放电等离子烧结温度对ZK61镁合金组织及力学性能的影响Effects of spark plasma sintering temperature on microstructure and mechanical properties of ZK61 magnesium alloy
郝峰晨,崔泽琴,王文先
摘要(Abstract):
以ZK61合金粉末为原料,通过放电等离子烧结的方法制备了ZK61生物镁合金块体,研究了不同烧结温度对合金块体微观组织和力学性能的影响。结果表明:制备出的ZK61合金块体内部结构致密,组织分布均匀,晶粒细小,块体致密度随烧结温度逐渐提高,在520℃时达到99.24%;随着烧结温度的升高,粉末颗粒间原子扩散作用增强,ZK61合金块体的力学性能也逐渐提高,在烧结温度为520℃时综合性能最好,其中显微硬度由370℃时的69.2 HV增加到79.3 HV,抗压强度和抗弯强度也获得最大值,分别为304 MPa和94.7 MPa,压缩率逐渐变大,韧性提高。
关键词(KeyWords): 放电等离子烧结;ZK61镁合金;微观组织;力学性能
基金项目(Foundation): 国家自然科学基金(51305292)
作者(Author): 郝峰晨,崔泽琴,王文先
DOI: 10.13289/j.issn.1009-6264.2017.03.006
参考文献(References):
- [1]Staiger M P,Pietak A M,Huadmai J,et al.Magnesium and its alloys as orthopedic biomaterials:a review[J].Biomaterials,2006,27(9):1728-1734.
- [2]黄晶晶,任伊宾,张炳春,等.镁及镁合金的生物相容性研究[J].稀有金属材料与工程,2007,36(6):1102-1105.HUANG Jing-jing,REN Yi-bin,ZHANG Bing-chun,et al.Study on biocompatility of magnesium and its alloys[J].Rare Metal Materials and Engineering,2007,36(6):1102-1105.
- [3]Song G.Control of biodegradation of biocompatable magnesium alloys[J].Corrosion Science,2007,49(4):1696-1701.
- [4]Li N,Zheng Y.Novel magnesium alloys developed for biomedical application:a review[J].Journal of Materials Science&Technology,2013,29(6):489-502.
- [5]Feng A,Han Y.The microstructure,mechanical and corrosion properties of calcium polyphosphate reinforced ZK60A magnesium alloy composites[J].Journal of Alloys and Compounds,2010,504(2):585-593.
- [6]Gu X N,Li N,Zheng Y F,et al.In vitro degradation performance and biological response of a Mg-Zn-Zr alloy[J].Materials Science and Engineering:B,2011,176(20):1778-1784.
- [7]张修庆,滕新营,王浩伟.镁基复合材料的制备工艺[J].热加工工艺,2004(3):58-61.ZHANG Xiu-qing,TENG Xin-yin,WANG Hao-wei.Preparation technics of magnesium matrix composites materials[J].Hot Working Technology,2004(3):58-61.
- [8]Jiang Q C,Wang H Y,Ma B X,et al.Fabrication of B4C particulate reinforced magnesium matrix composite by powder metallurgy[J].Journal of Alloys and Compounds,2005,386(1):177-181.
- [9]黄海广,张玉勤,蒋业华,等.放电等离子烧结温度对Ti-29Nb-13Ta-4.6Zr合金显微组织和力学性能的影响[J].稀有金属材料与工程,2013,42(6):1173-1177.HUANG Hai-guang,ZHANG Yu-qin,JIANG Ye-hua,et al.Effect of spark plasma sintering temperatures on microstructure and mechanical properties of Ti-29Nb-13Ta-4.6Zr alloy[J].Rare Metal Materials and Engineering,2013,42(6):1173-1177.
- [10]张久兴,刘科高,周美玲.放电等离子烧结技术的发展和应用[J].粉末冶金技术,2002,20(3):129-134.ZHANG Jiu-xing,LIU Ke-gao,ZHOU Mei-ling.Development and application of spark plasma sintering[J].Powder Metallurgy Technology,2002,20(3):129-134.
- [11]Wang L,Zhang J,Jiang W.Recent development in reactive synthesis of nanostructured bulk materials by spark plasma sintering[J].International Journal of Refractory Metals and Hard Materials,2013,39:103-112.
- [12]Orru R,Licheri R,Locci A M,et al.Consolidation/synthesis of materials by electric current activated/assisted sintering[J].Materials Science and Engineering:R:Reports,2009,63(4):127-287.
- [13]王迎春,李树奎,王富耻,等.放电等离子烧结温度对钨合金的组织及动态力学性能的影响[J].稀有金属材料与工程,2010,39(10):1807-1810.WANG Ying-chun,LI Shu-kui,WANG Fu-chi,et al.Effects of spark plasma sintering temperature on microstructure and dynamic mechanical properties of 93W-4.9Ni-2.1Fe alloy[J].Rare Metal Materials and Engineering,2010,39(10):1807-1810.
- [14]Mamedov V.Spark plasma sintering as advanced PM sintering method[J].Powder Metallurgy,2002,45(4):322-328.
- [15]Munir Z A,Quach D V,Ohyanagi M.Electric current activation of sintering:a review of the pulsed electric current sintering process[J].Journal of the American Ceramic Society,2011,94(1):1-19.
- [16]Paraskevas D,Dadbakhsh S,Vleugels J,et al.Solid state recycling of pure Mg and AZ31 Mg machining chips via spark plasma sintering[J].Materials&Design,2016,109:520-529.
- [17]杨伟东,樊建峰,张金玲,等.烧结温度对粉末冶金AZ91镁合金组织及硬度的影响[J].材料热处理学报,2013,34(1):38-42.YANG Wei-dong,FAN Jian-feng,ZHANG Jin-ling,et al.Effect of sintering temperature on microstructure and hardness of powder metallurgy AZ91magnesium alloy[J].Transactions of Materials and Heat Treatment,2013,34(1):38-42.
- [18]Matsugi K,Kuramoto H,Hatayama T,et al.Temperature distribution at steady state under constant current discharge in spark sintering process of Ti and Al2O3powders[J].Journal of Materials Processing Technology,2003,134(2):225-232.
- [19]Omori M.Sintering,consolidation,reaction and crystal growth by the spark plasma system(SPS)[J].Materials Science and Engineering A,2000,287(2):183-188.
- [20]Muhammad W N A W,Sajuri Z,Mutoh Y,et al.Microstructure and mechanical properties of magnesium composites prepared by spark plasma sintering technology[J].Journal of Alloys and Compounds,2011,509(20):6021-6029.
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