增材制造GH4099合金焊接接头强化相析出行为及其对接头力学性能的影响Precipitation behavior of strengthening phases in welded joints of additive manufactured GH4099 alloy and its influence on mechanical properties of joints
吴昌毅,舒登威,商文学,郭乾应
摘要(Abstract):
首先采用激光选区熔化(SLM)技术制备了GH4099合金,并对其进行了不同工艺的激光焊接及焊后时效处理,研究了焊接热输入与焊后时效处理对接头微观组织和力学性能的影响,分析了接头焊缝和热影响区中的强化相析出行为与硬度的变化规律。结果表明:采用激光焊接SLM GH4099合金可得到成型良好,无可视宏观缺陷,仅存在极少量微观缺陷的焊接接头;焊接接头中γ′相的平均尺寸随焊后时效处理的进行而逐渐增大,导致显微硬度增加,时效2 h后γ′相粗化速度和显微硬度提升程度放缓,时效10 h后,焊缝中的γ′相尺寸从0~10 nm增大到20~30 nm,热影响区中的γ′相呈现双峰分布特征,由小尺寸γ′相为主导转变为大尺寸γ′相为主导,同时焊缝和热影响区显微硬度均从时效前的约200 HV提升至约400 HV;焊接热输入会影响焊接接头在后续时效过程中的γ′相析出行为及力学性能,时效过程中低热输入样品的接头具有更快的γ′相长大速率;时效2和10 h后,低热输入样品的接头焊缝/热影响区均具有更大的γ′相尺寸,并且显微硬度均高于高热输入的接头。
关键词(KeyWords): GH4099高温合金;激光焊接;γ′相;力学性能
基金项目(Foundation): 国家高层次青年人才项目
作者(Author): 吴昌毅,舒登威,商文学,郭乾应
DOI: 10.13289/j.issn.1009-6264.2025-0389
参考文献(References):
- [1] Zhang L X,Shi J M,Li H W,et al.Interfacial microstructure and mechanical properties of ZrB2-SiC-C ceramic and GH99 superalloy joints brazed with a Ti-modified FeCoNiCrCu high-entropy alloy[J].Materials & Design,2016,97:230-238.
- [2] Li H,Wei H,He P,et al.Effects of alloying elements in GH99 superalloy on microstructure evolution of reactive brazing TiAl/GH99 joints[J].Intermetallics,2013,34:69-74.
- [3] Tian X Y,Feng J C,Shi J M,et al.Brazing of ZrB2-SiC-C ceramic and GH99 superalloy to form reticular seam with low residual stress[J].Ceramics International,2015,41(1):145-153.
- [4] Tan C,Weng F,Sui S,et al.Progress and perspectives in laser additive manufacturing of key aeroengine materials[J].International Journal of Machine Tools and Manufacture,2021,170:103804.
- [5] Thomas M,Baxter G J,Todd I.Normalised model-based processing diagrams for additive layer manufacture of engineering alloys[J].Acta Materialia,2016,108:26-35.
- [6] Hu Y L,Lin X,Li Y L,et al.Effect of heat treatment on the microstructural evolution and mechanical properties of GH4099 additive-manufactured by directed energy deposition[J].Journal of Alloys and Compounds,2019,800:163-173.
- [7] Yap C Y,Chua C K,Dong Z L,et al.Review of selective laser melting:Materials and applications[J].Applied Physics Reviews,2015,2(4).
- [8] Hu L,Huang J,Liu C,et al.Effects of coupling between the laser plasma and two arcs on metal transfer in CO2 laser double-wire MIG hybrid welding[J].Optics & Laser Technology,2018,105:152-161.
- [9] Yang H,Tao X,Ba X,et al.Study on coupling characteristics of different welding modes in laser-double TIG hybrid welding[J].Optics & Laser Technology,2023,167:109621.
- [10] Dal M,Fabbro R.An overview of the state of art in laser welding simulation[J].Optics & Laser Technology,2016,78:2-14.
