Mg-8Gd-(0,3)Sm-0.5Zr合金的动态再结晶生长动力学Dynamic recrystallization growth kinetics of Mg-8Gd-(0,3)Sm-0.5Zr alloys
朱利敏,李全安,陈晓亚,张清
摘要(Abstract):
利用铸造法制备了Mg-8Gd-(0,3)Sm-0.5Zr合金,并进行了525℃均匀化处理8 h,随后在温度为350~500℃及应变速率为0.002~1 s~(-1)的条件下进行热压缩试验,绘制并分析合金热压缩后的真应力-真应变曲线,构建其动态再结晶生长动力学双参数模型,并分析了合金生长动力学曲线特点及显微组织特征。结果表明:两种合金在热压缩时均发生了动态再结晶,通过双参数模型绘制动态再结晶动力学曲线,发现在高温低应变速率热压缩时,在真应变约0.2时,合金的动态再结晶的体积分数迅速增加至90%以上。对比分析Sm元素添加后的动态再结晶动力学曲线,发现Sm元素促进动态再结晶的进行,尤其在高温低应变速率热压缩时,在变形初期Sm的促进作用更明显。
关键词(KeyWords): Mg-8Gd-(0,3)Sm-0.5Zr合金;热压缩;动态再结晶
基金项目(Foundation): 国家自然科学基金(51571084);; 河南省自然科学基金面上项目(222300420435)
作者(Author): 朱利敏,李全安,陈晓亚,张清
DOI: 10.13289/j.issn.1009-6264.2023-0216
参考文献(References):
- [1] Muzyk M,Pakiela Z,Kurzydlowski K J.Generalized stacking fault energy in magnesium alloys:density functional theory calculations[J].Scripta Materialia,2012,66(5):219-222.
- [2] 刘丹丹,郭学峰,杨文朋.热挤压对15%Mg-2Si/Al-Si-Cu复合材料组织及性能的影响[J].材料热处理学报,2021,42(4):17-24.LIU Dan-dan,GUO Xue-feng,YANG Wen-peng.Effect of hot extrusion on microstructure and properties of 15%Mg-2Si/Al-Si-Cu composites[J].Transactions of Materials and Heat Treatment,2021,42(4):17-24.
- [3] 徐文良,李成杰,李学问.挤压温度对纯镁组织演变、力学性能和断裂行为的影响[J].材料热处理学报,2021,42(4):48-53.XU Wen-liang,LI Cheng-jie,LI Xue-wen.Effect of extrusion temperature on microstructure evolution,mechanical properties and fracture behavior of pure magnesium[J].Transactions of Materials and Heat Treatment,2021,42(4):48-53.
- [4] 张亚,马春江,卢晨.变形镁合金的塑性变形机制与动态再结晶[J].轻合金加工技术,2003,31(7):35-39.ZHANG Ya,MA Chun-jiang,LU Chen.Plastic strain mechanism and dynamic recrystallization (DRX) of magnesium alloy[J].Light Alloy Fabrication Technology,2003,31(7):35-39.
- [5] Yan X,Hu L X,Sun Y.Dynamic recrystallization kinetics of as-cast AZ91D alloy[J].Transactions of Nonferrous Metals Society of China,2014,24(6):1683-1689.
- [6] Quan Z Q,Shi Y,Wang Y X,et al.Constitutive modeling for the dynamic recrystallization evolution of AZ80 magnesium alloy based on stress-strain data[J].Materials Science and Engineering A,2011,528(28):8051-8059.
- [7] Wang Z T,Jiang J H,Liu X N,et al.Dynamics and kinematics models of dynamic recrystallization of AZ80 magnesium alloy during thermal deformation[J].Rare Metal Materials and Engineering,2019,48(7):2062-2067.
- [8] 朱利敏,李全安,陈晓亚,等.Mg-8Gd-0.5Zr合金热压缩过程中动态再结晶行为[J].材料导报,2019,33(12):4117-4121.ZHU Li-min,LI Quan-an,CHEN Xiao-ya,et al.Dynamic recrystallization behavior of Mg-8Gd-0.5Zr alloy during hot compression deformation[J].Materials Reports,2019,33(12):4117-4121.
