固溶温度对CNTs/7075复合材料组织和力学性能的影响Effect of solution temperature on microstructure and mechanical properties of CNTs/7075 composites fabricated by friction stir processing
钱涛,刘奋成,毛育青,刘强,钱鲁泓
摘要(Abstract):
采用搅拌摩擦加工(FSP)方法制备了CNTs/7075铝基复合材料,并对其进行固溶时效热处理,研究固溶温度对CNTs/7075组织和力学性能的影响。通过微观组织观察发现,母材中大颗粒的二次相在FSP中被搅碎,随固溶温度提高,被搅碎的细小的二次相逐渐回溶至基材中,且由于回溶后基体合金元素过饱和度增大,复合材料在时效过程中弥散析出的沉淀相数量增多。复合材料中的CuAl_2在固溶过程中回溶入基体中形成过饱和固溶体,在随后时效过程中析出η相(MgZn_2)以及少量S相(Al_2CuMg)。CNTs/7075复合材料的抗拉强度和伸长率随固溶温度升高先上升后下降,当固溶温度为470℃时,抗拉强度相对较高,达到550 MPa,高于母材,伸长率为3.4%,表现为脆性解理断裂。
关键词(KeyWords): CNTs/7075;搅拌摩擦加工;固溶温度;组织;力学性能
基金项目(Foundation): 国家自然科学基金(51565041,51365044,51465044);; 江西省教育厅科研项目(GJJ150710)
作者(Author): 钱涛,刘奋成,毛育青,刘强,钱鲁泓
DOI: 10.13289/j.issn.1009-6264.2016.s1.004
参考文献(References):
- [1]刘兵,彭超群,王日初,等.大飞机用铝合金的研究现状及展望[J].中国有色金属学报,2010(9):1705-1715.LIU Bing,PENG Chao-qun,WANG Ri-chu,et al.Recent development and prospects for giant plane aluminum alloys[J].The Chinese Journal of Nonferrous Metals,2010(9):1705-1715.
- [2]Izadi H,Gerlich A P.Distribution and stability of carbon nanotubes during multi-pass friction stir processing of carbon nanotube/aluminum composites[J].Carbon,2012,50(12):4744-4749.
- [3]Liu Q,Ke L M,Liu F C,et al.Microstructure and mechanical property of multi-walled carbon nanotubes reinforced aluminum matrix composites fabricated by friction stir processing[J].Materials&Design,2013,45:343-348.
- [4]Liu Z Y,Xiao B L,Wang W G,et al.Singly dispersed carbon nanotube/aluminum composites fabricated by powder metallurgy combined with friction stir processing[J].Carbon,2012,50(5):1843-1852.
- [5]Goh C S,Wei J,Lee L C,et al.Development of novel carbon nanotube reinforced magnesium nanocomposites using the powder metallurgy technique[J].Nanotechnology,2006,17(1):7-12.
- [6]程南璞,曾苏民,李萍,等.Si CP/Al复合材料热处理及统计分析[J].材料热处理学报,2007,28(5):15-19.CHENG Nan-pu,ZENG Su-min,LI Ping,et al.Heat treatment and statistical analysis of Si CP/Al composite[J].Transactions of Materials and Heat Treatment,2007,28(5):15-19.
- [7]范才河,陈刚,严红革,等.喷射共沉积7075/Si Cp复合材料热处理工艺的研究[J].矿冶工程,2006,26(2):106-108.FAN Cai-he,CHEN Gang,YAN Hong-ge,et al.Heat treatment of 7075/Si Cp composite bu spray co-deposition[J].Mining and Metallurgical Engineering,2006,26(2):106-108.
- [8]Nam D H,Kim Y K,Cha S I,et al.Effect of CNTs on precipitation hardening behavior of CNT/Al-Cu composites[J].Carbon,2012,50(13):4809-4814.
- [9]苏鸿英.美国铝合金热处理工艺技术的进展[J].有色金属工业,2003,(8):62.SU Hong-ying.American aluminum alloy heat treatment technology progress[J].China Nonferrous Metals,2003,(8):62.
- [10]Rhodes C G,Mahoney M W,Bingel W H,et al.Effects of friction stir welding on microstructure of 7075 aluminum[J].Scripta Materialia,1997,36(1):69-75.
- [11]赵青.热处理工艺对7075铝合金组织和力学性能的影响[D].郑州:郑州大学,2012.
- [12]李念奎,凌杲,聂波,等.铝合金材料及其热处理技术[M].北京:冶金工业出版社,2012,4.
- [13]Liu Z Y,Xiao B L,Wang W G,et al.Analysis of carbon nanotube shortening and composite strengthening in carbon nanotube/aluminum composites fabricated by multi-pass friction stir processing[J].Carbon,2014,69:264-274.
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