- [11] Ramkumar K D,Dev S,Prabhakar K V P,et al.Microstructure and properties of Inconel 718 and AISI 416 laser welded joints[J].Journal of Materials Processing Technology,2019,266:52-62.
- [12] Taheri M,Razavi M,Kashani-Bozorg S F,et al.Relationship between solidification and liquation cracks in the joining of GTD-111 nickel-based superalloy by Nd:YAG pulsed-laser welding[J].Journal of Materials Research and Technology,2021,15:5635-5649.
- [13] 赵亚楠,郭乾应,刘晨曦,等.后续热处理对激光 3D 打印 GH4099 合金微观组织和高温力学性能的影响[J].金属学报,2024,61(1):165-176.ZHAO Ya-nan,GUO Qian-ying,LIU Chen-xi,et al.Effects of subsequent heat treatment on microstructure and high-temperature mechanical properties of laser 3D printed GH4099 alloy[J].Acta Metallurgica Sinica,2024,61(1):165-176.
- [14] Harte A,Atkinson M,Smith A,et al.The effect of solid solution and gamma prime on the deformation modes in Ni-based superalloys[J].Acta Materialia,2020,194:257-275.
- [15] Li J,Ding R,Guo Q,et al.Effect of solution cooling rate on microstructure evolution and mechanical properties of Ni-based superalloy ATI 718Plus[J].Materials Science and Engineering A,2021,812:141113.
- [16] Nie Z,Guo Q,Chai J,et al.Initial γ′ phase formation mechanism in a GH4099 precipitation strengthened nickel-based superalloy[J].Scripta Materialia,2025,264:116702.
- [17] Chang K,Ma L,Li P,et al.Effect of heat treatment on microstructure and mechanical properties of GH4099 superalloy fabricated by selective laser melting[J].Journal of Alloys and Compounds,2023,934:167813.
- [18] Zhang Z,Zhao Y,Shan J,et al.The role of shot peening on liquation cracking in laser cladding of K447A nickel superalloy powders over its non-weldable cast structure[J].Materials Science and Engineering A,2021,823:141678.
- [19] Zhang Z,Zhao Y,Shan J,et al.Evolution behavior of liquid film in the heat-affected zone of laser cladding non-weldable nickel-based superalloy[J].Journal of Alloys and Compounds,2021,863:158463.
- [20] 程昊,周炼刚,刘健,等.热输入对Inconel 617镍基高温合金激光焊接接头显微组织与力学性能的影响[J].材料工程,2023,51(1):113-121.CHENG Hao,ZHOU Lian-gang,LIU Jian,et al.Effect of heat input on microstructure and mechanical properties of laser welded joint of Inconel 617 nickel-based superalloy[J].Journal of Materials Engineering,2023,51(1):113-121.
- [21] Naseri H,Sadrossadat S M,Hajjari E.Investigation of the effect of preweld heat treatment on the liquation cracking of GTD-111 superalloy[J].Materials Transactions,2020,61(5):903-908.
- [22] Taheri M,Halvaee A,Kashani-Bozorg S F.Effect of pre-and post-weld heat treatment on microstructure and mechanical properties of GTD-111 superalloy welds[J].Metals and Materials International,2021,27(5):1173-1192.
- [23] Xie J,Ma Y,Xing W,et al.Microstructure and mechanical properties of a new cast nickel-based superalloy K4750 joint produced by gas tungsten arc welding process[J].Journal of Materials Science,2019,54(4):3558-3571.
- [24] Li Z,Zhang Z,Zhang M,et al.Microstructure and mechanical properties of laser welded and post-weld heat-treated K439B superalloy[J].Transactions of Nonferrous Metals Society of China,2024,34(3):905-917.
- [25] Shim D S,Baek G Y,Seo J S,et al.Effect of layer thickness setting on deposition characteristics in direct energy deposition (DED) process[J].Optics & Laser Technology,2016,86:69-78.
