粉末注射成形无镍高氮不锈钢工艺Powder injection molding of nickel-free high nitrogen stainless steel
崔大伟,曲选辉
摘要(Abstract):
采用粉末注射成形工艺制备了无镍高氮奥氏体不锈钢(0Cr17Mn11Mo3N),研究了喂料的流变行为,注射工艺及烧结工艺。结果表明:64 vol%气雾化0Cr17Mn11Mo3粉末与适量的粘结剂(65 wt%石蜡+30 wt%高密度聚乙烯+5 wt%硬脂酸)混合后的喂料具有较好的流变性能;最佳注射工艺参数为注射压力75~95 MPa,相应的注射温度为160~170℃;提高烧结温度有利于提高烧结体的密度,但是对提高氮含量不利,而增加烧结氮气氛压力可以获得较高的氮含量,但是不利于提高烧结体密度,最佳的烧结工艺为0.1 MPa氮气压力下1300℃烧结2 h,此时烧结体相对密度可以达到99%,氮含量可达到0.78%。
关键词(KeyWords): 高氮;无镍;粉末注射成形;奥氏体不锈钢
基金项目(Foundation): 国家自然科学基金重点项目(50634010);; 国家“863”计划项目(2006AA032502)
作者(Author): 崔大伟,曲选辉
DOI: 10.13289/j.issn.1009-6264.2010.07.028
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