非对称双极脉冲磁控溅射制备Ti-Co-La-N纳米薄膜性能(英文)Properties of Ti-Co-La-N nano-films deposited by asymmetric bipolar pulsed reactive magnetron sputtering
李成明,陈良贤,刘政,黑立富,吕反修
摘要(Abstract):
利用非对称双极脉冲磁控溅射制备了不用Co-La掺杂量的Ti-Co-La-N纳米复合薄膜。分别用扫描电子显微镜、X射线衍射、纳米压痕仪、划痕仪以及摩擦磨损仪研究了薄膜的表面形貌、结合力、显微硬度和摩擦学性能。结果表明:复合薄膜主要有TiN相、Co2N相和LaN相组成;复合膜的纤维硬度达到14.61GPa,低于TiN的显微硬度;复合薄膜的显微硬度和结合力都随着Co-La掺杂量的增加而降低;在高速钢基体上复合薄膜的摩擦系数达到了0.6。
关键词(KeyWords): 纳米复合;Co-La掺杂;TiN
基金项目(Foundation):
作者(Author): 李成明,陈良贤,刘政,黑立富,吕反修
DOI: 10.13289/j.issn.1009-6264.2010.09.033
参考文献(References):
- [1]Rizzo A,Signore M A,Riccardis M F,et al.Influence of growth rate on the structural and morphological properties of TiN,ZrN and TiN/ZrN multilayers[J].Thin Solid Films,2007,515:6665-6671.
- [2]Braic M,Balaceanu M,Vladescu et al.TiN/ZrN heterostructures deposition and characterization[J].Surface and Coatings Technology,2006,200:6505-6510.
- [3]Barshilia H C,Rajam K S,Jain A,et al.A comparative study on the structure and properties of nanolayered TiN/NbN and TiAlN/TiN multilayer coatings prepared by reactive direct current magnetron sputtering[J].Thin Solid Films,2006,503:158-166.
- [4]Chen J T,Wang J,Zhang F,et al.Characterization and temperature controlling property of TiAlN coatings deposited by reactive magnetron co-sputtering[J].Journal of Alloys and Compounds,2009,472:91-96.
- [5]Fox-Rabinovich G S,Yamomoto K,Veldhuis S C.Tribological adaptability of TiAlCrN PVD coatings under high performance dry machining conditions[J].Surface and Coatings Technology,2005,200:1804-1813.
- [6]Santana A E,Karimi A,Derflinger V H,et al.Microstructure and mechanical behavior of TiAlCrN multilayer thin films[J].Surface and Coatings Technology,2004,177-178:334-340.
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