- [26] Acharya R,Das S.Additive manufacturing of IN100 superalloy through scanning laser epitaxy for turbine engine hot-section component repair:process development,modeling,microstructural characterization,and process control[J].Metallurgical and Materials Transactions A,2015,46(9):3864-3875.
- [27] Mashhuriazar A,Omidvar H,Sajuri Z,et al.Effects of pre-weld heat treatment and heat input on metallurgical and mechanical behaviour in HAZ of multi-pass welded IN-939 superalloy[J].Metals,2020,10(11):1453.
- [28] Hu X A,Xue Z Y,Zhao G L,et al.Laser welding of a selective laser melted Ni-base superalloy:microstructure and high temperature mechanical property[J].Materials Science and Engineering A,2019,745:335-345.
- [29] Rezaei M A,Naffakh-Moosavy H.The effect of pre-cold treatment on microstructure,weldability and mechanical properties in laser welding of superalloys[J].Journal of Manufacturing Processes,2018,34:339-348.
- [30] Yan F,Liu S,Hu C,et al.Liquation cracking behavior and control in the heat affected zone of GH909 alloy during Nd:YAG laser welding[J].Journal of Materials Processing Technology,2017,244:44-50.
- [31] Ojo O A,Richards N L,Chaturvedi M C.Microstructural study of weld fusion zone of TIG welded IN 738LC nickel-based superalloy[J].Scripta Materialia,2004,51(7):683-688.
- [32] Zhang J,Xin W,Ge Z,et al.Effect of high heat input welding on the microstructures,precipitates and mechanical properties in the simulated coarse grained heat affected zone of a low carbon Nb-V-Ti-N microalloyed steel[J].Materials Characterization,2023,199:112849.
- [33] Nie Z,Guo Q,Zhao Y,et al.Temperature dependence tensile behaviors of additively manufactured GH4099 Ni-based superalloy[J].Materials Science and Engineering A,2024,899:146464.
- [34] Cai Z,Li Z,Jiang F,et al.Influence of different heat treatment methods on the microstructure and high-temperature hardness of GH4099 superalloy fabricated by selective laser melting[J].Journal of Alloys and Compounds,2025,1039:183186.
- [35] Tan Y,You X,You Q,et al.Microstructure and deformation behavior of nickel based superalloy Inconel 740 prepared by electron beam smelting[J].Materials Characterization,2016,114:267-276.
- [36] Wang Z,Muránsky O,Zhu H,et al.On the kinetics of gamma prime (γ′) precipitation and its strengthening mechanism in Alloy 617 during a long-term thermal aging[J].Materialia,2020,11:100682.
- [37] Wen Y H,Simmons J P,Shen C,et al.Phase-field modeling of bimodal particle size distributions during continuous cooling[J].Acta Materialia,2003,51(4):1123-1132.
- [38] Lifshitz I M,Slyozov V V.The kinetics of precipitation from supersaturated solid solutions[J].Journal of Physics and Chemistry of Solids,1961,19(1/2):35-50.
- [39] Nie Y,Tang Q,Li Z,et al.Laser powder bed fusion of GH4099 superalloy:Parameter optimization and effect of heat treatment on microstructure and mechanical properties[J].Additive Manufacturing Frontiers,2024,3(2):200133.
- [40] Zhao X,Dang Y,Yin H,et al.Evolution of the microstructure and microhardness of a new wrought Ni-Fe based superalloy during high temperature aging[J].Journal of Alloys and Compounds,2015,644:66-70.
- [41] Xu Y,Li W,Yang X,et al.Evolution of grain structure,γ′precipitate and hardness in friction welding and post weld heat treatment of a new Ni-Fe based superalloy[J].Materials Science and Engineering A,2020,788:139596.
- [42] He H,Liao J,Xuan Y,et al.Precipitation behavior of γ′ phase with a multi-model morphology in the Ni-based superalloy GH4720Li during water quenching and subsequent artificial aging and related mechanisms[J].Materials Chemistry and Physics,2024,318:129214.
文章评论(Comment):
|
||||||||||||||||||
|
||||||||||||||||||