718 produced by selective laser melting:Sample orientation dependence and effects of post heat treatments[J].Materials Science and Engineering A,2018,713:294-306.
- [19] Cao G H,Sun T Y,Wang C H,et al.Investigations of γ′,γ″ and δ precipitates in heat-treated Inconel 718 alloy fabricated by selective laser melting[J].Materials Characterization,2018,136:398-406.
- [20] Zhao Y N,Guo Q Y,Ma Z Q,et al.Comparative study on the microstructure evolution of selective laser melted and wrought IN718 superalloy during subsequent heat treatment process and its effect on mechanical properties[J].Materials Science and Engineering A,2020,791:139735.
- [21] Martin M,Dadfarnia M,Nagao A,et al.Enumeration of the hydrogen-enhanced localized plasticity mechanism for hydrogen embrittlement in structural materials[J].Acta Materialia,2019,165:734-750.
- [22] Troiano A R.The role of hydrogen and other interstitials in the mechanical behavior of metals[J].Metallography,Microstructure,and Analysis,2016,5(6):557-569.
- [23] Nagumo M,Takai K.The predominant role of strain-induced vacancies in hydrogen embrittlement of steels:Overview[J].Acta Materialia,2019,165:722-733.
- [24] Lin Y C,McCarroll I E,Lin Y T,et al.Hydrogen trapping and desorption of dual precipitates in tempered low-carbon martensitic steel[J].Acta Materialia,2020,196:516-527.
- [25] Obasi G C,Zhang Z,Sampath D,et al.Effect of microstructure and alloy chemistry on hydrogen embrittlement of precipitation-hardened Ni-based alloys[J].Metallurgical and Materials Transactions A,2018,49(4):1167-1181.
- [26] Tehranchi A,Zhou X,Curtin W A.A decohesion pathway for hydrogen embrittlement in nickel:Mechanism and quantitative prediction[J].Acta Materialia,2020,185:98-109.
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