奚小波,缪宏,王洪亮,张瑞宏,张剑峰,王红军

• 1:扬州大学机械工程学院
• 2:南京工业职业技术学院

摘要(Abstract)：

通过高温封接工艺制备了双银Low-e真空平板玻璃,采用场发射扫描电镜观察不同封接温度下的试样膜层表面及断面微观形貌,并利用纳米压痕仪测试各试样力学性能以及各试样的临界载荷。结果表明,适当的封接温度可提高Low-e膜层的致密度,优化双银Low-e膜层的弹性模量、纳米硬度及膜层与玻璃基的结合性能,480℃下膜层的弹性模量、纳米硬度及临界载荷的综合性能较好;随封接温度升高,膜层的蠕变应力指数增大,超过500℃,该值增幅增大。

关键词(KeyWords)： 真空平板玻璃;双银Low-e膜;力学性能;纳米压痕;纳米划痕

Abstract:

Keywords:

基金项目(Foundation): 国家科学自然基金(51172199,51372216);; 国家青年科学基金(51302242);; 江苏省自然科学基金(BK2012530);; 江苏省农机三新工程项目(NJ2013-15);; 扬州市建设科技计划项目(2012BAD32B11)

作者(Author): 奚小波,缪宏,王洪亮,张瑞宏,张剑峰,王红军

DOI: 10.13289/j.issn.1009-6264.2014.09.034

参考文献(References)：

• [1]缪宏,张瑞宏,左敦稳,等.支撑柱对真空平板玻璃静态特性的影响[J].建筑材料学报,2013,16(1):153-158.MIAO Hong,ZHANG Rui-hong,ZUO Dun-wen,et al.Effect of shore on static characteristics of vacuum plate glass[J].Journal of Building Materials,2013,16(1):153-158.
• [2]缪宏,奚小波,张瑞宏,等.真空平板玻璃风载荷数值分析与试验研究[J].太阳能学报,2013,34(11):1888-1894.MIAO Hong,XI Xiao-bo,ZHANG Rui-hong,et al.Numerical calculation and experimental research on wind load of vacuum plate glass[J].Acta Energiae Solaris Sinica,2013,34(11):1888-1894.
• [3]刘甜甜,许海凤,韩翠林,等.真空玻璃研发和产业化动态[J].硅酸盐通报,2013,32(2):268-273.LIU Tian-tian,XU Hai-feng,HAN Cui-lin,et al.Research and industrialization development of vacuum glazing[J].Bulletin of the Chinese Ceramic Society,2013,32(2):268-273.
• [4]缪宏,左敦稳,张瑞宏,等.MATLAB的真空平板玻璃支撑柱应力数值分析[J].重庆建筑大学学报,2008,30(6):56-60.MIAO Hong,ZUO Dun-wen,ZHANG Rui-hong,et al.A matlab-based numerical simulation analysis of shore stress in vacuum plate glass[J].Journal of Chongqing Jianzhu University,2008,30(6):56-60.
• [5]缪宏,左敦稳,张瑞宏,等.大气压下真空平板玻璃的支撑应力[J].建筑材料学报,2008,11(6):757-761.MIAO Hong,ZUO Dun-wen,ZHANG Rui-hong,et al.Study of shore stress of vacuum plate glazing at the atmospheric pressure[J].Journal of Building Materials,2008,11(6):757-761.
• [6]周家斌,任毅,付志强,等.低辐射镀膜玻璃的研究开发进展[J].建筑结构学报,2007,28(4):104-108.ZHOU Jia-bin,REN Yi,FU Zhi-qiang,et al.Review of the research and development of low emissivity coating glass[J].Journal of Building Structures,2007,28(4):104-108.
• [7]Tao D Q,Zhang R H,Wan H L.The high-temperature sealing research of vacuum flat glass[J].Advanced Materials Research,2013,807-809:2688-2692.
• [8]张瑞宏.真空平板玻璃传热性能及支撑应力研究[D].北京:中国农业大学,2005.ZHANG Rui-hong.Research on vacuum plate glass's performance of heat transfer and its stress caused by supporting[D].Beijing:China Agricultural University,2005.
• [9]Turner G M,Collins R E.Measurement of heat flow through vacuum glazing at elevated temperature[J].International Journal of Heat and Mass Transfer,1997,40(6):1437-1446.
• [10]Collins R E,Turner G M,Fischer-Cripps A C,et al.Vacuum glazing-a new component for insulating windows[J].Building and Environment,1995,30(4):459-492.
• [11]孙敢.真空玻璃激光焊接的成型研究[D].扬州:扬州大学,2012.SUN Gan.Research on vacuum plate glass's forming by laser bonding[D].Yangzhou,Yangzhou University,2012.
• [12]Synowicki R A,Johs B D,Martin A C.Optical properties of soda-lime float glass from spectroscopic ellipsometry[J].Thin Solid Films,2011,519(9):2907-2913.
• [13]Hao X H,Ju Y L,Lu Y J.Experimental study on the sealing clearance between the labyrinth sealing displacer and cylinder in the10K G-M refrigerator[J].Cryogenics,2011,51(5):203-208.
• [14]缪宏,左敦稳,王珉,等.热处理对Q460钢冷挤压内螺纹表层组织与性能的影响[J].材料热处理学报,2012,33(3):68-72.MIAO Hong,ZUO Dun-wen,Wang Min,et al.Effect of heat treatment on microstructure and properties of cold extruded internal thread of Q460 steel[J].Transactions of Materials and Heat Treatment,2012,33(3):68-72.
• [15]Oliver W C,Pharr G.M.An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments[J].Journal of Materials Research,1992,7(6):1564-1583.
• [16]Kan Q H,Yan W Y,Kang G Z,et al.Oliver-pharr indentation method in determining elastic moduli of shape memory alloys-a phase transformable material[J].Journal of the Mechanics and Physics of Solids,2013,61(10):2015-2033.
• [17]张国尚,荆洪阳,徐连勇,等.纳米压痕法研究80Au/20Sn焊料蠕变应力指数[J].焊接学报,2009,30(8):73-76.ZHANG Guo-shang,JING Hong-yang,XU Lian-yong,et al.Investigation of creep stress exponent of 80Au/20Sn solder by nanoindentation[J].Transactions of the China Welding Institution,2009,30(8):73-76.
• [18]姬峰,薛松柏,刘霜,等.纳米压痕法测量锌铝钎料的室温蠕变应力指数[J].焊接学报,2013,34(2):75-78.JI Feng,XUE Song-bai,LIU Shuang,et al.Measurement of creep stress exponent of Zn-Al filler metal at room temperature by using nanoindentation[J].Transactions of the China Welding Institution,,2013,34(2):75-78.

文章评论(Comment)：