- [9] Robson J D,Henry D T,Davis B.Particle effects on recrystallization in magnesium manganese alloys:Particle-stimulated nucleation[J].Acta Materialia,2009,57(9):2739-2747.
- [10] Vaughan M W,Nasim W,Dogan E,et al.Interplay between the effects of deformation mechanisms and dynamic recrystallization on the failure of Mg-3Al-1Zn[J].Acta Materialia,2019,168:448-472.
- [11] Lee J H,Lee J U,Kim S H,et al.Dynamic recrystallization behavior and microstructural evolution of Mg alloy AZ31 through high-speed rolling[J].Journal of Materials Science and Technology,2018,34(10):1747-1755.
- [12] Zou J K,Chen J H,Yan H G,et al.Effects of Sn addition on dynamic recrystallization of Mg-5Zn-1Mn alloy during high strain rate deformation[J].Materials Science and Engineering A,2018,735:49-60.
- [13] Yu J M,Zhang Z M,Xu P,et al.Dynamic recrystallization behavior of Gd-containing Mg alloy under torsion deformation[J].Journal of Alloys and Compounds,2019,787:239-253.
- [14] Lv B J,Peng J,Wang Y J,et al.Dynamic recrystallization behavior and hot workability of Mg-2.0Zn-0.3Zr-0.9Y alloy by using hot compression test[J].Materials and Design,2014,53(1):357-365.
- [15] Zhao D Q,Yang Y S,Zhou J X,et al.Constitutive modeling for dynamic recrystallization kinetics of Mg-4Zn-2Al-2Sn alloy[J].Transactions of Nonferrous Metals Society of China,2018,28(2):340-347.
- [16] Liu J,Cui Z,Ruan L.A new kinetics model of dynamic recrystallization for magnesium alloy AZ31B[J].Materials Science and Engineering A,2011,529:300-310.
- [17] Sellars C M,Whiteman J A.Recrystallization and grain growth in hot rolling[J].Metal Science,1979,13 (3/4):187-194.
- [18] Chen M S,Lin Y C,Ma X S.The kinetics of dynamic recrystallization of 42CrMo steel[J].Materials Science and Engineering A,2012,556:260-266.
- [19] Zeng J,Wang F,Dong S,et al.A new dynamic recrystallization kinetics model of cast-homogenized magnesium alloys[J].Metallurgical and Materials Transactions A,2021,52:316-331.
- [20] Kim S I,Yoo Y C.Dynamic recrystallization behavior of AISI 304 stainless steel[J].Materials Science and Engineering A,2001,311(1/2):108-113.
- [21] Laasraoui A,Jonas J J.Prediction of steel flow stresses at high temperatures and strain rates[J].Metallurgical Transactions A,1991,22(7):1545-1558.
- [22] Serajzadeh S,Karimi Taheri A.Prediction of flow stress at hot working condition[J].Mechanics Research Communications,2003,30(1):87-93.
- [23] 李凡波,周海涛,秦径为,等.AZ81镁合金流变应力预测及动态再结晶动力学[J].塑性工程学报,2016,23(1):104-111.LI Fan-bo,ZHOU Hai-tao,QIN Jing-wei,et al.Flow stress prediction and dynamic recrystallzation kinetics of AZ80 magnesium alloy[J].Journal of Plasticity Engineering,2016,23(1):104-111.
- [24] Li H Z,Wang H J,Li Z,et al.Flow behavior and processing map of as-cast Mg-10Gd-4.8Y-2Zn-0.6Zr alloy[J].Materials Science and Engineering A,2010,528 (1):154-160.
- [25] Zhu L M,Li Q A,Chen X Y,et al.Effect of Sm on dynamic recrystallization of Mg-8Gd-0.5Zr alloy during hot compression[J].Journal of Alloys and Compounds,2021,865:158648.
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