电石渣热处理条件对合成超轻硬硅钙石的影响Influence of heat-treatment of carbide slag on preparation of ultra-light xonotlite
刘飞,曾令可,曹建新,林倩,张煜
摘要(Abstract):
采用DTA/TG研究了电石渣的热处理性能,采用XRD及SEM等检测手段,研究了经不同温度煅烧后电石渣的矿物组成、形貌以及热处理条件对石灰活性及合成硬硅钙石的影响。结果表明,电石渣经适当煅烧处理后可以作为钙质原料制备超轻硬硅钙石。不同电石渣煅烧温度对合成产物的晶相组成没有影响,但对石灰活性及合成产物的微观形貌有较大的影响。700、800℃煅烧电石渣制备的石灰乳活性大,合成得到的硬硅钙石粒子球形度完整;而900、1000℃煅烧电石渣制备的石灰乳活性小,合成得到的硬硅钙石球形粒子直径小,且倾向于紧密团聚。
关键词(KeyWords): 电石渣;石灰活性;超轻硬硅钙石;煅烧温度
基金项目(Foundation): 国家自然科学基金(50676033);; 贵州省科技攻关项目(黔科合GY字[2006]3030);; 贵阳市科学技术计划项目([2006]筑科工合同字第16-9号)
作者(Author): 刘飞,曾令可,曹建新,林倩,张煜
参考文献(References):
- [1]Yanagisawa K,Feng Q,Yamasaki N.Hydrothermal synthesis of xonotltie whiskers byion diffusion[J].Journal of Materials Science Letters,1997,16:889-891.
- [2]Yasuo A,Tamotsu Y,Shigeki A,et al.Crystal shape and size control of xonotlite[J].Inorg Mater Japan(Gypsum&Lime),1994,248:17-25.
- [3]陈淑祥,倪文,江翰,等.超轻硬硅钙石型硅酸钙绝热材料制备技术国内外研究现状[J].新型建筑材料,2004,(1):53-55.CHENShu-xiang,NI Wen,JIANG Han,et al.Present research situation ontechnology of extra light hard okenite thermal insulation materials at home andabroad[J].NewBuilding Materials,2004,(1):53-55.
- [4]Kazuo S,Kazuhiko K,Akira T.Effect of silica raw material onthe textures of synthesized xonotlite[J].Gypsum&Lime,1986,202:36-42.
- [5]Yasuo A,Tamotsu Y,Shigeti A,et al.Effect of additive on crystal shape and control of xonotlite[J].Inorganic Material,1995,258:310-319.
- [6]毛仲佳,盛建新.超轻型硅酸钙保温材料的研究[J].硅酸盐通报,1997,(1):50-54.MAOZhong-jia,SHENGJian-xin.Research on superlight calciumsilicate insulation[J].Bulletin of the Chinese Ceramic Society,1997,(1):50-54.
- [7]黄存捍,邓寅生,刑学玲.电石渣的综合利用途径探讨[J].焦作工学院学报(自然科学版),2004,23(2):143-146.HUANG Cun-han,DENG Yin-sheng,XING Xue-ling.Comprehensive ultilization of carbide slag[J].Journal of Jiaozuo Institute of Technology(NaturalScience),2004,23(2):143-146.
- [8]张友坤,康朝晖,李晓,等.电石渣的处理及回收利用[J].聚氯乙稀,2001,(1):52-54.ZHANG You-kun,KANGZhao-hui,LI Xiao,et al.The treatment and reutilization of carbide slag[J].Polyvinyl Chloride,2001,(1):52-54.
- [9]久保田和雄,高桥正英,片平善晴,等.ゾノトラィト系成型体[P].特开昭,60-204655,1985.
- [10]王文波,倪文,肖晋宜.原料活性匹配对制备超轻硬硅钙石制品的影响[J].非金属矿,2006,29(1):30-31.WANG Wen-bo,NI Wen,XIAOJin-yi.Influence of activity match of rawmaterials on preparation of super-light Xonotlite[J].Non-metallic Mines,2006,29(1):30-31.
- [11]李懋强,陈玉峰,夏淑琴,等.超轻微孔硅酸钙绝热材料的显微结构和工艺控制[J].硅酸盐学报,2000,28(5):401-406.LI Mao-qiang,CHENYu-feng,XIA Shu-qin,et al.Microstructure and processing of ultra-light calciumsilicate insulation material[J].Journal of theChinese Ceramic Society,2000,28(5):401-406.
- [12]王贞尧,吴梅梅,黄毓敏,等.石灰活性对中空硬硅钙石二次粒子球形貌的影响[J].耐火材料,1997,31(4):205-207.WANGZhen-yao,WU Mei-mei,HUANG Yu-min,et al.Effect of lime activity on the hollowsecondary particles of xonotlite[J].Refractories,1997,31(4):205-207.
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