纳米ZrO2含量对Ni/ZrO2刷镀层组织和硬度的影响Effect of content of nano-ZrO2 on microstructure and micro-hardness of Ni-ZrO2 composite coatings prepared with electro-brush plating
袁庆龙,凌文丹,李平,王海瑞
摘要(Abstract):
采用电刷镀技术制备了Ni/ZrO2纳米复合刷镀层,对镀层的表面组织结构、显微硬度进行了观察、测定和分析。结果表明:当镀液中纳米ZrO2颗粒含量为20 g/L时,复合镀层的形貌最为平整致密,晶粒最为细小,硬度达到峰值(581.4 HV);随着热处理温度的升高,Ni/ZrO2纳米复合镀层的显微硬度呈现先升高后下降的趋势,在250℃时达到极大值(688.9 HV),表现出较好的耐高温软化性能。
关键词(KeyWords): 电刷镀;Ni/ZrO2复合镀层;表面形貌;显微硬度
基金项目(Foundation): 河南省科技计划项目(102102210210)
作者(Author): 袁庆龙,凌文丹,李平,王海瑞
DOI: 10.13289/j.issn.1009-6264.2013.06.029
参考文献(References):
- [1]伍光凤,李晖,罗静.提高塑料模具使用寿命的表面处理技术[J].热加工工艺,2004(6):56-59.WU Guang-feng,LI Hui,LUO Jing.Technology of surface treating for prolonging plastic moulds service life[J].Hot Working Technology,2004(6):56-59.
- [2]常明,张庆茂,廖健宏,等.塑料模具精密修复技术的评述及展望[J].金属热处理,2006,31(7):1-5.CHANG Ming,ZHANG Qing-mao,LIAO Jian-hong,et al.Comments and prospects of the precise repairing technology of plastic moulds[J].HeatTreatment of Metal,2006,31(7):1-5.
- [3]张茁.塑料模具用不锈钢[J].现代制造,2002(7):84-84.ZHANG Zhuo.Stainless steel for plastic mold[J].Maschinen Markt,2002(7):84-84.
- [4]Straffrd K N,Subramanian C.Surface engineering:an enabling technology for manufacturing industry[J].Journal of Materials Processing Technology,1995,53(8):393-403.
- [5]徐江,卓城之,韩德忠,等.纳米颗粒增强Ni基复合镀渗层的腐蚀与冲蚀性能研究[J].稀有金属材料与工程,2010,39(2):318-324.XU Jiang,ZHUO Cheng-zhi,HAN De-zhong,et al.Microstructure,corrosion and erosion-corrosion properties of Ni based composite alloying layer[J].Rear Metal Materials and Engineering,2010,39(2):318-324.
- [6]Saeed Reza Allahkaram,Setareh Golroh,Morteza Mohammadalipour.Properties of Al2O3 nano-particle reinforced copper matrix composite coatingsprepared by pulse and direct current electroplating[J].Materials&Design,2011,32(8):4478-4484.
- [7]掲晓华,程秀,卢国辉,等.Ni-P-SiC(纳米)复合镀层的滑动磨损特性[J].金属热处理,2007,32(4):51-53.JIE Xiao-hua,CHENG Xiu,LU Guo-hui,et al.Solid wear behavior of Ni-P-SiC(nano)composite coatings[J].Heat Treatment of Metals,2007,32(4):51-53.
- [8]王伟,钱士强,周细应,等.高速电喷镀纳米ZrO2/Ni复合层组织及高温氧化性能[J].材料热处理学报,2009,30(5):192-195.WANG Wei,QIAN Shi-qiang,ZHOU Xi-ying,et al.Microstructure and high temperature oxidation resistance of nano-ZrO2/Ni composite coatingsprepared by high speed jet electroplating[J].Transactions of Materials and Heat Treatment,2009,30(5):192-195.
- [9]高蕊.微粉复合电刷镀工艺与镀层性能的研究[D].天津:天津大学,2008.
- [10]吴蒙华,傅欣欣,李智,等.超声电沉积镍/纳米碳化硅复合镀层组织结构研究[J].机械工程材料,2004,28(12):46-48.WU Meng-hua,FU Xin-xin,LI Zhi,et al.Microstructure of ultrasonic-electrodepositing Ni/nano-SiC composite coatings[J].Materials for MechanicalEngineering,2004,28(12):46-48.
- [11]薛玉君,朱狄,靳广虎,等.电沉积Ni-La2O3纳米复合镀层的摩擦磨损性能[J].摩擦学学报,2005,25(1):1-4.XUE Yu-jun,ZHU Di,JIN Guang-hu,et al.Friction and wear properties of electrodeposited Ni-La2O3 nanocomposite coatings[J].Tribology,2005,25(1):1-4.
- [12]陈丽君,邢忠月,史海生.快速镍电刷镀层的分析[J].上海钢研,1990(4):67-69.CHEN Li-jun,XING Zhong-yue,SHI Hai-sheng.The selective plating Ni-layers analysis[J].Steel Research of Shanghai,1990(4):67-69.
- [13]卢柯.金属纳米晶体的界面热力学特性[J].物理学报,1995,44(9):1454-1460.LU Ke.Thermondynamic properties of interfaces in nanocrystalline metals[J].Acta Physica Sinica,1995,44(9):1454-1460.
- [14]Meng Q,Zhou N,Rong Y.Size effect on the Fe nanocrystalline phase transformation[J].Acta Mater,2002,50(18):4563-4570.
- [15]徐龙堂.电刷镀镍基含纳米粉复合镀层性能、结构和共沉积机理[D].北京:北京工业大学,2002,4-16.
- [16]张文峰,付珺.热处理对Ni-ZrO2复合电铸层显微硬度的影响[J].铸造,2009,58(5):436-439.ZHANG Wen-feng,FU Jun.Effect of heat treatment on micro-hardness of Ni-ZrO2 nano-composite electroforming deposits[J].Foundry,2009,58(5):436-439.
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